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Basic Information
| CAS No.: | 3132-99-8 |
|---|---|
| Name: | 3-Bromobenzaldehyde |
| Article Data: | 224 |
| Molecular Structure: | |
|
|
|
| Formula: | C7H5BrO |
| Molecular Weight: | 185.02 |
| Synonyms: | NSC 66828;m-Bromobenzaldehyde;Benzaldehyde,m-bromo- (6CI,7CI,8CI);3-Formyl-1-bromobenzene;3-Formylbromobenzene; |
| EINECS: | 221-526-9 |
| Density: | 1.577 g/cm3 |
| Melting Point: | 18-21 °C(lit.) |
| Boiling Point: | 235.3 °C at 760 mmHg |
| Flash Point: | 96.1 °C |
| Solubility: | decomposes in water |
| Appearance: | clear colorless to yellow liquid after melting |
| Hazard Symbols: |
 Xn, Xi
|
| Risk Codes: | 22-36/37/38 |
| Safety: | 26-36 |
| PSA: | 17.07000 |
| LogP: | 2.26160 |
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Synthetic route
- 15852-73-0
(3-Bromophenyl)methanol
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With fluorosulfonyl fluoride; potassium carbonate; dimethyl sulfoxide at 20℃; for 12h; chemoselective reaction; | 99% |
| With N-chloro-N-(benzenesulfonyl)benzenesulfonamide In acetonitrile at 20 - 25℃; for 0.25h; Inert atmosphere; chemoselective reaction; | 98% |
| With tert.-butylhydroperoxide; 2,2′-((1E,1′E)-(1,2-phenylenebis(azanylylidene))bis(methanylylidene))diphenolcopper(II); sodium hydroxide In water; acetonitrile at 20℃; | 97% |
- 14473-91-7, 20595-41-9, 32862-97-8
3-bromocinnamic acid
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With aluminum oxide; potassium permanganate In dichloromethane at 20℃; | 99% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-dibromobenzene With tri-n-butyllithium magnesate complex In toluene at 0℃; for 1.5h; Stage #2: N,N-dimethyl-formamide In toluene at 0℃; for 0.5h; Stage #3: With citric acid at 20℃; | 99% |
| Stage #1: 1,3-dibromobenzene With n-butyllithium; isopropylmagnesium chloride In tetrahydrofuran; hexane at 0 - 5℃; for 1h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 1h; Further stages.; | 90% |
| Stage #1: 1,3-dibromobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 0.583333h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at -78 - 20℃; for 1.5h; | 63.21% |
- 62247-78-3
1-bromo-3-(dibromomethyl)benzene
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With dimethyl sulfoxide at 120℃; for 1h; | 95% |
| With potassium carbonate In dimethylsulfoxide-d6 at 60℃; for 24h; Kinetics; Hydrolysis; |
- 75148-49-1
3-bromobenzaldehyde diethylacetal
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With iron(III) p-toluenesulfonate hexahydrate In water for 1h; Reflux; | 95% |
| bismuth(III) iodide In water at 20℃; for 20h; | 89% |
| With copper(II) sulfate; sodium iodide In acetone at 56℃; for 0.75h; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| at 120℃; for 1h; | 95% |
Conditions
| Conditions | Yield |
|---|---|
| With bromine fluoride In ethanol; chloroform at -40℃; for 0.0833333h; | A 94% B 5% |
| With bromine fluoride In ethanol; chloroform at -40℃; for 0.833333h; | A 5% B 90% |
- 82436-20-2
2-(3-bromophenyl)-1,3-dithiolane
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h; | 94% |
- 50793-32-3
C6H4(3-Br)(CHSCH2CH2CH2S-cyclic)
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; iodic acid at 20℃; for 0.0125h; | 94% |
| With quinolinium monofluorochromate(VI) In acetonitrile for 2.5h; Heating; | 93% |
| With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 2h; | 92% |
| With 2,6-dicarboxypyridinium chlorochromate In acetonitrile for 1.91667h; Heating; | 90% |
- 17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide
- 3132-99-8
m-bromobenzoic aldehyde
Conditions
| Conditions | Yield |
|---|---|
| With carbon tetrabromide In water; acetonitrile at 45℃; for 2h; sonication; | 93% |
| In(OSO2CF3)3 In acetone at 20℃; for 2.5h; | 93% |
| With copper(II) sulfate; sodium iodide In acetone at 56℃; for 0.666667h; | 92% |
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3-Bromobenzaldehyde
Chemistry
Product Name: 3-Bromobenzaldehyde
Synonyms: m-bromo-benzaldehyd;nsc66828; 3-bromo-benzaldehyd;AKOS BBS-00003144;Benzaldehyde, m-bromo-;3-BROMOBENZALDEHYDE;AKOS B004042;benzaldehyde,3-bromo-;
The Molecular formula of 3-bromo benzaldehyde(3132-99-8): C7H5BrO
The Molecular Weight of 3-bromo benzaldehyde(3132-99-8): 185.02
Molecular Structure :
EINECS: 221-526-9
Melting point: 18-21 °C(lit.)
Boiling point: 233-236 °C(lit.)
density: 1.587 g/mL at 25 °C(lit.)
refractive index: n20/D 1.593(lit.)
Flash point: 96 °C
color: very faintly to deep brownish-yellow
Water Solubility: DECOMPOSES
Sensitive: Air Sensitive
Synonyms: m-bromo-benzaldehyd;nsc66828; 3-bromo-benzaldehyd;AKOS BBS-00003144;Benzaldehyde, m-bromo-;3-BROMOBENZALDEHYDE;AKOS B004042;benzaldehyde,3-bromo-;
The Molecular formula of 3-bromo benzaldehyde(3132-99-8): C7H5BrO
The Molecular Weight of 3-bromo benzaldehyde(3132-99-8): 185.02
Molecular Structure :
EINECS: 221-526-9
Melting point: 18-21 °C(lit.)
Boiling point: 233-236 °C(lit.)
density: 1.587 g/mL at 25 °C(lit.)
refractive index: n20/D 1.593(lit.)
Flash point: 96 °C
color: very faintly to deep brownish-yellow
Water Solubility: DECOMPOSES
Sensitive: Air Sensitive
Safety Profile
The Hazard Codes of 3-bromo benzaldehyde(3132-99-8): 
Xn,Xi
The Risk Statements information of 3-bromo benzaldehyde(3132-99-8):
22: Harmful if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 3-bromo benzaldehyde(3132-99-8):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RIDADR: 2810
WGK Germany: 3
RTECS: CU4820000
F: 10
Hazard Note: Irritant
Xn,Xi The Risk Statements information of 3-bromo benzaldehyde(3132-99-8):
22: Harmful if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 3-bromo benzaldehyde(3132-99-8):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RIDADR: 2810
WGK Germany: 3
RTECS: CU4820000
F: 10
Hazard Note: Irritant