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41052-75-9

Basic Information
CAS No.: 41052-75-9
Name: 2-Chlorophenylhydrazine hydrochloride
Article Data: 9
Molecular Structure:
Molecular Structure of 41052-75-9 (2-Chlorophenylhydrazine hydrochloride)
Formula: C6H7ClN2.HCl
Molecular Weight: 179.049
Synonyms: Hydrazine,(2-chlorophenyl)-, monohydrochloride (9CI);Hydrazine, (o-chlorophenyl)-,hydrochloride (6CI);(o-Chlorophenyl)hydrazizne hydrochloride;o-Chlorophenylhydrazine hydrochloride;
EINECS: 255-194-1
Density: 1.32g/cm3
Melting Point: 200-203 °C (dec.)(lit.)
Boiling Point: 252.1 °C at 760 mmHg
Flash Point: 106.2 °C
Solubility: soluble in water
Appearance: white to slightly yellow crystalline needles or chunks
Hazard Symbols: HarmfulXn, DangerousN, IrritantXi
Risk Codes: 20/21/22-50-50/53-36/37/38
Safety: 36/37-61-36/37/39-29-26-22-36
Transport Information: UN 3077 9/PG 3
PSA: 38.05000
LogP: 3.20090
Synthetic route
95-51-2

2-Chloroaniline

41052-75-9

o-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
Stage #1: o-chloroaniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃;
Stage #2: With hydrogenchloride; tin(ll) chloride In water at 0 - 20℃;
Stage #1: o-chloroaniline With hydrogenchloride; sodium nitrite In water for 0.333333h; Cooling with ice;
Stage #2: With hydrogenchloride; tin(II) chloride dihdyrate In water at -10 - -5℃; for 2h;
Stage #1: o-chloroaniline With hydrogenchloride; sodium nitrite In water at -10 - 0℃; for 0.5h;
Stage #2: With hydrogenchloride; tin(II) chloride dihdyrate In water
Stage #1: o-chloroaniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 1h;
Stage #2: With thionyl chloride In water at 0 - 20℃;
Stage #1: o-chloroaniline With hydrogenchloride In water at 0℃;
Stage #2: With sodium nitrite In water at 0℃; for 0.5h;
Stage #3: With hydrogenchloride; tin(II) chloride hydrate In water at 0℃; for 4h;
41052-75-9

o-chlorophenylhydrazine hydrochloride

123-06-8

Ethoxymethylenemalononitrile

64096-89-5

5-amino-1-(2-chlorophenyl)-1H-pyrazole-4-carbonitrile

Conditions
ConditionsYield
With triethylamine In ethanol at 20℃; for 1.5h; Reflux; Inert atmosphere;100%
With triethylamine
With sodium acetate In ethanol for 1h; Michael Addition; Reflux;
41052-75-9

o-chlorophenylhydrazine hydrochloride

94-05-3

ethyl (ethoxymethylene)cyanoacetate

14678-86-5

ethyl 5-amino-1-(2-chlorophenyl)-1H-pyrazole-4-carboxylate

Conditions
ConditionsYield
In ethanol at 80℃; for 12h;99%
41052-75-9

o-chlorophenylhydrazine hydrochloride

108-24-7

acetic anhydride

14580-00-8

N’-(2-chlorophenyl)acetohydrazide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 24h;98%
13669-28-8

1-methyl-4-methylene-1-azacyclohexane

201230-82-2

carbon monoxide

41052-75-9

o-chlorophenylhydrazine hydrochloride

7-chloro-3-(1-methylpiperidin-4-yl)-1H-indole

Conditions
ConditionsYield
With sulfuric acid; hydrogen; Rh(acac)2(CO)2 at 100℃; under 45003.6 Torr; for 72h;96%
1332635-72-9

C15H14F3NO3

41052-75-9

o-chlorophenylhydrazine hydrochloride

3-(2-chlorophenylhydrazonotrifluoroethyl)-7-(N,N-diethylamino)coumarin

Conditions
ConditionsYield
With toluene-4-sulfonic acid In chlorobenzene Reflux;96%

C17H18N4O*ClH

41052-75-9

o-chlorophenylhydrazine hydrochloride

C23H23ClN6*ClH

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 78℃;95%
4530-20-5

BOC-glycine

41052-75-9

o-chlorophenylhydrazine hydrochloride

tert-butyl (2-(2-(2-chlorophenyl)hydrazineyl)-2-oxoethyl)carbamate

Conditions
ConditionsYield
Stage #1: BOC-glycine With benzotriazol-1-ol; dicyclohexyl-carbodiimide In tetrahydrofuran at 0℃; for 0.25h;
Stage #2: o-chlorophenylhydrazine hydrochloride In tetrahydrofuran at 0 - 20℃; for 1.5h;
95%
41052-75-9

o-chlorophenylhydrazine hydrochloride

108-94-1

cyclohexanone

53475-34-6

8-chloro-2,3,4,9-tetrahydro-1H-carbazole

Conditions
ConditionsYield
With 1,3-bis(3-sulfopropyl)-1H-imidazol-3-ium trifluoromethanesulfonate In water at 100℃; for 0.333333h; Fischer Indole Synthesis; Microwave irradiation; Green chemistry;94%
With 1-(3-sulfopropyl)pyridinium p-toluenesulfonate In water at 100℃; for 0.25h;90%
With acetic acid; trifluoroacetic acid for 2h; Reflux;80%
41052-75-9

o-chlorophenylhydrazine hydrochloride

5305-40-8

2,6-dichloro-pyrimidine carbaldehyde

1429924-47-9

4,6-dichloro-5-{(E)-[(2-chlorophenyl)hydrazono]methyl}pyrimidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere;92%
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Specification

The CAS register number of 2-Chlorophenylhydrazine hydrochloride is 41052-75-9. It also can be called as 1-(2-Chlorophenyl)hydrazine hydrochloride and the IUPAC name about this chemical is (2-chlorophenyl)hydrazine hydrochloride. The molecular formula about this chemical is C6H7ClN2.HCl and the molecular weight is 179.05. It belongs to the following product categories which include Multisubstituted Benzene; Aromatic Hydrazides, Hydrazines, Hydrazones and Oximes; Phenylhydrazine; Hydrazines; Nitrogen Compounds; Organic Building Blocks and so on. This chemical can be used as dye and pharmaceutical intermediates.

Physical properties about 2-Chlorophenylhydrazine hydrochloride are: (1)ACD/LogP: 1.76; (2)#H bond acceptors: 2; (3)#H bond donors: 3; (4)#Freely Rotating Bonds: 2; (5)Polar Surface Area: 6.48Å2 ; (6)Flash Point: 106.2 °C; (7)Enthalpy of Vaporization: 48.94 kJ/mol; (8)Boiling Point: 252.1 °C at 760 mmHg; (9)Vapour Pressure: 0.0197 mmHg at 25°C.

Uses of 2-Chlorophenylhydrazine hydrochloride: it can be used to produce N-azepan-2-ylidene-N'-(2-chloro-phenyl)-hydrazine with 7-methoxy-3,4,5,6-tetrahydro-2H-azepine at heating. This reaction will need solvent methanol with reaction time of 8 hours. The yield is about 50%.

When you are using this chemical, please be cautious about it as the following:
This chemical is very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. It is harmful by inhalation, in contact with skin and if swallowed. This chemical is irritating to eyes, respiratory system and skin. If you want to use this chemical, please Do not empty into drains and do not breathe dust. When you are using it, wear suitable protective clothing, gloves and eye/face protection. After using this chemical, please avoid release to the environment and refer to special instructions / safety data sheets. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: Clc1ccccc1NN.Cl
(2)InChI: InChI=1/C6H7ClN2.ClH/c7-5-3-1-2-4-6(5)9-8;/h1-4,9H,8H2;1H
(3)InChIKey: ADODRSVGNHNKAT-UHFFFAOYAL
(4)Std. InChI: InChI=1S/C6H7ClN2.ClH/c7-5-3-1-2-4-6(5)9-8;/h1-4,9H,8H2;1H
(5)Std. InChIKey: ADODRSVGNHNKAT-UHFFFAOYSA-N