CAS No.307-30-2,1H,1H-PENTADECAFLUORO-1-OCTANOL Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	307-30-2
Name:	1H,1H-PENTADECAFLUORO-1-OCTANOL
Article Data:	16

Formula:	C8H3 F15 O
Molecular Weight:	400.087
Synonyms:	(Pentadecafluoroheptyl)methanol;(Perfluoroheptyl)methanol; 1,1-Dihydropentadecafluorooctan-1-ol; 1,1-Dihydropentadecafluorooctanol;1,1-Dihydroperfluorooctanol; 1,1-Dihydroperfluorooctyl alcohol;1H,1H-Pentadecafluoro-1-octanol; 1H,1H-Pentadecafluoro-n-octanol;1H,1H-Pentadecafluorooctanol; 1H,1H-Perfluoro-1-octanol;1H,1H-Perfluorooctanol; Pentadecafluoro-1,1-dihydrooctanol; Unitex DJ 10; a,a-Dihydroperfluorooctanol
EINECS:	206-197-1
Density:	1,338 g/cm³
Melting Point:	44-47 °C(lit.)
Boiling Point:	163-165 °C(lit.)
Flash Point:	>110°C
Appearance:	white crystalline mass
Hazard Symbols:	Xi
Risk Codes:	36/37/38
Safety:	26-36
PSA:	20.23000
LogP:	4.35280

Synthetic route

: 106608-82-6
isopropyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctanoate

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With RuCl2(DPPEA)(±DAIPEN); hydrogen; sodium methylate In isopropyl alcohol; benzene at 100℃; under 750.075 - 45004.5 Torr; for 40h; Autoclave;	95%

: 335-67-1
Perfluorooctanoic acid

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With diethyl ether; pyrographite; ruthenium at 175℃; under 257428 Torr; Hydrogenation;
Multi-step reaction with 2 steps 1: 90 percent / thionyl chloride, N,N-dimethylformamide / 4 h / Heating 2: 77 percent / sodium bis(2-methoxyethoxy)aluminum hydride / diethyl ether; toluene / 0.5 h / Heating View Scheme
Multi-step reaction with 2 steps 1: chloroform 2: lithium alanate; diethyl ether View Scheme

: 335-64-8
pentadecafluorooctanoyl chloride

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With sodium bis(2-methoxyethoxy)aluminium dihydride In diethyl ether; toluene for 0.5h; Heating;	77%
With lithium aluminium tetrahydride; diethyl ether

: 335-67-1
Perfluorooctanoic acid

A: 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol-d2

B: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With formic acid; water-d2; ruthenium trichloride; triphenylphosphine at 200℃; for 8h;
With hydrogen; water-d2; 5 wt% Ru/C at 160℃; under 44134.3 Torr; for 8h;

: 3108-24-5
ethyl perfluorooctanoate

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With lithium aluminium tetrahydride

: 376-27-2
methyl perfluorooctanoate

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With lithium aluminium tetrahydride

: 307-96-0
pentadecafluoro-octanoic acid butyl ester

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

Conditions

Conditions	Yield
With lithium aluminium tetrahydride; diethyl ether

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 20769-85-1
2-bromoisobutyric acid bromide

: 2-bromo-2-methylbutyrylic acid-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl) ester

Conditions

Conditions	Yield
With dmap; triethylamine In tetrahydrofuran at 20℃;	97%

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 36653-82-4
1-Hexadecanol

: 1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octyloxy)-hexadecane

Conditions

Conditions	Yield
With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine In benzene at 65℃; for 2h;	96%

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 107-05-1
3-chloroprop-1-ene

: 812-72-6
8-(allyloxyl)-1,1,1,2,2,3,3,4,4,5,5,6,6,7,7-pentadecafluorooctane

Conditions

Conditions	Yield
With sodium hydroxide; tetramethylammonium hydrogen sulfate at 40℃; for 12h;	96%

Total:31 Page 1 of 1 1

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Chemistry

IUPAC Name: 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol
Product Name: 1H,1H-Pentadecafluoro-1-octanol
The MF of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol (CAS NO.307-30-2) is C₈H₃F₁₅O.

The MW of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol (CAS NO.307-30-2) is 400.08.
Synonyms of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol (CAS NO.307-30-2): 1-Octanol, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro- ; 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol ; 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctyl alcohol ; 1H,1H-Pentadecafluoro-1-octanol ; 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-1-octanol
Product Categories: Fluorous Chemistry;Fluorous Compounds;Synthetic Organic Chemistry;Fluorous Synthesis;Rf-Tagged Building Blocks and Precursors
Apperance: white crystalline mass
Index of Refraction: 1.285
EINECS: 206-197-1
Density: 1.665 g/ml
Flash Point: 49.2 °C
Boiling Point: 164 °C
Melting Point: 38-40 °C
BRN: 1716494

Uses

2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol (CAS NO.307-30-2) is used as fine chemicals, chemical synthesis, medicine, pesticide intermediates.

Safety Profile

Safety information of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctan-1-ol (CAS NO.307-30-2):
Hazard Codes Irritant Xi
Risk Statements
36/37/38 Irritating to eyes, respiratory system and skin
Safety Statements
26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36 Wear suitable protective clothing
WGK Germany 3
Hazard Note Irritant
TSCA T