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28343-22-8

Basic Information
CAS No.: 28343-22-8
Name: Phenol, 4-ethenyl-2,6-dimethoxy-
Article Data: 32
Molecular Structure:
Molecular Structure of 28343-22-8 (Phenol, 4-ethenyl-2,6-dimethoxy-)
Formula: C10H12 O3
Molecular Weight: 180.203
Synonyms: Phenol,2,6-dimethoxy-4-vinyl- (8CI); 2,6-Dimethoxy-4-ethenylphenol;2,6-Dimethoxy-4-vinylphenol; 3,5-Dimethoxy-4-hydroxystyrene;4-Vinyl-2,6-dimethoxyphenol; 4-Vinylsyringol; Canolol; Syringlyethene;Vinylsyringol
Density: 1.113g/cm3
Boiling Point: 285.4°Cat760mmHg
Flash Point: 126.4°C
PSA: 38.69000
LogP: 2.05240
Synthetic route
530-59-6

sinapinic acid

28343-22-8

canolol

Conditions
ConditionsYield
With Cocos nucifera juice at 20℃; for 48h; Inert atmosphere;94%
With aluminum oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinone In methanol for 0.25h; microwave irradiation;84%
With 1,10-Phenanthroline; copper hydroxide In 1-methyl-pyrrolidin-2-one at 130℃; for 1.1h; Inert atmosphere; Green chemistry;31%
33900-62-8

1-(4-Hydroxy-3,5-dimethoxyphenyl)ethanol

28343-22-8

canolol

Conditions
ConditionsYield
With MoO2Cl2(DMSO)2; dimethyl sulfoxide for 0.166667h; Microwave irradiation;90%
With MoO2(2+)*C2H6OS*2Cl(1-) In dimethyl sulfoxide for 0.166667h; Microwave irradiation;90%
With 1-hexyl-3-methyl-1-imidazolium bromide at 150℃; for 0.25h; Microwave irradiation;
141-82-2

malonic acid

134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
With pyridine; acetic acid at 130℃; for 0.116667h; microwave irradiation;67%
With piperidine In 1-methyl-pyrrolidin-2-one for 3h; Reflux;67.5%
With piperidine In toluene at 115℃; Knoevenagel-Doebner-Stobbe Reaction;47%
134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
With Methyltriphenylphosphonium bromide; sodium hexamethyldisilazane In tetrahydrofuran for 5.5h; Cooling;59%
1779-49-3

Methyltriphenylphosphonium bromide

134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With sodium hexamethyldisilazane In tetrahydrofuran for 1.5h; Cooling;
Stage #2: syringic aldehyde In tetrahydrofuran for 4h;
18%
forest plant material

forest plant material

A

91-10-1

1,3-dimethoxy-2-hydroxy-benzene

B

6638-05-7

2,6-dimethoxy-4-methylphenol

C

14059-92-8

4-ethylsyringol

D

28343-22-8

canolol

Conditions
ConditionsYield
With air Oxidation; Formation of xenobiotics; Further byproducts given;
1252786-17-6

C4H11N*C11H12O5

A

1252786-39-2

C4H11N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 51 %Spectr.
B 5 %Spectr.

C4H11NO*C11H12O5

A

C4H11NO*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 50 %Spectr.
B 5 %Spectr.
1252786-19-8

C2H7NO*C11H12O5

A

1252786-41-6

C2H7NO*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 15 %Spectr.
B 7 %Spectr.
1252786-21-2

C5H11N*C11H12O5

A

1252786-43-8

C5H11N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 67 %Spectr.
B 4 %Spectr.
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