CAS No.4182-80-3,N,N,N',N'-Tetrakis[4-(dibutylamino)phenyl]benzene-1,4-diamine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	4182-80-3
Name:	N,N,N',N'-Tetrakis[4-(dibutylamino)phenyl]benzene-1,4-diamine
Article Data:	5

Formula:	C₆₂H₉₂N₆
Molecular Weight:	921.453
Synonyms:	1,4-Benzenediamine,N,N,N',N'-tetrakis[4-(dibutylamino)phenyl]- (9CI);p-Phenylenediamine, N,N,N',N'-tetrakis[p-(dibutylamino)phenyl]-(7CI,8CI);NIR-AM 1;
EINECS:	224-057-8
Density:	1.024 g/cm³
Melting Point:	92-94 °C
Boiling Point:	916.7 °C at 760 mmHg
Flash Point:	340.7 °C
PSA:	19.44000
LogP:	18.25260

Synthetic route

: 542-69-8
1-iodo-butane

: 3283-07-6
N1,N1,N4,N4-tetrakis(4-aminophenyl)-p-phenylenediamine

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

Conditions

Conditions	Yield
With potassium carbonate In 1-methyl-pyrrolidin-2-one at 80 - 93℃; for 4h;	96%
With potassium carbonate In 1-methyl-pyrrolidin-2-one at 80 - 93℃; for 4h; Product distribution / selectivity;	96%

: 109-65-9
1-bromo-butane

: 3283-07-6
N1,N1,N4,N4-tetrakis(4-aminophenyl)-p-phenylenediamine

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

Conditions

Conditions	Yield
With potassium carbonate In 1-methyl-pyrrolidin-2-one at 80 - 96℃; for 6h; Product distribution / selectivity;	89%

: 53358-54-6
1-bromo-4-(N,N-dibutyl)aniline

: 106-50-3
1,4-phenylenediamine

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

Conditions

Conditions	Yield
With sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium(0) In 1,4-dioxane at 100℃; for 18h;

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: C62H92N6(2+)*2ClO4(1-)

Conditions

Conditions	Yield
Stage #1: N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene With Oxone In acetonitrile at 20℃; for 3h; Stage #2: With sodium perchlorate In acetonitrile at 20℃; for 1h; Product distribution / selectivity;	98%
Stage #1: N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene With iron(II) perchlorate hydrate In N,N-dimethyl-formamide at 70℃; for 5h; Inert atmosphere; Stage #2: With caesium hexafluorophosphate at 20℃; Inert atmosphere;	98%
With Oxone; potassium perchlorate In water; ethyl acetate; acetonitrile at 20℃; for 3.5h; Product distribution / selectivity;	95%

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: C62H92N6(2+)*2F6P(1-)

Conditions

Conditions	Yield
Stage #1: N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene With silver nitrate In N,N-dimethyl-formamide at 70℃; for 5h; Inert atmosphere; Stage #2: With caesium hexafluorophosphate at 20℃; Inert atmosphere;	96%

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: C62H92N6(2+)*O4S(2-)

Conditions

Conditions	Yield
With Oxone; sulfuric acid In water; ethyl acetate; acetonitrile at 20℃; for 3.5h;	92%

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate

: C62H92N6(2+)*2C4BO8(1-)

Conditions

Conditions	Yield
Stage #1: N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene With silver nitrate In N,N-dimethyl-formamide at 70℃; for 5h; Inert atmosphere; Stage #2: lithium bis[1,2-oxalato(2-)-O,O'] borate at 20℃; Inert atmosphere;	90%

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: 189114-61-2
silver(I) triflimide

: bis(trifluoromethanesulfone)imidate N,N,N',N'-tetrakis(p-dibutylaminophenyl)-p-phenylene diimmonium

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 60℃; for 3h; Product distribution / selectivity;

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: 405074-81-9
1-[bis(trifluoromethanesulfonyl)methyl]-2,3,4,5,6-pentafluorobenzene

: 2C9F11O4S2(1-)*C62H92N6(2+)

Conditions

Conditions	Yield
With silver nitrate In N,N-dimethyl-formamide at 60℃; for 0.5h;

: 4182-80-3
N,N,N’,N’-tetrakis[p-di(butyl)aminophenyl]-p-phenylene

: 60805-12-1
tris-(trifluoromethanesulfonyl)methane acid

: 2C4F9O6S3(1-)*C62H92N6(2+)

Conditions

Conditions	Yield
With silver nitrate In water; N,N-dimethyl-formamide at 60℃; for 0.5h;

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Chemistry

Molecular Structure of N,N,N',N'-Tetrakis[4-(dibutylamino)phenyl]benzene-1,4-diamine (CAS NO.4182-80-3):

IUPAC Name: 1-N,1-N-dibutyl-4-N-[4-[4-(dibutylamino)-N-[4-(dibutylamino)phenyl]anilino]phenyl]-4-N-[4-(dibutylamino)phenyl]benzene-1,4-diamine
Empirical Formula: C₆₂H₉₂N₆
Molecular Weight: 921.4341
H bond acceptors: 6
H bond donors: 0
Freely Rotating Bonds: 34
Polar Surface Area: 19.44Å²
Molar Refractivity: 302.38 cm³
Molar Volume: 899.8 cm³
Index of Refraction: 1.586
Surface Tension: 43.5 dyne/cm
Density: 1.023 g/cm³
Flash Point: 340.7 °C
Enthalpy of Vaporization: 133.37 kJ/mol
Boiling Point: 916.7 °C at 760 mmHg
Vapour Pressure: 1.48E-34 mmHg at 25°C
Product Categories: Pharmaceutical Intermediates

Specification

N,N,N',N'-Tetrakis[4-(dibutylamino)phenyl]benzene-1,4-diamine , its cas register number is 4182-80-3. It also can be called 1,4-Benzenediamine, N,N,N,N-tetrakis4-(dibutylamino)phenyl- ; N,N,N',N'-Tetrakis(4-dibutylaminophenyl)-p-phenylenediamine ; N,N,N',N'tetrakis(p-n-butylaminophenyl)-p-phenylenediamine and so on.