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36177-92-1

Basic Information
CAS No.: 36177-92-1
Name: N-BUTYL TRIACETONEDIAMINE
Article Data: 14
Molecular Structure:
Molecular Structure of 36177-92-1 (N-BUTYL TRIACETONEDIAMINE)
Formula: C13H28N2
Molecular Weight: 212.379
Synonyms: 2,2,6,6-Tetramethyl-4-(butylamino)piperidine;4-(Butylamino)-2,2,6,6-tetramethylpiperidine;4-N-Butylamino-2,2,6,6-tetramethylpiperidine;Butyl-(2,2,6,6-tetramethylpiperidin-4-yl)-amine;N-(2,2,6,6-Tetramethyl-4-piperidinyl)butylamine;N-(2,2,6,6-Tetramethyl-4-piperidyl)butanamine;N-Butyl-2,2,6,6-tetramethyl-4-piperidinamine;N-Butyl-2,2,6,6-tetramethyl-4-piperidineamine;
EINECS: 252-899-6
Density: 0.87 g/cm3
Boiling Point: 249.7 °C at 760 mmHg
Flash Point: 97 °C
Solubility: 797.5g/L at 20℃
Hazard Symbols: Xn
Risk Codes: 22
PSA: 24.06000
LogP: 3.40500
Synthetic route
826-36-8

2,2,6,6-Tetramethyl-4-piperidone

109-73-9

N-butylamine

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
Pt on carbon In water98%
With hydrogen at 100℃; under 6750.68 Torr; for 5h; Pressure; Temperature; Autoclave;97.4%
Stage #1: 2,2,6,6-Tetramethyl-4-piperidone; N-butylamine With acetic acid at 25℃; for 12h;
Stage #2: With methanol; sodium tetrahydroborate for 8h; Temperature; Reagent/catalyst;
95.2%
36768-62-4

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE

123-72-8

butyraldehyde

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
With hydrogen In toluene at 60 - 120℃; under 7500.75 Torr; for 5h; Reagent/catalyst; Autoclave;15%
826-36-8

2,2,6,6-Tetramethyl-4-piperidone

109-73-9

N-butylamine

A

2403-88-5

4-hydroxy-2,2,6,6-tetramethylpiperidine

B

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
With hydrogen In 1,4-dioxane at 120℃; under 30003 Torr;
826-36-8

2,2,6,6-Tetramethyl-4-piperidone

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: ethanol / Reflux
2: 5%-palladium/activated carbon; hydrogen / cyclohexane / 4 h / 60 - 120 °C / 11251.1 Torr / Autoclave
View Scheme
35517-43-2

butyl-(2,2,6,6-tetramethyl-piperidin-4-ylidene)-amine

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
With 5%-palladium/activated carbon; hydrogen In cyclohexane at 60 - 120℃; under 11251.1 Torr; for 4h; Autoclave;
108-77-0

1,3,5-trichloro-2,4,6-triazine

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

2-chloro-4,6-bis-((2,2,6,6-tetramethyl-piperidin-4-yl)butylamino)-1,3,5-triazine

Conditions
ConditionsYield
With sodium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 60℃; for 12h; Reagent/catalyst; Solvent; Temperature; Cooling with ice;98.3%
With sodium carbonate In toluene at 80℃; for 3h; Product distribution / selectivity;
With sodium carbonate In toluene at 80℃; for 3h; Product distribution / selectivity;
Stage #1: 1,3,5-trichloro-2,4,6-triazine; 4-n-butylamino-2,2,6,6-tetramethylpiperidine In xylene at 20℃; for 0.5h;
Stage #2: With sodium hydroxide In water; xylene at 20 - 95℃; for 2h;
With potassium hydroxide In water; toluene at 20 - 45℃; Reagent/catalyst; Solvent;
50-00-0

formaldehyd

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

36177-99-8

butyl-methyl-(1,2,2,6,6-pentamethyl-piperidin-4-yl)-amine

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In methanol; water at 80 - 140℃; under 15001.5 - 31503.2 Torr; Solvent; Autoclave;93.7%
36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

124172-46-9

N-butyl-N-(2,2,6,6-tetramethyl-piperidin-4-yl)formamide

Conditions
ConditionsYield
With acetic acid; boric acid In xylene for 6h; Inert atmosphere; Reflux;92%

C90H165Cl3N22O3

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

C129H246N28O3

Conditions
ConditionsYield
With sodium hydroxide In water; xylene Reflux;90.9%
67-66-3

chloroform

128-39-2

2,6-di-tert-butylphenol

108-94-1

cyclohexanone

36177-92-1

4-n-butylamino-2,2,6,6-tetramethylpiperidine

1-(3,5-di-tert-butyl-4-hydroxy-phenyl)-cyclohexanecarboxylic acid butyl-(2,2,6,6-tetramethyl-piperidin-4-yl)-amide

Conditions
ConditionsYield
With sodium hydroxide at 10℃;85%
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  • n-butyl triacetonediamine manufacture

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    36177-92-1

    n-butyl triacetonediamine manufacture

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  • N-BUTYL TRIACETONEDIAMINE 36177-92-1 95%

  • Casno:

    36177-92-1

    N-BUTYL TRIACETONEDIAMINE 36177-92-1 95%

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  • CSR201608-4329

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    36177-92-1

    CSR201608-4329

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    Supplement, prompt shipment, high purity Application:powder material

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  • N-butyl-2,2,6,6-tetramethylpiperidin-4-amine

  • Casno:

    36177-92-1

    N-butyl-2,2,6,6-tetramethylpiperidin-4-amine

    Min.Order: 0

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  • 4-Piperidinamine,N-butyl-2,2,6,6-tetramethyl-

  • Casno:

    36177-92-1

    4-Piperidinamine,N-butyl-2,2,6,6-tetramethyl-

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Specification

The 4-Piperidinamine,N-butyl-2,2,6,6-tetramethyl-, with the CAS registry number 36177-92-1, has the IUPAC name N-butyl-2,2,6,6-tetramethylpiperidin-4-amine. Its molecular formula is C13H28N2 and its molecular weight is 212.37. Additionally, its classification codes are TSCA Flag P [A commenced PMN (Premanufacture Notice) substance]; TSCA Flag S [Substance is identified in a proposed or final SNUR (Significant New Use Rule) under TSCA].

Other characteristics of the 4-Piperidinamine,N-butyl-2,2,6,6-tetramethyl- can be summarised as followings: (1)ACD/LogP: 3.43; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -0.67; (4)ACD/LogD (pH 7.4): -0.56; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 1; (8)ACD/KOC (pH 7.4): 1; (9)#H bond acceptors: 2; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 4; (12)Polar Surface Area: 6.48 Å2; (13)Index of Refraction: 1.471; (14)Molar Refractivity: 67.48 cm3; (15)Molar Volume: 241.4 cm3; (16)Polarizability: 26.75×10-24cm3; (17)Surface Tension: 30.6 dyne/cm; (18)Density: 0.87 g/cm3; (19)Flash Point: 97 °C; (20)Enthalpy of Vaporization: 48.69 kJ/mol; (21)Boiling Point: 249.7 °C at 760 mmHg; (22)Vapour Pressure: 0.0226 mmHg at 25°C.

You can still convert the following datas into molecular structure: 
1.SMILES: N(C1CC(NC(C)(C)C1)(C)C)CCCC
2.InChI: InChI=1/C13H28N2/c1-6-7-8-14-11-9-12(2,3)15-13(4,5)10-11/h11,14-15H,6-10H2,1-5H3
3.InChIKey: FDAKZQLBIFPGSV-UHFFFAOYAH