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Basic Information
| CAS No.: | 29390-67-8 |
|---|---|
| Name: | 6-Monodeoxy-6-monoamino-beta-cyclodextrine |
| Article Data: | 71 |
| Molecular Structure: | |
|
|
|
| Formula: | C42H71 N O34 |
| Molecular Weight: | 1134.01 |
| Synonyms: | 2,4,7,9,12,14,17,19,22,24,27,29,32,34-Tetradecaoxaoctacyclo[31.2.2.23,6.28,11.213,16.218,21.223,26.228,31]nonatetracontane,b-cyclodextrin deriv.;6-Amino-6-deoxy-b-cyclodextrin;6-Amino-6-deoxycyclomaltoheptaose; 6-Deoxy-6-amino-b-cyclodextrin; 6-Monoamino-b-cyclodextrin; 6-Monodeoxy-6-monoamino-b-cyclodextrin; 6A-Amino-6A-deoxy-b-cyclodextrin;Mono(6-amino-6-deoxy)-b-cyclodextrin; Mono(6-deoxy-6-amino)-b-cyclodextrin |
| Density: | 1.608±0.06 g/cm3(Predicted) |
| Melting Point: | 203 °C (decomp) |
| Boiling Point: | 1527.8±60.0 °C(Predicted) |
| PSA: | 559.84000 |
| LogP: | -14.56390 |
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Synthetic route
- 98169-85-8
mono(6-azido-6-deoxy)β-cyclodextrin
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| With triphenylphosphine In N,N-dimethyl-formamide for 1h; Ambient temperature; | 99% |
| Stage #1: mono(6-azido-6-deoxy)β-cyclodextrin With triphenylphosphine In N,N-dimethyl-formamide for 2h; Stage #2: With water In N,N-dimethyl-formamide for 0.5h; Heating; | 97% |
| Stage #1: mono(6-azido-6-deoxy)β-cyclodextrin With triphenylphosphine In N,N-dimethyl-formamide at 20℃; Stage #2: With ammonium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 95% |
- 67217-55-4
mono-6-deoxy-6-(p-tolylsulphonyl)-β-cyclodextrin
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| With ammonia In water at 20℃; for 168h; | 90% |
| With ammonium hydroxide In water at 50℃; for 72h; | 79% |
| With ammonium hydroxide In water at 85℃; for 0.5h; Microwave irradiation; | 60% |
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| With ammonium hydroxide In water at 20℃; | 88% |
- 67217-55-4
mono-6-deoxy-6-(p-tolylsulphonyl)-β-cyclodextrin
A
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
B
- 7585-39-9
β‐cyclodextrin
Conditions
| Conditions | Yield |
|---|---|
| With ammonia In water at 60℃; for 5h; Product distribution / selectivity; | A 70% B 30% |
- 98169-85-8
mono(6-azido-6-deoxy)β-cyclodextrin
A
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
B
- 7585-39-9
β‐cyclodextrin
Conditions
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; triphenylphosphine 1) DMF; Yield given. Multistep reaction. Yields of byproduct given; |
- 138435-33-3
6-deoxy-6-(N-hydroxylamino)-β-cyclodextrin
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In water under 1292.9 Torr; for 20h; |
Conditions
| Conditions | Yield |
|---|---|
| With water In various solvent(s) at 25℃; pH=4.0; Kinetics; Further Variations:; Reagents; |
A
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| In water-d2 at 25℃; Equilibrium constant; |
- 7585-39-9
β‐cyclodextrin
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: β‐cyclodextrin With p-toluenesulfonyl chloride In pyridine Stage #2: With sodium azide In N,N-dimethyl-formamide Stage #3: With palladium on activated charcoal; hydrazine hydrate |
- 79-34-5
1,1,2,2-tetrachloroethane
- 29390-67-8
6(I)-amino-6(I)-deoxycyclomaltoheptaose
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide; triphenylphosphine In [(2)H6]acetone; water |
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