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28973-48-0

Basic Information
CAS No.: 28973-48-0
Name: (9alpha,13alpha,14alpha)-3-methoxymorphinan-17-carbaldehyde
Article Data: 8
Molecular Structure:
Molecular Structure of 28973-48-0 ((9alpha,13alpha,14alpha)-3-methoxymorphinan-17-carbaldehyde)
Formula: C18H23 N O2
Molecular Weight: 285.386
Synonyms: 9a,13a,14a-Morphinan-17-carboxaldehyde, 3-methoxy- (8CI);(+)-3-Methoxy-N-formylmorphinan; (+)-N-Formyl-3-methoxymorphinan
Density: 1.18g/cm3
Boiling Point: 473.9°Cat760mmHg
Flash Point: 240.4°C
PSA: 29.54000
LogP: 3.48380
Synthetic route
29144-31-8

(S)-2-Formyl-1-<(4-methoxyphenyl)methyl>-1,2,3,4,5,6,7,8-octahydroispquinoline

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
With phosphoric acid In neat (no solvent) at 80℃; for 10h; Reagent/catalyst; Temperature; Time; Green chemistry;98%
125-71-3

dextromethorphan

B

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
With oxygen; lithium perchlorate; 9,10-Dicyanoanthracene In acetonitrile at 20℃; Irradiation;A 83 % Spectr.
B 10 % Spectr.
With oxygen; 9,10-Dicyanoanthracene In acetonitrile at 20℃; Irradiation;A 43 % Spectr.
B 57 % Spectr.
With potassium carbonate; tris(p-bromophenyl)aminium hexafluorophosphate In water; acetonitrile at -20℃; Solvent; Reagent/catalyst; Temperature; Inert atmosphere;
36397-14-5

(+)-3-methoxymorphinan hydrochloride

109-94-4

formic acid ethyl ester

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
With ammonium hydroxide; formic acid Heating; Yield given;

dextromethorphan hydrobromide

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / a.) 20percent aq. NH4OH, b.) K2CO3, 1-chloroethyl chloroformate / 1,2-dichloro-ethane / 6 h / Heating
2: a.) 20percent aq. NH4OH, b.) 100percent HCOOH / Heating
View Scheme
104-01-8

4-Methoxyphenylacetic acid

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 5 h / 150 °C
2: POCl3 / benzene / Heating
3: pyridine; tetrahydrofuran / 8 h / 0 °C
4: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr
View Scheme
51072-35-6

1-(4-methoxybenzyl)-3,4,5,6,7,8-hexahydro-isoquinoline

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; tetrahydrofuran / 8 h / 0 °C
2: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr
View Scheme
51072-34-5

N-(2-cyclohex-1-enylethyl)-2-(4-methoxyphenyl)-acetamide

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: POCl3 / benzene / Heating
2: pyridine; tetrahydrofuran / 8 h / 0 °C
3: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr
View Scheme
116172-20-4

(Z)-2-Formyl-1-<(4-methoxyphenyl)methylene>-1,2,3,4,5,6,7,8-octahydroisoquinoline

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr
View Scheme
3399-73-3

2-(1-cyclohexenyl)ethylamine

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 5 h / 150 °C
2: POCl3 / benzene / Heating
3: pyridine; tetrahydrofuran / 8 h / 0 °C
4: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr
View Scheme

(-)-octabase mandelate salt

28973-48-0

(+)-3-methoxy-N-formylmorphinan

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 48 h / Reflux
2: phosphoric acid / neat (no solvent) / 10 h / 80 °C / Green chemistry
View Scheme
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    (9A,13A,14A)-3-METHOXYMORPHINAN-17-CARBALDEHYDECAS

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    Morphinan-17-carboxaldehyde,3-methoxy-, (9a,13a,14a)- (9CI)

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    (9alpha,13alpha,14alpha)-3-methoxymorphinan-17-carbaldehyde

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    N-Formyl Dextromethorphan

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    (9alpha,13alpha,14alpha)-3-methoxymorphinan-17-carbaldehyde

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  • Casno:

    28973-48-0

    N-Formyl Dextromethorphan

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    N-Formyl DextromethorphanAppearance:detailed in specifications Storage:Keep in dry and cool place Package:according to clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis,Pharmaceuticals, Agroche

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    28973-48-0

    N-Formyl Dextromethorphan

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  • Casno:

    28973-48-0

    (9alpha,13alpha,14alpha)-3-methoxymorphinan-17-carbaldehyde

    Min.Order: 0

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    Zhejiang Jiuzhou Chemical Co.,Ltd is a market-oriented and innovation-driven biopharmaceutical company. The company is focusing on the R&D, manufacturing and sales of pharmaceutica

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  • Morphinan-17-carboxaldehyde,3-methoxy-, (9a,13a,14a)- (9CI)-

  • Casno:

    28973-48-0

    Morphinan-17-carboxaldehyde,3-methoxy-, (9a,13a,14a)- (9CI)-

    Min.Order: 1 Gram

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    HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

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