CAS No.4535-90-4,2-METHYLAMINOETHYL CHLORIDE HYDROCHLORIDE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	4535-90-4
Name:	2-METHYLAMINOETHYL CHLORIDE HYDROCHLORIDE
Article Data:	23

Formula:	C3H8 Cl N . Cl H
Molecular Weight:	130.017
Synonyms:	Ethanamine,2-chloro-N-methyl-, hydrochloride (9CI); Ethylamine, 2-chloro-N-methyl-,hydrochloride (6CI,7CI,8CI); 2-(Methylamino)ethyl chloride hydrochloride;2-Chloro-N-methylethylamine hydrochloride; N-Methyl-2-chloroethylaminehydrochloride
Density:	g/cm³
Melting Point:	89 °C
Boiling Point:	110.3°Cat760mmHg
Flash Point:	20.5°C
Safety:	Poison by intravenous route. Moderately toxic by intraperitoneal route. When heated to decomposition it emits very toxic fumes of Cl⁻ and NO_x. See also AMINES.
PSA:	12.03000
LogP:	1.63750

Synthetic route

: 109-83-1
(2-hydroxyethyl)(methyl)amine

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride; thionyl chloride In dichloromethane Ambient temperature;	96%
With thionyl chloride In dichloromethane	96%
With thionyl chloride In chloroform for 6h; Heating;	95%

: 62640-03-3
2-(methylamino)ethan-1-ol hydrochloride

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

Conditions

Conditions	Yield
With sulfuryl dichloride In chloroform at 0℃; for 3h; Reflux;	80%
With thionyl chloride In chloroform at 0℃; Heating / reflux;

: 1072-44-2
N-methylaziridine

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride

methyl-<2-hydroxy-ethyl>-amine hydrochloride: methyl-<2-hydroxy-ethyl>-amine hydrochloride

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride at 160 - 180℃;
With hydrogenchloride at 160 - 180℃;

N-methyl-N-β-naphthhydroxyethyl-p-toluenesulfonic acid amide: N-methyl-N-β-naphthhydroxyethyl-p-toluenesulfonic acid amide

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride at 170℃;

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

: 501-53-1
benzyl chloroformate

: 68767-11-3
benzyl (2-chloroethyl)methylcarbamate

Conditions

Conditions	Yield
With sodium hydroxide for 0.5h;	100%

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

: C15H19ClN2O2S

Conditions

Conditions	Yield
With triethylamine In methanol	96%

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 263719-70-6
N1-BOC,N3-methyl,N3-(2-chloroethyl) sulfamide

Conditions

Conditions	Yield
With isocyanate de chlorosulfonyle; triethylamine In dichloromethane; tert-butyl alcohol at 0 - 25℃; for 2h;	93%
With triethylamine In dichloromethane at 0 - 25℃; for 2.5h;	4.50 g

: 1261237-73-3
cis-[PdCl2(2,6-diisopropylphenylisonitrile)2]

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

: C29H41Cl2N3Pt

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 20℃;	88%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 1′-(diphenylphosphino)-1-isocyanoferrocene

: 4535-90-4
N-methyl-2-chloroethylamine hydrochloride

: C26H25Cl2FeN2PPd

Conditions

Conditions	Yield
With triethylamine In dichloromethane Inert atmosphere; Schlenk technique;	85%

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Chemistry

IUPAC Name: 2-Chloroethyl(methyl)azanium chloride
The MF of Methyl-beta-chloroethylamine hydrochloride (CAS NO.4535-90-4) is C₃H₉Cl₂N.

The MW of Methyl-beta-chloroethylamine hydrochloride (CAS NO.4535-90-4) is 130.01626.
Synonyms of Methyl-beta-chloroethylamine hydrochloride (CAS NO.4535-90-4): N-Methyl-beta-chloroethylamine hydrochloride ; 2-Chloroethyl(methyl)ammonium chloride ; Ethylamine, 2-chloro-N-methyl-, hydrochloride
Flash Point: 20.5 °C
Boiling Point: 110.3 °C
EINECS: 224-882-3

Uses

Methyl-beta-chloroethylamine hydrochloride (CAS NO.4535-90-4) is used as chemical reagent, organic intermediates, fine chemicals, pharmaceutical research and development.

Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mouse	LD50	intraperitoneal	2301mg/kg (2301mg/kg)	BEHAVIORAL: ATAXIA	Journal of Pharmacology and Experimental Therapeutics. Vol. 94, Pg. 249, 1948.
mouse	LD50	intravenous	100mg/kg (100mg/kg)		Journal of Pharmacology and Experimental Therapeutics. Vol. 91, Pg. 224, 1947.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intravenous route. Moderately toxic by intraperitoneal route. When heated to decomposition it emits very toxic fumes of Cl⁻ and NO_x. See also AMINES.