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532-12-7

Basic Information
CAS No.: 532-12-7
Name: MYOSMINE
Article Data: 44
Molecular Structure:
Molecular Structure of 532-12-7 (MYOSMINE)
Formula: C9H10 N2
Molecular Weight: 146.192
Synonyms: Pyridine,3-(1-pyrrolin-2-yl)- (6CI,7CI,8CI); 2-(3-Pyridyl)-1-pyrroline; Myosmine
Density: 1.12g/cm3
Melting Point: 42-44°C
Boiling Point: 82-83°C 0,5mm
Flash Point: 101.8°C
Appearance: Light Yellow Powder
Hazard Symbols: R22:Harmful if swallowed.;
Risk Codes: R22;
Safety: 119254
PSA: 25.25000
LogP: 1.10010
Synthetic route
36740-10-0

4-oxo-4-(pyridin-3-yl)butanenitrile

532-12-7

Myosmine

Conditions
ConditionsYield
With ammonia; hydrogen; nickel In ethanol at 0℃;85%
With ammonia; hydrogen; nickel In ethanol for 20h;69%

1-(pyridin-3-yl)cyclobutane-1-carboxamide

532-12-7

Myosmine

Conditions
ConditionsYield
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile at 20℃; for 12h;83%
93-60-7

methyl 3-pyridinecarboxylate

117593-76-7

N-butenylpyrrolidone

532-12-7

Myosmine

Conditions
ConditionsYield
Stage #1: methyl 3-pyridinecarboxylate; 1-(but-1-enyl) pyrrolidin-2-one With sodium hydride In N,N-dimethyl-formamide at 90℃; for 2h;
Stage #2: With hydrogenchloride In water at 110℃; for 12h;
Stage #3: With sodium hydroxide In water at 0℃; pH=14;
77.2%
1308392-26-8

1-(but-1-enyl)-3-nicotinoylpyrrolidin-2-one

532-12-7

Myosmine

Conditions
ConditionsYield
Stage #1: 1-(but-1-enyl)-3-nicotinoylpyrrolidin-2-one With hydrogenchloride In water for 12h; Reflux;
Stage #2: With sodium hydroxide In water at 0℃; pH=> 13;
70%
87549-96-0

1-(pyridin-3-yl)cyclobutanol

532-12-7

Myosmine

Conditions
ConditionsYield
With hydrogen azide; sulfuric acid In dichloromethane at 0℃;65%
With hydrogen azide; sulfuric acid In dichloromethane at 0℃; Mechanism; substrate: 1-(3-pyridyl) cyclopentanol;65%
36740-10-0

4-oxo-4-(pyridin-3-yl)butanenitrile

A

532-12-7

Myosmine

B

5746-86-1

rac-nornicotine

Conditions
ConditionsYield
With ammonia; hydrogen; nickel In ethanol for 40h; Product distribution; various concentrations and temperatures;A 53%
B 13%
123-75-1

pyrrolidine

1120-90-7

3-iodopyridine

A

110-86-1

pyridine

B

532-12-7

Myosmine

Conditions
ConditionsYield
With tert-butylethylene; RhCl(CO)(PFur3)2; caesium carbonate In 1,4-dioxane at 120℃; for 12h;A n/a
B 39%
22083-74-5

3-(1-methyl-pyrrolidin-2-yl)-pyridine

A

532-12-7

Myosmine

B

525-74-6

N-methylmyosmine

C

487-19-4

nicotirine

D

15569-85-4

cotinine

E

3-(1-Methyl-2,3-dihydro-1H-pyrrol-2-yl)-pyridine

Conditions
ConditionsYield
With 9,10-Dicyanoanthracene; oxygen In acetonitrile for 22h; Mechanism; Irradiation; also TiO2 as electron acceptor, in absence of O2;A 0.27%
B n/a
C 0.11%
D 1.05%
E n/a
614-18-6

3-pyridinecarboxylic acid ethyl ester

2399-66-8

1-benzoylpyrrolidin-2-one

141-52-6

sodium ethanolate

71-43-2

benzene

532-12-7

Myosmine

Conditions
ConditionsYield
at 110 - 115℃; Erhitzen des Reaktionsprodukts mit wss.Salzsaeure auf 130grad.;
614-18-6

3-pyridinecarboxylic acid ethyl ester

2399-66-8

1-benzoylpyrrolidin-2-one

532-12-7

Myosmine

Conditions
ConditionsYield
With sodium ethanolate; benzene Erhitzen des Reaktionsprodukts mit wss. HCl auf 130grad;
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    China (Mainland)  |  Contact Details

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    United States  |  Contact Details

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    China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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