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32779-36-5

Basic Information
CAS No.: 32779-36-5
Name: 5-Bromo-2-chloropyrimidine
Article Data: 23
Molecular Structure:
Molecular Structure of 32779-36-5 (5-Bromo-2-chloropyrimidine)
Formula: C4H2BrClN2
Molecular Weight: 193.43
Synonyms: 5-bromo-2-chloro-pyrimidine;Pyrimidine, 5-bromo-2-chloro-;2-chloro-5-bromopyrimidine;
EINECS: -0
Density: 1.86 g/cm3
Melting Point: 76-81 °C(lit.)
Boiling Point: 291.552 °C at 760 mmHg
Flash Point: 130.126 °C
Solubility: insoluble in water
Appearance: off-white to beige crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/39-37/39-36
PSA: 25.78000
LogP: 1.89250
Synthetic route
38353-06-9

5-bromopyrimidin-2-ol

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With trichlorophosphate at 80℃;88%
With trichlorophosphate In N,N-dimethyl-aniline for 4h; Heating / reflux;75%
With N,N-dimethyl-aniline; trichlorophosphate for 4h; Heating;73%
38353-06-9

5-bromo-1H-pyrimidin-2-one

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With N,N-dimethyl-aniline; trichlorophosphate for 6h; Heating / reflux;84%
4595-59-9

5-bromopyrimidine

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With trichlorophosphate at 0 - 120℃; for 4.16667h;80%
With trichlorophosphate at 0 - 120℃; for 4.25h;

5-bromo-2-hydroxypyrimidine

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With N,N-dimethyl-aniline; trichlorophosphate77%
7752-82-1

5-bromo-2-aminopyrimidine

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With tert.-butylnitrite; N-benzyl-N,N,N-triethylammonium chloride In dichloromethane at 20℃; Inert atmosphere;36%
205672-25-9

4-amino-5-bromo-2-chloropyrimidine

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With tetrahydrofuran; tert.-butylnitrite; dimethyl sulfoxide at 30℃; for 2h; Green chemistry;27%
1722-12-9

2-chloropyrimidine

32779-36-5

5-Bromo-2-chloropyrimidine

Conditions
ConditionsYield
With N-Bromosuccinimide; boron trifluoride diethyl etherate In acetonitrile at 20℃; Solvent; Reflux;14.1 g
With bromine; acetic acid Reflux;29 g
With bromine; acetic acid Reflux;29 g
32779-36-5

5-Bromo-2-chloropyrimidine

74-89-5

methylamine

31402-54-7

5-bromo-N-methylpyrimidin-2-amine

Conditions
ConditionsYield
In methanol; water for 72h; Reflux;100%
With potassium carbonate In tetrahydrofuran; water; tert-butyl alcohol at 150℃; for 0.25h; microwave;98%
Stage #1: 5-Bromo-2-chloropyrimidine; methylamine In methanol at 115℃; for 48h; Sealed vessel;
Stage #2: With sodium hydroxide In dichloromethane; water
93%
32779-36-5

5-Bromo-2-chloropyrimidine

67-63-0

isopropyl alcohol

121487-12-5

5-bromo-2-(propan-2-yloxy)pyrimidine

Conditions
ConditionsYield
With sodium at 20℃;100%
Stage #1: isopropyl alcohol With sodium hydride
Stage #2: 5-Bromo-2-chloropyrimidine for 15h; Reflux;
With sodium hydride at 60℃; for 24.5h; Heating / reflux;
110-91-8

morpholine

32779-36-5

5-Bromo-2-chloropyrimidine

84539-22-0

4-(5-bromopyrimidin-2-yl)morpholine

Conditions
ConditionsYield
Stage #1: morpholine With potassium carbonate In acetonitrile at 20℃; for 1h;
Stage #2: 5-Bromo-2-chloropyrimidine In acetonitrile for 18h; Reflux;
100%
With potassium carbonate In acetonitrile at 85℃; for 10h;95%
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 16h;85%
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    5-Bromo-2-chloropyrimidine CAS No.:32779-36-5 Name: 5-Bromo-2-chloropyrimidine Molecular Structure Molecular Formula: C4H2BrClN2 Molecular Weight: 193.43

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Chemistry

CAS No. 32779-36-5
Chemical Name: 5-Bromo-2-chloropyrimidine
Molecular Formula: C4H2BrClN2
Formula Weight: 193.43
5-Bromo-2-chloropyrimidine Property
mp : 76-81 °C(lit.)
bp : 95°C 15mm
Fp : 95°C/15mm
WATER Solubility : insoluble

Production

Synonyms: PYRIMIDINE, 5-BROMO-2-CHLORO-;2-CHLORO-5-BROMOPYRIMIDINE;2C5BP;5-BROMO-2-CHLOROPYRIMIDINE;5-BROMO-2-CHLOROPYRIMIDNE;5-BROMO-2-CHLOROPYRIMIDINE(MINIMUM85%);MAJORIMPURITYIS2,5-DIBROMOPYRIMIDINE ;5-BROMO-2-CHLOROPYRIMIDINE(MINIMUM95%) ;5-Bromo-2-chloroPYRIMIDINE 85%;5-Bromo-2-chloroPYRIMIDINE, 98+%

Safety Profile

Safety
5-Bromo-2-Chloropyrimidine
Hazard Codes : Xi 
Risk Statements : 36/37/38 
Safety Statements : 26-36/39-37/39-36