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Detail of "3308-94-9"

  • CAS Number:
  • 3308-94-9
  • Name:
  • 1,3-Dioxolane,2-(3-chloropropyl)-2-(4-fluorophenyl)-

  • Superlist Name:
  • 2-(3-Chloropropyl)-2-(4-fluorophenyl)-1,3-dioxolane
  • Molecular Structure:
  • Formula:
  • C12H14ClFO2
  • Molecular Weight:
  • 244.69
  • Synonyms:
  • 1,3-Dioxolane,2-(3-chloropropyl)-2-(p-fluorophenyl)- (7CI,8CI);1,1-(Ethylenedioxy)-4-chloro-1-(4-fluorophenyl)butane;1-Chloro-4,4-(ethylenedioxy)-4-(4-fluorophenyl)butane;2-(3-Chloropropyl)-2-(4-fluorophenyl)dioxolane;2-(3-Chloropropyl)-2-(4'-fluorophenyl)-1,3-dioxolane;2-(3-Chloropropyl)-2-(p-fluorophenyl)dioxolane;3-Chloropropyl4-fluorophenyl ketone ethylene ketal;3-p-Fluorobenzoylpropyl chloride ethyleneketal;4,4-(Ethylenedioxy)-4-(4-fluorophenyl)butyl chloride;4-(p-Fluorophenyl)-4,4-ethylenedioxy-1-chlorobutane;4-Chloro-1-(p-fluorophenyl)-1-butanonecyclic ethylene acetal;4-Chloro-p-fluorobutyrophenone cyclic ethylene acetal;
  • EINECS:
  • 221-993-9
  • Density:
  • 1.205 g/cm3
  • Boiling Point:
  • 320.05 °C at 760 mmHg
  • Flash Point:
  • 147.361 °C
  • Solubility:
  • Insoluble in water
  • Appearance:
  • clear colourless to faint yellow oily liquid
  • Hazard Symbols:
  • IrritantXi
  • Risk Codes:
  • 36/37/38
  • Safety:
  • 37/39-26 Details

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CAS No.3308-94-9 2-(3-Chloropropyl)-2-(4-fluorophenyl)-1,3-dioxolane

Assay:98%

Supplier:Hangzhou Dayangchem Co., Ltd. [ China (Mainland)]

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ISO 3875Integral
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CAS No.3308-94-9 2-(3-Chloropropyl)-2-(4-fluorophenyl)-1,3-dioxolane

Supplier:ChemOrganic Limited [ China (Mainland)]

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1375Integral
1375

Tel:0571-28183299

Address:Room 608,Building B , Zhejiang University science park, #525 Xixi Road ,hangzhou,China.

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CAS No.3308-94-9 2-(3-Chloropropyl)-2-(4-fluorophenyl)-1,3-dioxolane

Supplier:Shijiazhuang JuSha Imp. & Exp. Co., Ltd [ China (Mainland)]

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Supplier
910Integral
910

Tel:86-311-89877166

Address:Room 307, XinCheng Building, No. 351 YouYi Street, Shijiazhuang, China

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Reference

4-Piperidinol derivatives
4-Piperidinol derivatives. Ikawa, Kenji; Tokuyama, Kanji; Kiyokawa, Masumi; Maezono, Norihide; Tokuno, Noboru; Maeda, Takashi; Uno, Ikuo (Shionogi and Co., Ltd., Japan). Japan. Kokai JP 51118769 18 Oct 1976 Showa, 6 pp. (Japanese). (Japan). CODEN: JKXXAF. CLASS: IC: C07D211-52. APPLICATION: JP 75-42564 8 Apr 1975. 3308-94-9 and 52-86-8 are also in the experiment. DOCUMENT TYPE: Patent CA Section: 27 (Heterocyclic Compounds (One Hetero Atom)) Section cross-reference(s): 17 I (R = Cl, Me) were prepd. by relfuxing HN(CH2CH2CO2Me)2 with the ethylene ketal of 4-FC6H4CO(CH2)3Cl and NaHCO3 in PhMe to give 83.5% the ethylene ketal (II) of 4-FC6H4CO(CH2)3N(CH2CH2CO2Me)2, cyclization of II in C6H6 with Na-MeOH to give 93.3% III, refluxing III in 1:6 H2O-MeOH to give 58% ethylene ketal of (IV) of V, deketalization of IV by heating in 50% AcOH to give 82.7% V, and Grignard reaction of V with 4-RC6H4MgBr. .
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