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52605-52-4

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Basic Information
CAS No.: 52605-52-4
Name: 1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride
Article Data: 4
Molecular Structure:
Molecular Structure of 52605-52-4 (1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride)
Formula: C13H18Cl2N2.HCl
Molecular Weight: 309.666
Synonyms: Piperazine,1-(3-chlorophenyl)-4-(3-chloropropyl)-, monohydrochloride (9CI);
EINECS: 258-038-0
Melting Point: 198-203 °C(lit.)
Boiling Point: 395.8 °C at 760 mmHg
Flash Point: 193.2 °C
Solubility: 3.9g/L at 28℃
Appearance: off-white solid
Hazard Symbols: IrritantXi,HarmfulXn
Risk Codes: 36/37/38-20/21/22
Safety: 26-37/39-24/25
PSA: 6.48000
LogP: 3.89580
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Synthetic route
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52605-52-4

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Conditions
ConditionsYield
Stage #1: 1-(3-chlorophenyl)piperazine hydrochloride; 1.3-chlorobromopropane With tetrabutylammomium bromide; potassium carbonate In acetonitrile for 0.0111111h; Microwave irradiation;
Stage #2: With hydrogenchloride In 1,4-dioxane; acetone Solvent;		88%
ice-H2 O

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52605-52-4

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Conditions
ConditionsYield
With sodium hydroxide In hydrogenchloride; water; acetone55.6%
...Expand
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3-chloropropanaldehyde

13078-15-4

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1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

Conditions
ConditionsYield
Stage #1: 3-chloropropanaldehyde; 1-(3-chlorophenyl)piperazine hydrochloride In dichloromethane for 0.25h; Inert atmosphere;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane Inert atmosphere;
52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

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trazodone

Conditions
ConditionsYield
With sodium hydroxide In isopropyl alcohol for 26h; Reagent/catalyst; Inert atmosphere; Reflux;92%
With tetrabutylammomium bromide; potassium carbonate In acetonitrile for 0.0222222h; Time; Microwave irradiation;92%
52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

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Conditions
ConditionsYield
With hydrazine In isopropyl alcohol85%
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5-ethyl-4-(2-phenoxyethyl)-2H-1,2,4-triazol-3(4H)-one

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nefazadone

Conditions
ConditionsYield
With sodium hydroxide In isopropyl alcohol for 7h; Heating;84%
52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

1,2,4-triazolo<4,3-a>pyridin-3(2H)-one sodium salt

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trazodone hydrochloride

Conditions
ConditionsYield
With tetrabutylammomium bromide; sodium carbonate In isopropyl alcohol at 80 - 85℃; for 12h; Reagent/catalyst;83%
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daidzein

52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

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Conditions
ConditionsYield
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 80℃; for 4h;68.2%
13754-86-4

1,5,6,7-tetrahydro-indol-4-one

52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

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1-{3-[4-(3-chlorophenyl)piperazine-1-yl]propyl}-1,5,6,7-tetrahydroindol-4-one

Conditions
ConditionsYield
With hydrogenchloride; sodium hydroxide In 1,4-dioxane; dichloromethane; dimethyl sulfoxide
With hydrogenchloride; sodium hydroxide In 1,4-dioxane; dichloromethane; dimethyl sulfoxide
Stage #1: 1,5,6,7-tetrahydro-indol-4-one With sodium hydroxide In dimethyl sulfoxide at 25℃; for 0.25h;
Stage #2: 1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride In dimethyl sulfoxide
With hydrogenchloride; sodium hydroxide In 1,4-dioxane; dichloromethane; dimethyl sulfoxide
5-(2Methyl-1,4-dixolan-2yl)-4-(2-phenoxyethyl)-2,4-dihydro-3H-1,2,4-triazol-3-one

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52605-52-4

1-(3-chloropropyl)-4-(3-chlorophenyl)piperazine hydrochloride

2-(3-[4-(3-Chlorophenyl)-1-piperazinyl]propyl)-5-(2-methyl-1,4-dioxolan-2-yl)-2,4-dihydro-4-(2-phenoxyethyl)-3H-1,2,4-triazol-3-one

Conditions
ConditionsYield
With sodium hydroxide; Ki In acetonitrile
...Expand
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  • 1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride CAS:52605-52-4

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    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

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  • 1-(3-chlorophenyl)-4-(3-chloropropyl)-piperazine hydrochloride

  • Casno:

    52605-52-4

    1-(3-chlorophenyl)-4-(3-chloropropyl)-piperazine hydrochloride

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    high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

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Chemistry

Molecular Structure of 1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride (CAS NO.52605-52-4):

IUPAC Name: 1-(3-chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride 
Empirical Formula: C13H19Cl3N2
Molecular Weight: 309.6624
H bond acceptors: 2
H bond donors: 0
Freely Rotating Bonds: 4
Polar Surface Area: 3.24 Å2
Flash Point: 193.2 °C
Enthalpy of Vaporization: 64.6 kJ/mol
Boiling Point: 395.8 °C at 760 mmHg
Vapour Pressure: 1.79E-06 mmHg at 25°C
Melting point: 198-203 °C(lit.)
Smiles
N1(c2cc(Cl)ccc2)CCN(CC1)CCCCl.Cl
EINECS: 258-038-0
Product Categories: Piperidines, Piperidones, Piperazines; Piperazine derivates; Building Blocks; Halogenated Heterocycles; Heterocyclic Building Blocks; Piperazines; PiperazinesHeterocyclic Building Blocks

Safety Profile

Hazard Codes: IrritantXi,HarmfulXn
Risk Statements: 36/37/38-20/21/22
R36/37/38:Irritating to eyes, respiratory system and skin. 
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed.
Safety Statements: 26-37/39-24/25
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39:Wear suitable gloves and eye/face protection. 
S24/25:Avoid contact with skin and eyes.
WGK Germany: 3
F: 10-21

Specification

  1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride , with CAS number of 52605-52-4, can be called piperazine, 1-(3-chlorophenyl)-4-(3-chloropropyl)-, hydrochloride (1:1) ; 1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazine hydrochloride (1:1) .