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CAS No.: | 4441-12-7 |
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Name: | Trimorpholinophosphine oxide |
Article Data: | 9 |
Molecular Structure: | |
Formula: | C12H24N3O4P |
Molecular Weight: | 305.314 |
Synonyms: | Phosphineoxide, trimorpholino- (6CI,7CI,8CI);NSC 41250;Phosphoric acid trimorpholide;Phosphoric trimorpholide; |
EINECS: | 224-662-7 |
Density: | 1.3 g/cm3 |
Melting Point: | 188-190 °C |
Boiling Point: | 476.4 °C at 760 mmHg |
Flash Point: | 241.9 °C |
Solubility: | 607.20g/L(25 oC) |
Risk Codes: | 36/37/38 |
Safety: | 26-36 |
PSA: | 64.29000 |
LogP: | -0.09520 |
trimorpholylmethane
di-morpholin-4-yl-phosphinic acid chloride
tris(morpholino)phenylphosphine oxide
Conditions | Yield |
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In benzene at 60℃; for 1h; | 60% |
trimorpholylmethane
tris(morpholino)phenylphosphine oxide
Conditions | Yield |
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With trichlorophosphate In benzene for 1h; | 50% |
Conditions | Yield |
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With trichlorophosphate | |
With trichlorophosphate In acetonitrile at -0.16℃; for 4h; | |
With trichlorophosphate In acetonitrile at -0.16℃; for 4h; | |
With trichlorophosphate |
morpholine
P,P-dichlorophenylphosphine oxide
tris(morpholino)phenylphosphine oxide
Conditions | Yield |
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With triethylamine In hexane; toluene for 39h; Cooling with ice; |
Conditions | Yield |
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With eosin y In dichloromethane at 20℃; for 16h; Inert atmosphere; Irradiation; | 88% |
tris(morpholino)phenylphosphine oxide
Conditions | Yield |
---|---|
In chloroform at 20℃; Inert atmosphere; Schlenk technique; | 82.5% |
Conditions | Yield |
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In ethanol; dichloromethane for 24h; | 80.2% |
tris(morpholino)phenylphosphine oxide
LaCl3(tris(morpholino)phenylphosphine oxide)3
Conditions | Yield |
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In chloroform at 20℃; Inert atmosphere; Schlenk technique; | 78.3% |
tris(morpholino)phenylphosphine oxide
Conditions | Yield |
---|---|
In ethanol; dichloromethane for 24h; | 76.6% |
1,1,1,5,5,5-hexafluoroacetylacetone
tris(morpholino)phenylphosphine oxide
neodymium(III) acetate
Conditions | Yield |
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Stage #1: 1,1,1,5,5,5-hexafluoroacetylacetone; neodymium(III) acetate In ethanol; water at 20℃; for 4h; Stage #2: tris(morpholino)phenylphosphine oxide In ethanol; water | 70.2% |