CAS No.3218-36-8,4-Biphenylcarboxaldehyde Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	3218-36-8
Name:	4-Biphenylcarboxaldehyde
Article Data:	536

Formula:	C₁₃H₁₀O
Molecular Weight:	182.222
Synonyms:	4-Biphenylcarboxaldehyde(6CI,7CI,8CI);Benzaldehyde, p-phenyl- (3CI);4-Biphenylaldehyde;4-Formyl-1,1'-biphenyl;4-Formylbiphenyl;Biphenyl-4-carbaldehyde;NSC 46066;p-Biphenylaldehyde;p-Biphenylcarboxaldehyde;p-Phenylbenzaldehyde;
EINECS:	221-742-3
Density:	1,107 g/cm³
Melting Point:	57-59 °C(lit.)
Boiling Point:	326.6 °C at 760 mmHg
Flash Point:	186.1 °C
Solubility:	17mg/L at 20℃
Appearance:	off-white crystalline powder
Hazard Symbols:	Xi
Risk Codes:	36/37/38
Safety:	26-36
PSA:	17.07000
LogP:	3.16610

Synthetic route

: 104-88-1
4-chlorobenzaldehyde

: 98-80-6
phenylboronic acid

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With potassium carbonate In methanol at 100℃; for 0.166667h; Suzuki-Miyaura Coupling; Microwave irradiation;	100%
With 2,2-bis-(N-2-morpholinethylbenzimidazolium)-ethylether dichloride; potassium tert-butylate; palladium diacetate In water; N,N-dimethyl-formamide at 50℃; for 3h; Reagent/catalyst; Suzuki Coupling;	100%
With caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane for 1h; Suzuki-Miyaura coupling; Heating;	99%

: 1122-91-4
4-bromo-benzaldehyde

: 98-80-6
phenylboronic acid

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With sodium phosphate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 6h; Suzuki-Miyaura reaction;	100%
With sodium carbonate; palladium on activated charcoal In ethanol at 20℃; for 5h; Suzuki-Miyaura cross-coupling;	100%
With potassium carbonate; bis(2-diphenylphosphinoxynaphthalen-1-yl)methane; palladium diacetate In methanol at 20℃; for 1h; Suzuki cross-coupling reaction;	100%

: 3597-91-9
biphenyl-4-yl methanol

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With n-butyltriphenylphosphonium permanganate In acetonitrile at 20℃; for 0.25h;	100%
With silica-supported Jones reagent In dichloromethane for 0.00269444h;	99.7%
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-methyl-N-[3-(4'-diacetoxyiodo)phenoxy-1-propyl]pyrrolidinium 4-methylbenzenesulfonate In dichloromethane at 20℃; for 6h;	99%

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 98-80-6
phenylboronic acid

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With [Pd(N-(naphthyl)-salicylaldimine(-2H))(triphenylphosphine)]; sodium hydroxide at 120℃; for 3h; Suzuki Coupling;	100%
With tetra-n-propylammonium bromide; sodium carbonate In water at 100℃; for 0.5h; Catalytic behavior; Suzuki-Miyaura Coupling;	100%
With potassium carbonate; palladium dichloride In water at 20 - 90℃; Suzuki coupling; Inert atmosphere;	99%

: 79913-05-6
1,1-diacetoxy-1-(4-biphenyl)methane

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
zeolite HSZ-360 for 0.333333h; Irradiation;	99%
With zirconium(IV) chloride In methanol at 20℃; for 0.05h;	96%
With 2,6-dicarboxypyridinium chlorochromate In acetonitrile at 20℃; for 0.5h;	70%

: 591-50-4
iodobenzene

: 87199-17-5
4-formylphenylboronic acid,

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With bis(1,1'-ethylene-3,3'-divinylimidazole-2,2'-diylidene)nickel(II) dibromide dihydrate; potassium carbonate In water; N,N-dimethyl-formamide at 100℃; for 8h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique;	99%
With potassium carbonate In water; N,N-dimethyl-formamide at 30℃; for 4h; Suzuki-Miyaura Coupling; Irradiation; Inert atmosphere;	98%
With potassium phosphate In ethanol; water at 80℃; for 3h; Suzuki-Miyaura Coupling;	98%

: 108-86-1
bromobenzene

: 87199-17-5
4-formylphenylboronic acid,

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With potassium carbonate In ethanol; water at 80℃; for 2h; Suzuki-Miyaura Coupling;	99%
With palladium diacetate In water; isopropyl alcohol at 27℃; for 1h; Suzuki-Miyaura Coupling;	96%
With C12H12Cl2N4O2Pd; caesium carbonate In water at 60℃; for 5h; Suzuki-Miyaura Coupling;	90%

: 143-66-8
sodium tetraphenyl borate

: 1122-91-4
4-bromo-benzaldehyde

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With sodium hydroxide; palladium diacetate In water at 110℃; for 2h; Suzuki-type reaction;	99%
With sodium carbonate at 100℃; for 0.666667h; Suzuki Coupling;	97%
With sodium carbonate at 80℃; for 0.716667h; Catalytic behavior; Suzuki Coupling;	97%

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: 104-88-1
4-chlorobenzaldehyde

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With potassium carbonate In water at 20℃; for 6h; Suzuki-Miyaura Coupling;	99%

: 40143-27-9
biphenyl-4-carbaldehyde oxime

: 3218-36-8
4-Phenylbenzaldehyde

Conditions

Conditions	Yield
With 1-benzyl-4-aza-1-azoniabiyclo<2.2.2>octane peroxodisulfate In acetonitrile for 0.25h; Heating;	98%
With 1-benzyl-4-aza-1-azoniabiyclo<2.2.2>octane peroxodisulfate In acetonitrile for 0.25h; Oxidation; Heating;	98%
With tris[trinitratocerium(IV)] paraperiodate at 90℃; for 0.166667h;	95%
With Nitrogen dioxide In acetonitrile at 25℃; for 0.0833333h;

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Chemistry

The molecular formula of 4-Biphenylcarboxaldehyde(3218-36-8) is C₁₃H₁₀O and its formula weight is 182.22.
The density of 4-Biphenylcarboxaldehyde(3218-36-8) is 1.107 g/cm³ and it has a melting point of 57-59 °C(lit.). The boiling point is 184 °C11 mm Hg(lit.). Its flash point is 172°C.
The chemical synonyms of 4-Biphenylcarboxaldehyde(3218-36-8) are P-PHENYLBENZALDEHYDE;P-BIPHENYLCARBOXALDEHYDE;P-DIPHENYLALDEHYDE;P-DIPHENYLCARBOXALDEHYDE;[1,1'-BIPHENYL]-4-CARBALDEHYDE;(1,1'-BIPHENYL)-4-CARBOXALDEHYDE;4-PHENYLBENZALDEHYDE;4-BIPHENYLALDEHYDE
The molecular structure of 4-Biphenylcarboxaldehyde(3218-36-8):

Toxicity Data With Reference

RTECS#: CAS# 3218-36-8: DV1767000
LD50/LC50: RTECS: Not available.
Carcinogenicity: 4-BIPHENYLCARBOXALDEHYDE, 99% - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: See actual entry in RTECS for complete information.

Safety Profile

Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 1
RTECS DV1767000
F 10-23
Hazard Note Irritant

Specification

Chemical Stability: Stable under normal temperatures and pressures.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents, strong bases.
Hazardous Decomposition Products Carbon monoxide, irritating and toxic fumes and gases, carbon dioxide.
Hazardous Polymerization Has not been reported.