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29632-74-4

Basic Information
CAS No.: 29632-74-4
Name: 2-Fluoro-4-iodoaniline
Article Data: 8
Molecular Structure:
Molecular Structure of 29632-74-4 (2-Fluoro-4-iodoaniline)
Formula: C6H5FIN
Molecular Weight: 237.015
Synonyms: 2-fluoro-4-iodin anline;
Density: 2.008 g/cm3
Melting Point: 55-57 °C(lit.)
Boiling Point: 248.6 °C at 760 mmHg
Flash Point: 104.2 °C
Solubility: insoluble in water
Appearance: off-white to brown powder
Hazard Symbols: HarmfulXn, ToxicT, IrritantXi
Risk Codes: 36/37/38-20/21/22
Safety: 26-36-37/39-26/37/39
PSA: 26.02000
LogP: 2.59370
Synthetic route
348-54-9

2-Fluoroaniline

29632-74-4

2-fluro-4-iodoaniline

Conditions
ConditionsYield
With iodine; sodium hydrogencarbonate In water at 60 - 80℃; for 2h;77%
With iodine; sodium hydrogencarbonate In water at 60℃; for 3h;76%
Stage #1: 2-Fluoroaniline With n-butyllithium In diethyl ether; hexane at -78℃; for 1h;
Stage #2: With poly[4-(dibutyliodostannyl)butyl]styrene In diethyl ether; hexane at 20℃; for 18h;
Stage #3: With Iodine monochloride In diethyl ether; hexane at -78 - 20℃;
67%
29632-74-4

2-fluro-4-iodoaniline

1066-54-2

trimethylsilylacetylene

518342-58-0

2-fluoro-4-((trimethylsilyl)ethynyl)aniline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 21h; Sonogashira Cross-Coupling; Inert atmosphere;100%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Inert atmosphere;100%
With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide at 20℃; for 15h; Sonogashira Coupling;88%
867130-26-5

4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid

29632-74-4

2-fluro-4-iodoaniline

934664-24-1

4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylic acid

Conditions
ConditionsYield
Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4h;
Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity;
100%
Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4.08333h;
Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity;
100%
Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4.08333h;
Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity;
100%
463-71-8

thiophosgene

29632-74-4

2-fluro-4-iodoaniline

945530-32-5

2-fluoro-4-iodo-1-isothiocyanatobenzene

Conditions
ConditionsYield
In chloroform; water at 20℃; for 16h;100%
In chloroform; water at 20℃; for 16h;100%
In dichloromethane; water at 20℃;96.8%
50-00-0

formaldehyd

29632-74-4

2-fluro-4-iodoaniline

791112-16-8

N-(4-iodo-2-fluorophenyl)formamide

Conditions
ConditionsYield
With acetic anhydride In tetrahydrofuran; toluene at 20℃;100%
29632-74-4

2-fluro-4-iodoaniline

140-90-9

sodium O-ethyl dithiocarbonate

54420-94-9

6-iodobenzo[d]thiazole-2-thiol

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 95℃; for 5h;100%
29632-74-4

2-fluro-4-iodoaniline

61079-72-9

2,3,4,-trifluorobenzoic acid

391211-97-5

3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)-benzoic acid

Conditions
ConditionsYield
With lithium amide In tetrahydrofuran99%
With lithium amide In N,N-dimethyl-formamide Inert atmosphere;85%
With lithium amide In tetrahydrofuran at 45 - 55℃; for 1.25 - 2.5h; Product distribution / selectivity;80%
29632-74-4

2-fluro-4-iodoaniline

945559-14-8

1-azido-2-fluoro-4-iodobenzene

Conditions
ConditionsYield
Stage #1: 2-fluro-4-iodoaniline With trifluoroacetic acid; sodium nitrite at 0℃; for 0.5h;
Stage #2: With sodium azide In water at 0℃; for 1h;
99%
Stage #1: 2-fluro-4-iodoaniline With hydrogenchloride; sodium nitrite In water at -5℃; for 0.5h;
Stage #2: With sodium azide In water at -5℃; for 1h;
97%
910209-21-1

sodium cyclopropylsulfinate

29632-74-4

2-fluro-4-iodoaniline

1147558-09-5

C9H10FNO2S

Conditions
ConditionsYield
With N,N`-dimethylethylenediamine; copper (I) trifluoromethane sulfonate benzene In dimethyl sulfoxide at 120℃; for 16h;99%
copper(I) trifluoromethanesulfonate benzene complex; N,N`-dimethylethylenediamine In dimethyl sulfoxide at 120℃; for 16h;99%
With N,N`-dimethylethylenediamine; copper(I) trifluoromethanesulfonate benzene In dimethyl sulfoxide at 120℃; for 16h;99%
29632-74-4

2-fluro-4-iodoaniline

4023-34-1

cyclopropanecarboxylic acid chloride

1061683-60-0

N-(2-fluoro-4-iodophenyl)cyclopropanecarboxamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0 - 20℃;99%
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    Product name: 2-Fluoro-4-Iodoaniline CAS No.: 29632-74-4 Molecule Formula:C6H5FIN Molecule Weight:237.01 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING I

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    29632-74-4

    2-Fluoro-4-iodoaniline

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    Product Name: 2-Fluoro-4-iodoaniline Synonyms: 2-FLUORO-4-IODOANILINE;2-FLUORO-4-IODOBENZENAMINE;2-Fluoro-4-idioaniline;2-FLUORO-4-IODO-PHENYLAMINE;2-Fluoro-4-iodoaniline 98%;2-Fluoro-4-iodoaniline98%;2-Fluoro-4-iodoanili;2-fluo-4-iodoaniline C

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    29632-74-4

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  • 2-Fluoro-4-Iodoaniline cas no. 29632-74-4 98%

  • Casno:

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    29632-74-4

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Chemistry

The Molecular formula of  2-Fluoro-4-iodoaniline(29632-74-4) : C6H5FIN
The Molecular Weight of   2-Fluoro-4-iodoaniline(29632-74-4) :  237.01
Molecular Structure : 
Melting point: 55-57 °C(lit.)
Flash point: >230 °F
WATER Solubility: insoluble
Sensitive: Light Sensitive
Appearaance: light brown to brown Solid
Synonyms: 2-FLUORO-4-IODOBENZENAMINE;2-FLUORO-4-IODO-PHENYLAMINE;2-Fluoro-4-idioaniline;2-Fluoro-4-iodoaniline 98%;2-FLUORO-4-IODOANILINE;2-Fluoro-4-iodoaniline98%;

Safety Profile

The Hazard Codes of 2-Fluoro-4-iodoaniline(29632-74-4):    Xi,Xn ,   T
The Risk Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
20/21/22:  Harmful by inhalation, in contact with skin and if swallowed 
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
37/39:  Wear suitable gloves and eye/face protection 
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection 
RIDADR: PG3
WGK Germany: 3
Hazard Note: Toxic