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290297-26-6

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CAS No.: 290297-26-6
Name: 2-[3,5-bis(trifluoromethyl)phenyl]-N,2-dimethyl-N-[4-(2-methylphenyl)-6-(4-methylpiperazin-1-yl)pyridin-3-yl]propanamide
Article Data: 12
Molecular Structure:
Molecular Structure of 290297-26-6 (2-[3,5-bis(trifluoromethyl)phenyl]-N,2-dimethyl-N-[4-(2-methylphenyl)-6-(4-methylpiperazin-1-yl)pyridin-3-yl]propanamide)
Formula: C30H32 F6 N4 O
Molecular Weight: 578.601
Synonyms: 2-[3,5-Bis(trifluoromethyl)phenyl]-N-[6-(4-methylpiperazin-1-yl)-4-o-tolylpyridin-3-yl]-N-methylisobutyramide;Netupitant; Ro 67-31898/000
Density: 1.255
Melting Point: 156.2-160.0 °C
Boiling Point: 597.4°C at 760 mmHg
Flash Point: 315.1°C
PSA: 39.68000
LogP: 6.78990
Related products
Synthetic route
290297-25-5

methyl-[6-(4-methyl-piperazin-1-yl)-4-o-tolyl-pyridin-3-yl]-amine

289686-69-7

2-(3,5-bis-trifluoromethyl-phenyl)-2-methyl-propionyl chloride

290297-26-6

netupitant

Conditions
ConditionsYield
With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine In dichloromethane at 35 - 40℃; for 3h; Cooling with ice;81%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 35 - 40℃; for 3h; Cooling with ice;81%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 10℃; for 2h;74%
109-01-3

1-methyl-piperazine

401891-55-2

2-(3,5-bis(trifluoromethyl)phenyl)-N-(6-chloro-4-(o-tolyl)pyridin-3-yl)-N,2-dimethylpropanamide

290297-26-6

netupitant

Conditions
ConditionsYield
With potassium carbonate In dichloromethane at 80℃; for 3h;80%

2-[3,5-bis(trifluoromethyl)phenyl]-2-methylpropionyl chloride

290297-25-5

methyl-[6-(4-methyl-piperazin-1-yl)-4-o-tolyl-pyridin-3-yl]-amine

290297-26-6

netupitant

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane Heating;
109-01-3

1-methyl-piperazine

Merrifield resin-OC(O)CH2CH2CH(OH)CH2I

Merrifield resin-OC(O)CH2CH2CH(OH)CH2I

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 2 h / 100 °C
2: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
3: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
4: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme

6-chloro-4-o-tolyl-nicotinoyl chloride

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 7.8 g / NH3 / tetrahydrofuran; H2O / 0.5 h / 0 °C
2: 2 h / 100 °C
3: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
4: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
5: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
342417-00-9

6-chloro-4-(o-tolyl)nicotinamide

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 2 h / 100 °C
2: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
3: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
4: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
Multi-step reaction with 4 steps
1.1: 2 h / 100 °C
2.1: N-Bromosuccinimide / methanol; dichloromethane / 6 h / -5 °C
2.2: 5.33 h / 5 °C
3.1: dichloromethane; toluene / 2 h / 50 °C
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
Multi-step reaction with 4 steps
1.1: 2 h / 100 °C
2.1: N-Bromosuccinimide / methanol; dichloromethane / 16 h / -5 °C
2.2: 5.3 h / -5 °C
3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 2 h / 50 °C
4.1: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
342416-99-3

6-chloro-4-o-tolyl-nicotinic acid

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: SOCl2; DMF / tetrahydrofuran / 2.5 h / 50 °C
2: 7.8 g / NH3 / tetrahydrofuran; H2O / 0.5 h / 0 °C
3: 2 h / 100 °C
4: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
5: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
6: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
Multi-step reaction with 5 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / 50 °C
1.2: 0.5 h / 0 °C
2.1: 2 h / 100 °C
3.1: N-Bromosuccinimide / methanol; dichloromethane / 6 h / -5 °C
3.2: 5.33 h / 5 °C
4.1: dichloromethane; toluene / 2 h / 50 °C
5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
Multi-step reaction with 5 steps
1.1: thionyl chloride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 50 °C
1.2: 0.5 h / 0 °C
2.1: 2 h / 100 °C
3.1: N-Bromosuccinimide / methanol; dichloromethane / 16 h / -5 °C
3.2: 5.3 h / -5 °C
4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 2 h / 50 °C
5.1: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
342417-04-3

N-tert-butyl-6-chloro-4-(o-tolyl)nicotinamide

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 4 h / 100 °C
2: MeSO3H / 5 h / 100 °C
3: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
4: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
5: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
Multi-step reaction with 5 steps
1: 100 °C
2: methanesulfonic acid / 100 °C
3: N-Bromosuccinimide / dichloromethane / -5 °C
4: RedAl / toluene / 50 °C
5: N-ethyl-N,N-diisopropylamine / dichloromethane / 40 °C
View Scheme
342417-01-0

4-(2-methylphenyl)-6-(4-methylpiperazinyl)-3-pyridinecarboxamide

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 99 percent / N-bromosuccinimide / CH2Cl2; methanol / 7 h / -5 °C
2: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
3: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / dichloromethane / -5 °C
2: RedAl / toluene / 50 °C
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 40 °C
View Scheme
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide / methanol; dichloromethane / 6 h / -5 °C
1.2: 5.33 h / 5 °C
2.1: dichloromethane; toluene / 2 h / 50 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide / methanol; dichloromethane / 16 h / -5 °C
1.2: 5.3 h / -5 °C
2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 2 h / 50 °C
3.1: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
342417-02-1

[6-(4-methyl-piperazin-1-yl)-4-o-tolylpyridin-3-yl]-carbamic acid methyl ester

290297-26-6

netupitant

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Red-Al / toluene; CH2Cl2 / 1 h / 50 °C
2: 13.5 g / i-Pr2NEt / CH2Cl2 / 3 h / 0 °C
View Scheme
Multi-step reaction with 2 steps
1: RedAl / toluene / 50 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 40 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 2 h / 50 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C
View Scheme
Multi-step reaction with 2 steps
1: dichloromethane; toluene / 2 h / 50 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
Multi-step reaction with 2 steps
1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 2 h / 50 °C
2: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 - 40 °C / Cooling with ice
View Scheme
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    Product Name： 2-[3,5-bis(trifluoromethyl)phenyl]-N,2-dimethyl-N-[4-(2-methylphenyl)-6-(4-methylpiperazin-1-yl)pyridin-3-yl]propanamideChemicalBook Assay： 99.0% Cas No.： 290297-26-6

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  •  CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-519-88802789

    Address:No.300,Yanling Middle Road, Changzhou, Jiangsu, China

       Inquiry Now

  • Netupitant cas no. 290297-26-6 98%

  • Casno:

    290297-26-6

    Netupitant cas no. 290297-26-6 98%

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

    Established in 2007, Win-Win chemical CO., Ltd is a privately held corporation headquartered in Wenzhou Longwan Industry Distric, dedicated to the global pharmaceutical companies a

  •  Win-Win chemical Co.Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-577-64498589

    Address:No.49 YuShi West Road, Longwan District,325000

       Inquiry Now

  • Netupitant

  • Casno:

    290297-26-6

    Netupitant

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food, cosmetics and other fine chemicals. Our products including but not li

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food,

  •  Koning Pharmchem Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-574-87369228

    Address:Lingqiao Road

       Inquiry Now

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