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Detail of "28299-41-4"

  • CAS Number:
  • 28299-41-4
  • Name:
  • Benzene,1,1'-oxybis[methyl-

  • Molecular Structure:
  • Formula:
  • C14H14 O
  • Molecular Weight:
  • 198.26
  • Synonyms:
  • Tolyl ether(7CI,8CI); Baylectrol 4900; Dicresyl ether; Dimethyldiphenyl ether; Ditolylether
  • Density:
  • 1.029g/cm3
  • Melting Point:
  • 47-49 °C(lit.)
  • Boiling Point:
  • 285 °C(lit.)
  • Flash Point:
  • 114.3°C
  • Safety:
  • WGK Germany 2
    RTECS DA6625000
    Details

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Reference

Azo dyes
Azo dyes. Moells, Han Heinz; Schiwy, Willy; Hoernle, Reinhold; Nebeling, Reinhard (Bayer A.-G., Ger.). Ger. Offen. DE 2607122 25 Aug 1977, 25 pp. (German). (Germany). CODEN: GWXXBX. CLASS: IC: C09B041-00. APPLICATION: DE 76-2607122 21 Feb 1976. DOCUMENT TYPE: Patent CA Section: 40 (Dyes, Fluorescent Whitening Agents, and Photosensitizers) Neg. substituted aniline derivs. are diazotized in the presence of a reaction product of a H2SO4, HCHO, and ditolyl ether [28299-41-4], biphenyl [92-52-4], or naphthalene [91-20-3], coupled with the desired coupler, neutralized with aq. NaOH, milled, and spray dried to give a azo dye compn. which is easily dispersible in H2O. Another related process which combines azo components and couples is described.
Sulfonated aromatic reaction products useful in tanning leather
Sulfonated aromatic reaction products useful in tanning leather. Wuermli, Albert (Ciba-Geigy A.-G., Switz.). Ger. Offen. DE 2717141 10 Nov 1977, 55 pp. (German). (Germany). CODEN: GWXXBX. CLASS: IC: C08G008-18. PRIORITY: CH 76-5046 22 Apr 1976. DOCUMENT TYPE: Patent CA Section: 41 (Leather and Related Materials) The title tanning materials comprised 100 parts sulfonated product from 10-90% Me-substituted di-Ph ether and 90-10% Me-substituted PhOH (1 mol of product) contg. 1-2 mols. sulfonating agent, e.g. H2SO4, and 1-6 parts HCHO, or 4-24 parts mixt. of an aminoplast and HCHO, or 4-24 parts aminoplast precondensate. Thus, 300 parts ditolyl ether [28299-41-4] and 500 parts PhOH [108-95-2] were mixed and sulfonated 3 h at 125-30° with 765 parts oleum, the sulfonated mixt. was heated 5 h at 160° and reduced pressure of 15 torr, 100 parts of the product was dissolved in 20 parts H2O, 5 parts of a 30% aq. HCHO soln. was added and heated 2 h at 80-5°, the condensate was dild. with 85 parts H2O and adjusted to pH 4.0 with 44 parts 25% aq. NH3 soln., and 6 parts 85% HCO2H were added to give 255 parts of a red-brown colored, clear, thin sirup contg. solids 43.7, tannins 27.4, and nontannins 16.3%.
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