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Detail of "4071-88-9"

  • MSDS Download
  • CAS Number:
  • 4071-88-9
  • Name:

  • Acetic acid,2-(trimethylsilyl)-, ethyl ester

  • Superlist Name:
  • Ethyl (trimethylsilyl)acetate
  • Molecular Structure:
  • Formula:
  • C7H16O2Si
  • Molecular Weight:
  • 160.29
  • Synonyms:
  • 2-(Trimethylsilyl)acetic acid ethyl ester;Ethyl 2-(trimethylsilyl)acetate;Ethyl a-(trimethylsilyl)acetate;NSC108051;NSC 234752;Aceticacid, (trimethylsilyl)-, ethyl ester (7CI,8CI,9CI);(Trimethylsilyl)acetic acidethyl ester;
  • EINECS:
  • 223-783-2
  • Density:
  • 0.874 g/cm3
  • Boiling Point:
  • 157.5 °C at 760 mmHg
  • Flash Point:
  • 35.8 °C
  • Solubility:
  • Decomposes in water
  • Appearance:
  • clear colorless liquid
  • Risk Codes:
  • 10
  • Safety:
  • 16 Details
  • Transport Information:
  • UN 3272 3/PG 3
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Reference

Indeneacetic acid derivatives
Indeneacetic acid derivatives. (Merck and Co., Inc., USA). Japan. Kokai JP 50123651 29 Sep 1975 Showa, 9 pp. (Japanese). (Japan). CODEN: JKXXAF. CLASS: IC: C07C051-33. PRIORITY: CA 74-193779 28 Feb 1974. DOCUMENT TYPE: Patent CA Section: 26 (Condensed Aromatic Compounds) Indeneacetic acid derivs. (I; R = alkyl, aralkyl, alkali or alk. earth metal; Z = S, SO) were prepd. by condensation of the indanone deriv. (II) with LiCH2CO2R, followed by dehydration of the hydroxy compd., and condensation of the resultant indene deriv. 4071-88-9 and 62634-81-5 are also in the experiment. with p-MeSC6H4CHO (III), and optional oxidn. Thus, 1.1 mol LiCH2CO2CMe3 in PhMe was added to 1 mol II in PhMe and the mixt. heated 2 h at 65.degree. to give tert-Bu 5-fluoro-2-methylindene-3-acetate, which was treated with 2 molar equiv. III in MeOH contg. pyridine and Triton B to give I (R = Me3C, Z = S). .
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