CAS No.500-66-3,Olivetol Suppliers

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Basic Information

Molecular Structure:
CAS No.:	500-66-3
Name:	Olivetol
Article Data:	44

Formula:	C₁₁H₁₆O₂
Molecular Weight:	180.247
Synonyms:	5-Pentylbenzene-1,3-diol;1,3-Dihydroxy-5-pentylbenzene;3,5-Dihydroxyamylbenzene;Resorcinol, 5-pentyl- (8CI);Olivetol(6CI);5-n-Amylresorcinol;5-Pentylresorcinol;5-n-Pentylresorcinol;
EINECS:	207-908-8
Density:	1.069 g/cm³
Melting Point:	46-48 °C(lit.)
Boiling Point:	313.259 °C at 760 mmHg
Flash Point:	148.758 °C
Solubility:	insoluble in water
Appearance:	light purple to brown crystalline mass
Hazard Symbols:	Xi
Risk Codes:	36/37/38
Safety:	26-36/39
PSA:	40.46000
LogP:	2.83050

Synthetic route

: 22976-40-5
1,3-dimethoxy-5-pentylbenzene

: 500-66-3
Olivetol

Conditions

Conditions	Yield
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Solvent; Reagent/catalyst; Inert atmosphere;	95%
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Inert atmosphere;	92%
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Inert atmosphere;	92%

: 58016-28-7
methyl 2,4-dihydroxy-6-pentylbenzoate

: 500-66-3
Olivetol

Conditions

Conditions	Yield
With water; potassium hydroxide at 50 - 100℃;	94%

: 1,3-Bis-benzyloxy-5-((Z)-pent-1-enyl)-benzene

: 500-66-3
Olivetol

Conditions

Conditions	Yield
With sodium; butan-1-ol at 80 - 90℃; for 1h;	81%
With hydrogen; palladium on activated charcoal In ethanol Yield given;

: 3,5-diamino-1-pentylbenzene

: 500-66-3
Olivetol

Conditions

Conditions	Yield
Stage #1: 3,5-diamino-1-pentylbenzene With sulfuric acid; sodium nitrite In dichloromethane at 5℃; Stage #2: With sulfuric acid; sodium sulfate In water for 1h; Reflux;	78%

: 27871-89-2
methyl 6-n-pentyl-2-hydroxy-4-oxo-cyclohex-2-ene-1-carboxylate

: 500-66-3
Olivetol

Conditions

Conditions	Yield
With bromine In N,N-dimethyl-formamide at 160℃; for 10h; Cooling with ice;	69.3%
With bromine In N,N-dimethyl-formamide at 80 - 160℃;	69.3%
With bromine In N,N-dimethyl-formamide at 160℃; for 11.5h; Cooling with ice;	69.3%
With bromine In N,N-dimethyl-formamide at 160℃; for 10h; Cooling with ice;	69.3%
With bromine In N,N-dimethyl-formamide at 80 - 160℃; for 11.5h; Cooling with ice;	69.3%

: 74732-76-6
4-Benzenesulfinyl-5-pentyl-cyclohexane-1,3-dione

: 500-66-3
Olivetol

Conditions

Conditions	Yield
With calcium carbonate In benzene for 5h; Heating;	48%

: 58016-30-1
5-n-amyl-2-bromocyclohex-2-ene-3-ol-1-one

A: 78463-35-1
4-bromo-5-pentylbenzene-1,3-diol

B: 78463-34-0
4,6-dibromo-5-pentylbenzene-1,3-diol

C: 500-66-3
Olivetol

Conditions

Conditions	Yield
In diphenylether heating to 155 deg C during 1 h;	A 32% B 10% C 40%

...Expand

: 67-56-1
methanol

: 491-47-4
olivetoric acid

A: 3734-54-1
6,8-dihydroxy-3-pentyl-1H-2-benzopyran-1-one

B: 500-66-3
Olivetol

Conditions

Conditions	Yield
at 150 - 200℃;

...Expand

: 64-18-6
formic acid

: 491-47-4
olivetoric acid

A: 3734-54-1
6,8-dihydroxy-3-pentyl-1H-2-benzopyran-1-one

B: 500-66-3
Olivetol

...Expand

: 13956-29-1
CBD

: 628-13-7
pyridine hydrochloride

A: 99-87-6
4-methylisopropylbenzene

B: 500-66-3
Olivetol

Conditions

Conditions	Yield
at 210 - 230℃;

...Expand

Raw Materials

64-18-6

Downstream Products

142-62-1

Total:175 Page 1 of 5 1 2 3 4 5 Next>>

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Chemistry

Molecular Formula: C₁₆H₂₆N₂O₂
Molecular Weight: 278.3898 g/mol
EINECS: 207-908-8
Index of Refraction: 1.546
Surface Tension: 43.5 dyne/cm
Melting point: 46-48 °C
Density: 1.068 g/cm³
Flash Point: 148.8 °C
Solubility in water: Slightly soluble
Enthalpy of Vaporization: 57.64 kJ/mol
Boiling Point: 313.3 °C at 760 mmHg
Vapour Pressure: 0.000273 mmHg at 25 °C
Appearance: Off-white crystals or olive to light purple waxy solid
Product Category of Olivetol (CAS NO.500-66-3): API intermediates
Following is the structure of Olivetol (CAS NO.500-66-3):

Safety Profile

Hazard Codes: Irritant Xi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36:Wear suitable protective clothing.
S39:Wear eye / face protection.
WGK Germany: 3
RTECS: VH2880000

Specification

Olivetol, its cas register number is 500-66-3. It also can be called 3,5-Dihydroxyamylbenzene ; 3-06-00-04695 (Beilstein Handbook Reference) ; 5-Pentyl-1,3-benzenediol ; 5-Pentylresorcinol ; 5-n-Amylresorcinol ; 5-n-Pentylresorcinol. And its IUPAC name is [3-(diethylamino)-2,2-dimethylpropyl] 4-aminobenzoate. Olivetol (CAS NO.500-66-3) is hazardous, so the first aid measures and others should be known. Such as: When on the skin: first, should flush skin with plenty of water immediately for at least 15 minutes while removing contaminated clothing and shoes. Secondly, get medical aid. Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Then get medical aid soon. While, it's inhaled: Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical aid. And as soon as to get medical aid. If you have the ingesting of the product : Never give anything by mouth to an unconscious person. Get medical aid. Do not induce vomiting. If conscious and alert, rinse mouth and drink 2-4 cupfuls of milk or water.
In addition, Olivetol should be stored in a tightly closed container, or stored in a cool, dry, well-ventilated area away from incompatible substances as well as stored protected from light.

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