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407-25-0

Basic Information
CAS No.: 407-25-0
Name: Trifluoroacetic anhydride
Article Data: 75
Molecular Structure:
Molecular Structure of 407-25-0 (Trifluoroacetic anhydride)
Formula: C4F6O3
Molecular Weight: 210.033
Synonyms: Aceticacid, trifluoro-, anhydride (6CI,8CI,9CI);2,2,2-Trifluoroacetic anhydride;Bis(trifluoroacetic) anhydride;Hexafluoroacetic anhydride;NSC 96965;Perfluoroacetic anhydride;Trifluoroacetic acid anhydride;Trifluoroacetyl anhydride;Trifluoroacetic anhydride(TFAA);
EINECS: 206-982-9
Density: 1.641 g/cm3
Melting Point: -63.5 °C
Boiling Point: 39.5 °C at 760 mmHg
Flash Point: -26 °C
Solubility: hydrolysis with water
Appearance: Clear, colorless liquid
Hazard Symbols: CorrosiveC, ToxicT
Risk Codes: 14-20-35-52/53-34-23/24/25
Safety: 26-36/37/39-43-45-61-9-8-28A-27
Transport Information: UN 3265 8/PG 1
PSA: 43.37000
LogP: 1.18080
Synthetic route
64899-09-8

N-(n-butyl)-2,4-dinitrotrifluoroacetanilide

A

13059-86-4

2,4-dinitro-N-butylaniline

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
With tris buffers; cetyltrimethylammonim bromide at 25℃; Rate constant; hydrolysis, other quaterner amines;A 99.7%
B n/a
76-05-1

trifluoroacetic acid

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
With fuming sulphuric acid at 130℃; Large scale;99%
With fuming sulphuric acid at 78 - 130℃; Large scale;99%
With sulfuric acid; sulfur trioxide at 130℃;99%
421-59-0

trifluoromethyldiiodophosphine

2966-50-9

silver trifluoroacetate

A

1682-76-4

Trifluormethylphosphonigsaeure-bis(trifluoressigsaeure)anhydrid

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
within 10 h;A n/a
B 98%
10 min; isolation from volatile part of product;A n/a
B 72%
1493-13-6

trifluorormethanesulfonic acid

76-05-1

trifluoroacetic acid

A

407-25-0

trifluoroacetic anhydride

B

68602-57-3

trifluoroacetyl triflate

Conditions
ConditionsYield
With phosphorus pentoxide at -20 - 240℃; for 3.5h;A n/a
B 75%
86024-51-3

Cl2SNTeF5

2966-50-9

silver trifluoroacetate

A

86024-52-4

F5TeNSO

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
In neat (no solvent) Cl2S=NTeF5 and CF3COOAg stirred at room temp. and warmed to 45°Cand stirred for 1 h; O=S=NTeF5 and (CF3CO)2O condensed into -196°C trap under vac., separation achieved by trap-to-trap distillation through -45 (O=S=NTeF5) and -78°C cooled traps; elem. anal.;A 68%
B n/a
407-38-5

2,2,2-trifluoroethyl trifluoroacetate

A

353-50-4

Carbonyl fluoride

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
With chlorine at 22.84℃; under 760 Torr; Irradiation; Synthetic gas;A 35%
B 45%
13257-51-7

mercury(II) trifluoroacetate

2757-23-5

chloro(chlorosulfanyl)methanone

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
at 50 - 55℃; for 3h;30%
650-09-9

O,O-Diethyl O-Trifluoroacetyl Phosphate

A

107-49-3

Tetraethyl pyrophosphate

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
Erhitzen im Vakuum;
350-70-9

tris(trifluoro acetyloxy)borane

A

330-25-6

tetrakis-trifluoroacetoxy-diboroxane

B

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
at 100℃; under 0.0001 Torr;
at 100℃; under 0.0001 Torr;
2966-50-9

silver trifluoroacetate

407-25-0

trifluoroacetic anhydride

Conditions
ConditionsYield
With phosphorus at 180℃;
With sulfur at 300℃;
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Chemistry

Product Name: Trifluoroacetic anhydride

Molecular Formula: C4F6O3
Molecular Weight: 210.03g/mol
Mol File: 407-25-0.mol
Einecs: 206-982-9
Appearance: Clear, colorless liquid
Melting Point: -65 °C, 208 K, -85 °F
Boiling point: 40 °C, 313 K, 104 °F
Storage Temperature: 2-8°C
Density: 1.641  g/cm3 
Index of Refraction: 1.291
Water Solubility: Hydrolysis
Sensitive: Moisture Sensitive
Surface Tension: 19.3 dyne/cm
Enthalpy of Vaporization: 28.41 kJ/mol 
Vapour Pressure of Trifluoroacetic anhydride (CAS NO.407-25-0): 439 mmHg at 25 °C
Product Categories: Halogen compounds; Organics; Organic Fluorides; Acylation (GC Derivatizing Reagents); Analytical Chemistry; Fluorinated Building Blocks; Fluorinating Reagents & Building Blocks for Fluorinated Biochemical Compounds; GC Derivatizing Reagents; Synthetic Organic Chemistry

Production

 Trifluoroacetic anhydride (CAS NO.407-25-0) may be prepared from trifluoroacetic acid by dehydrating with excess α-halogenated acid chlorides. For example, with dichloroacetyl chloride:
2 CF3COOH + Cl2CHCOCl → (CF3CO)2O + Cl2CHCOOH + HCl

Toxicity Data With Reference

 Trifluoroacetic anhydride (CAS NO.407-25-0) hasn't been listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65. And the toxicological properties have not been fully investigated. You can see actual entry in RTECS for complete information.

Safety Profile

Safety Information of Trifluoroacetic anhydride (CAS NO.407-25-0):
Hazard Codes: C,T
Risk Statements: 14-20-35-52/53-34-23/24/25 
14:  Reacts violently with water
20:  Harmful by inhalation
23:  Toxic by inhalation 
24:  Toxic in contact with skin 
25:  Toxic if swallowed 
34:  Causes burns 
35:  Causes severe burns 
52:  Harmful to aquatic organisms 
53:  May cause long-term adverse effects in the aquatic environment 
Safety Statements: 26-36/37/39-43-45-61-9-8-28A-27
8:  Keep container dry 
9:  Keep container in a well-ventilated
place 
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
27:  Take off immediately all contaminated clothing 
28:  After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer) 
36:  Wear suitable protective clothing  
37:  Wear suitable gloves   
39:  Wear eye/face protection 
43:  In case of fire, use ... (indicate in the space the precise type of fire-fighting equipment. If water increases the risk add - Never use water) 
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) 

Specification

 Trifluoroacetic anhydride , its CAS NO. is 407-25-0,the synonyms is Aceticacid,trifluoro-,anhydride ; Anhydrid kyseliny trifluoroctove ; Anhydridkyselinytrifluoroctove ; Hexafluoroacetic anhydride ; Hexafluoroaceticanhydride ; Perfluoroacetic anhydride ; Perfluoroaceticanhydride ; Trifluoroacetic . In addition, Trifluoroacetic anhydride (CAS NO.407-25-0) could be stable under normal temperatures and pressures, and it absorbs moisture or water from the air. It is not compatible with water, metals, strong oxidizing agents, strong acids, strong bases, alcohols, alkali metals. And also prevent it to broken down into hazardous decomposition products: carbon monoxide, carbon dioxide, hydrogen fluoride gas, fluorine. It will not occur hazardous polymerization.