CAS No.2956-58-3,N,N'-ETHYLENEBISACRYLAMIDE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	2956-58-3
Name:	N,N'-ETHYLENEBISACRYLAMIDE
Article Data:	13

Formula:	C₈H₁₂N₂O₂
Molecular Weight:	168.195
Synonyms:	Acrylamide,N,N'-ethylenebis- (6CI,7CI,8CI);Ethylenebisacrylamide;N,N'-Bisacryloylethylenediamine;N,N'-Diacryloyl-1,2-diaminoethane;N,N'-Ethylenebisacrylamide;
Density:	1.034 g/cm³
Melting Point:	138-140 °C(lit.)
Boiling Point:	456.3 °C at 760 mmHg
Flash Point:	213 °C
Solubility:	Soluble in water and methanol.
Appearance:	WHITE TO OFF-WHITE TO FAINT RED POWDER,CRYSTALS OR CRYSTALLINE POWDER
Hazard Symbols:	Xi,Xn,F
Risk Codes:	36/37/38-40-11
Safety:	26-36/37/39-20
PSA:	58.20000
LogP:	0.37260

Synthetic route

: 107-15-3
ethylenediamine

: 814-68-6
acryloyl chloride

A: 2956-58-3
N,N'-ethylenebisacrylamide

B: 333-18-6
1,2-diaminoethane dihydrochloride

Conditions

Conditions	Yield
In acetonitrile for 2h; Ambient temperature;	A 85% B n/a

...Expand

: 107-15-3
ethylenediamine

: 814-68-6
acryloyl chloride

: 2956-58-3
N,N'-ethylenebisacrylamide

Conditions

Conditions	Yield
With sodium acetate; hydroquinone In chloroform for 1h; Heating;	80%
With 4-methoxy-phenol In dichloromethane at 0 - 5℃; for 6h;	56%
With sodium hydroxide In water; acetonitrile at 20℃; for 6h; Cooling with ice;	40%
With sodium acetate In chloroform at 0 - 60℃; for 2.33h;	36%
With triethylamine In chloroform

: 107-15-3
ethylenediamine

: 79-10-7
acrylic acid

: 74-86-2
acetylene

: 2956-58-3
N,N'-ethylenebisacrylamide

Conditions

Conditions	Yield
With carbon monoxide; tetracarbonyl nickel; acetone

...Expand

N.N'-bis-<3-chloro-propionyl>-ethylenediamine: N.N'-bis-<3-chloro-propionyl>-ethylenediamine

: 2956-58-3
N,N'-ethylenebisacrylamide

Conditions

Conditions	Yield
With potassium hydroxide at 85 - 90℃;

: 2680-03-7
N,N-Dimethylacrylamide

: 2956-58-3
N,N'-ethylenebisacrylamide

: 2-methoxy-6-[(4-vinyl)benzyloxy]benzylamine hydrochloride

polymer, reverse-phase suspension copolymerization, NH2 content 305 μmol/g; monomer(s): 2-methoxy-6-[(4-vinyl)benzyloxy]benzylamine hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide: polymer, reverse-phase suspension copolymerization, NH2 content 305 μmol/g; monomer(s): 2-methoxy-6-[(4-vinyl)benzyloxy]benzylamine hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide

Conditions

Conditions	Yield
With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate; N,N-dimethyl-formamide In tetrachloromethane; hexane; water at 35℃; for 120h;	99%

...Expand

: 591-50-4
iodobenzene

: 2956-58-3
N,N'-ethylenebisacrylamide

: 37946-57-9
N,N'-Dicinnamoyl-ethylendiamin

Conditions

Conditions	Yield
With PNODAM-5 catalyst In n-heptane; N,N-dimethyl acetamide at 100℃; Heck reaction;	96%

: 2680-03-7
N,N-Dimethylacrylamide

: 2956-58-3
N,N'-ethylenebisacrylamide

: 4-(2-aminoethyl)styrene hydrochloride

polymer, reverse-phase suspension copolymerization, NH2 content 932 μmol/g; monomer(s): 4-(2-aminoethyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide: polymer, reverse-phase suspension copolymerization, NH2 content 932 μmol/g; monomer(s): 4-(2-aminoethyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide

Conditions

Conditions	Yield
With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.75h;	92%

...Expand

: 2680-03-7
N,N-Dimethylacrylamide

: 2956-58-3
N,N'-ethylenebisacrylamide

: 4-aminomethylstyrene hydrochloride

polymer, reverse-phase suspension copolymerization, NH2 content 696 μmol/g; monomer(s): 4-aminomethylstyrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide: polymer, reverse-phase suspension copolymerization, NH2 content 696 μmol/g; monomer(s): 4-aminomethylstyrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide

Conditions

Conditions	Yield
With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.5h;	92%

...Expand

: 2680-03-7
N,N-Dimethylacrylamide

: 2956-58-3
N,N'-ethylenebisacrylamide

: 4-(4-aminobutyl)styrene hydrochloride

polymer, reverse-phase suspension copolymerization, NH2 content 894 μmol/g; monomer(s): 4-(4-aminobutyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide: polymer, reverse-phase suspension copolymerization, NH2 content 894 μmol/g; monomer(s): 4-(4-aminobutyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide

Conditions

Conditions	Yield
With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.5h;	92%

...Expand

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 2956-58-3
N,N'-ethylenebisacrylamide

: 3-(1,4,8,11tetraaza-cyclotetradec-1-yl)-N-[2-(3-1,4,8,11tetraaza-cyclotetradec-1-yl-propionylamino)-ethyl]-propionamide

Conditions

Conditions	Yield
With 2,4-di-tert-Butylphenol; toluene-4-sulfonic acid In chloroform Ambient temperature; 2-4d;	82%

Total:70 Page 1 of 2 1 2 Next>>

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Specification

The 2-Propenamide,N,N'-1,2-ethanediylbis-, with the CAS registry number 2956-58-3, is also known as N,N'-Ethylenebis(acrylamide). It belongs to the product category of Anilines, Aromatic Amines and Nitro Compounds. This chemical's molecular formula is C₈H₁₂N₂O₂ and molecular weight is 168.19308. Its IUPAC name is called N-[2-(prop-2-enoylamino)ethyl]prop-2-enamide. The product should be sealed and stored in cool and dry place at temperature of 2-8 °C.

Physical properties of 2-Propenamide,N,N'-1,2-ethanediylbis-: (1)ACD/LogP: -1.28; (2)ACD/LogD (pH 5.5): -1.28; (3)ACD/LogD (pH 7.4): -1.28; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 4.82; (7)ACD/KOC (pH 7.4): 4.82; (8)#H bond acceptors: 4; (9)#H bond donors: 2; (10)#Freely Rotating Bonds: 5; (11)Index of Refraction: 1.475; (12)Molar Refractivity: 45.81 cm³; (13)Molar Volume: 162.6 cm³; (14)Surface Tension: 34.6 dyne/cm; (15)Density: 1.034 g/cm³; (16)Flash Point: 213 °C; (17)Enthalpy of Vaporization: 71.63 kJ/mol; (18)Boiling Point: 456.3 °C at 760 mmHg; (19)Vapour Pressure: 1.63E-08 mmHg at 25°C.

Preparation: this chemical can be prepared by acryloyl chloride and ethane-1,2-diamine. This reaction will need reagent Et₃N and solvent CHCl₃.

Uses of 2-Propenamide,N,N'-1,2-ethanediylbis-: it can be used to produce N,N'-Dicinnamoyl-ethylendiamin at temperature of 100 °C. This reaction is a kind of Heck reaction. It will need reagent PNODAM-5 catalyst and solvent heptane, N,N-dimethyl-acetamide. The yield is about 96%.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause inflammation to the skin or other mucous membranes. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing, gloves and eye/face protection.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: C=CC(=O)NCCNC(=O)C=C
(2)InChI: InChI=1S/C8H12N2O2/c1-3-7(11)9-5-6-10-8(12)4-2/h3-4H,1-2,5-6H2,(H,9,11)(H,10,12)
(3)InChIKey: AYGYHGXUJBFUJU-UHFFFAOYSA-N