Detail of "55886-71-0"

CAS Number:
55886-71-0
Name:
benzenethiolate; cobalt; N-[(Z)-3-nitrosobut-2-en-2-yl]hydroxylamine; 4-tert-butylpyridine
Molecular Structure:
Formula:
C₂₃H₃₄CoN₅O₄S-
Molecular Weight:
535.5459
Density:
g/cm³
Boiling Point:
197.1°Cat760mmHg
Flash Point:
63.3°C

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(Benzenethiolato-S)(4-tert-butylpyridine-N)bis(dimethylglyoximato-N,N') cobalt(III) and (4-tert-butylpyridine-N)bis(dimethylglyoximato-N,N')(4-methoxybenzenet hiolato-S)cobalt(III): Inouye, Yoshinobu; Kambe, Tohru; Tada, Masaru (Dep. Chem., Univ. Tsukuba, Tsukuba, Ibaraki 305, Japan). Acta Crystallographica, Section C: Crystal Structure Communications, C54(7), 945-947 (English) 1998 Munksgaard International Publishers Ltd. CODEN: ACSCEE. ISSN: 0108-2701. DOCUMENT TYPE: Journal CA Section: 75 (Crystallography and Liquid Crystals) Section cross-reference(s): 78 Crystals of (benzenethiolato-S)(4-tert-butylpyridine-N)bis(dimethylglyoximato-N,N') cobalt(III) (I) are monoclinic, space group P21/a, with a 23.630(6), b 10.9850(10), c 9.779(3) ?, and b 91.060(10)°; Z = 4, dc = 1.396; R = 0.034, Rw(F2) = 0.090 for 4469 reflections. Crystals of (4-tert-butylpyridine-N)bis(dimethylglyoximato-N,N')(4-methoxybenzenet hiolato-S)cobalt(III) (II) are orthorhombic, space group P212121, with a 12.8980(10), b 18.482(2), c 11.4120(10) ?; Z = 4, dc = 1.Several reagents such as 55886-71-0 is used here.376; R = 0.035, Rw(F2) = 0.090 for 2704 reflections. The Co-S distances are 2.2800(8) and 2.2885(15) ? in I and II, resp. The electron-donating substituent on the para position of the arylthiolate lengthens the Co-S bond. .