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2617-47-2

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Basic Information
CAS No.: 2617-47-2
Name: HYDROXYMETHYL PHOSPHONIC ACID
Article Data: 29
Molecular Structure:
Molecular Structure of 2617-47-2 (HYDROXYMETHYL PHOSPHONIC ACID)
Formula: CH5 O4 P
Molecular Weight: 112.022
Synonyms: Phosphonicacid, (hydroxymethyl)- (6CI,7CI,8CI,9CI); (Hydroxymethyl)phosphonate;(Hydroxymethyl)phosphonic acid; Hydroxymethanephosphonic acid;Methanehydroxyphosphonic acid; NSC 41905; NSC 63035; Phosphonomethanol
Density: 1.815g/cm3
Melting Point: 95-97℃
Boiling Point: 413°Cat760mmHg
Flash Point: 203.6°C
PSA: 87.57000
LogP: -0.88610
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Conditions
ConditionsYield
Stage #1: 2,2'-oxybis-acetic acid With methanesulfonic acid; phosphorus trichloride at 50 - 80℃; for 3h; Inert atmosphere;
Stage #2: With water at 120℃; for 2h; Inert atmosphere;
Stage #3: With sodium hydroxide at 140℃; for 2h; Inert atmosphere;		A n/a
B 34.9%
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B

C4H9NO7P2(4-)*4Na(1+)

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hydroxymethylphosphonic acid

Conditions
ConditionsYield
With sodium hydroxide In Tetraethylene glycol dimethyl ether; water at 90℃; for 22h;A 81.2 %Spectr.
B 13.5%
C 5.3 %Spectr.
With sodium hydroxide In methanol; water at 90℃; for 22h;A 83.1 %Spectr.
B 10.3%
C 6.5 %Spectr.
With sodium hydroxide In water; glycerol at 90℃; for 22h;A 87.8 %Spectr.
B 8.5%
C 3.7 %Spectr.
...Expand
50-00-0

formaldehyd

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With phosphorus trichloride und anschliessenden Behandeln mit Wasser;
With phosphonic Acid; triethylamine
With phosphorus; diethylamine
With P4O6 inert solvent; Yield given;
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Trimethyl borate

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With phosphorus pentachloride; oxygen at 0℃;
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chloromethylphosphonic acid

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With water at 250℃;
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(phenylmethoxy)methylphosphonic acid diethyl ester

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With hydrogenchloride at 100 - 150℃;
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2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With hydrogenchloride
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diethyl (1-hydroxymethyl)phosphonate

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With hydrogenchloride
Stage #1: diethyl (1-hydroxymethyl)phosphonate With boron tribromide In hexane; toluene at 70℃; for 6h;
Stage #2: With methanol In hexane; toluene at 20℃;
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(diethoxyphosphanyloxy-methyl)-phosphonic acid diethyl ester

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With hydrogenchloride
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formaldehyd

A

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nitrilo-tris(methylenephosphonic acid)

B

2617-47-2

hydroxymethylphosphonic acid

Conditions
ConditionsYield
With ammonium chloride; phosphorus trichloride Mechanism;
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