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56-24-6

Basic Information
CAS No.: 56-24-6
Name: TRIMETHYLTIN HYDROXIDE
Article Data: 50
Molecular Structure:
Molecular Structure of 56-24-6 (TRIMETHYLTIN HYDROXIDE)
Formula: C3H10 O Sn
Molecular Weight: 180.822
Synonyms: Tin,hydroxytrimethyl- (7CI); Trimethyltin hydroxide (6CI);Hydroxytrimethylstannane; Hydroxytrimethyltin; Trimethylhydroxytin;Trimethylstannanol; Trimethylstannyl hydroxide
Density: g/cm3
Melting Point: 118°C
Boiling Point: 80°C
Flash Point: °C
Solubility: Soluble in water.
Hazard Symbols: A poison. TWA 0.1 mg(Sn)/m3; STEL 0.2 mg(Sn)/m3 (skin).
Risk Codes:  T+:Very toxic;
">  T+:Very toxic;
Safety: Poison by subcutaneous route. When heated to decomposition it emits acrid smoke and irritating fumes. See also TIN COMPOUNDS.

Analytical Methods:

   

For occupational chemical analysis use NIOSH: Organotin Compounds 5504.

PSA: 20.23000
LogP: 0.81360
Synthetic route
27640-06-8

(CH3)3SnCH2C6H4-m-Cl

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water byproducts: m-chlorotoluene; refluxing for 52 h;;85%
With NaOH In ethanol; water byproducts: m-chlorotoluene; refluxing for 52 h;;85%
In methanol; deuteromethanol byproducts: m-chlorotoluene; alkaline decompn. at 50°C;;
In methanol; deuteromethanol byproducts: m-chlorotoluene; alkaline decompn. at 50°C;;
1692-18-8

bis(trimethyltin)oxide

74-86-2

acetylene

A

1112-00-1

trimethylstannylacetylene

B

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
at 8-12 atm in a sealed tube;;A 65.5%
B n/a
697-91-6

2,6-dichloro-1,4-benzoquinone

661-69-8

hexamethyldistannane

A

76279-09-9

C6Cl2H2(OSn(CH3)3)2

B

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
In benzene keeping at room temp. (N2) for 4 d; various yields in various conditions; evapn.; elem. anal.;A 63%
B n/a
7029-29-0

tris(trimethylstannyl)stibine

A

1692-18-8

bis(trimethyltin)oxide

B

68354-51-8

tetrakis(trimethylstannyl)distibane

C

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With oxygen In neat (no solvent) stibane left in air for 3 d; suspending in Ar-satd. acetone, decanting, recrystn. of red residue from toluene (2nd and 3rd product isolated from acetone suspn.); elem. anal.;A n/a
B 47%
C n/a
16393-88-7

trimethyl(trimethylstannyl)silane

A

107-46-0

Hexamethyldisiloxane

B

661-69-8

hexamethyldistannane

C

1631-73-8

trimethylstannane

D

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With bromobenzene; calcium In water for 1h; Ambient temperature; Further byproducts given;A 36%
B 8%
C 42%
D 10%
16393-88-7

trimethyl(trimethylstannyl)silane

A

107-46-0

Hexamethyldisiloxane

B

934-56-5

trimethyl(phenyl)stannane

C

661-69-8

hexamethyldistannane

D

1631-73-8

trimethylstannane

E

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With bromobenzene; water; calcium In gas Ca vaporized at 900°C in vac. (ca. 5E-3 Torr), Me3SiSnMe3 introduced as vapor, mixed vapor condensed on cold (77 K) walls, warmed to room temp., excess of C6H5Br admitted as vapor, left to stand for 1 h, hydrolyzed with water; org. layer extd. with ether, products identified by GC-MASS, GLC;A 36%
B 2%
C 8%
D 42%
E 10%
1066-44-0

trimethyltin bromide

B

594-27-4

tetramethylstannane

C

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With zinc In water
With Zn In water
1015-53-8

(pentafluorophenyl)trimethyltin

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With F(1-) or Cl(1-) or CN(1-) In water byproducts: C6F5H;
With F(1-) or Cl(1-) or CN(1-) In ethanol; water byproducts: C6F5H;
With NaF or NaOH In water byproducts: C6HF5;
86108-56-7

2-(trimethylstannyl)-1-methylimidazole

A

616-47-7

1-methyl-1H-imidazole

B

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With water
108202-42-2

((methyl)3tin)2C(CON(methyl)2)2

56-24-6

trimethyltin(IV) hydroxide

Conditions
ConditionsYield
With water byproducts: N,N,N',N'-tetramethylmalondiamide; hydrolysis;
Downstream Products
594-27-4
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Chemistry

IUPAC Name: Trimethyl tin hydrate (56-24-6)
Synonyms: Trimethyltin hydrate ; Hydroxytrimethyl-stannan ; Hydroxytrimethylstannane ; Hydroxytrimethyl-ti ; Hydroxytrimethyltin ; Trimethylhydroxytin ; Trimethylstannanol
CAS: 56-24-6
Molecular Formula of Trimethyl tin hydrate (56-24-6): C3H10OSn
Molecular Weight of Trimethyl tin hydrate (56-24-6) :180.82
 Molecular Structure of Trimethyl tin hydrate (56-24-6) :
Mol File: 56-24-6.mol
Flash Point: 25.8 °C 
Enthalpy of Vaporization: 41.64 kJ/mol 
Boiling Point: 119.1 °C at 760 mmHg
Melting point: 118°C  
Vapour Pressure: 7.91 mmHg at 25°C

Toxicity Data With Reference

1.    

scu-mus LDLo:1800 µg/kg

    JPETAB    Journal of Pharmacology and Experimental Therapeutics. 28 (1926),367.

Safety Profile

Risk Statements  20/21/22
20/21/22: Trimethyl tin hydrate (56-24-6) is  harmful by inhalation, in contact with skin and if swallowed  
Safety Statements  22-36/37/39-45
22:  Do not breathe dust 
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) 
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection  
RIDADR  3146
HazardClass  6.1
PackingGroup  III

Standards and Recommendations

OSHA PEL: TWA 0.1 mg(Sn)/m3 (skin)
ACGIH TLV: TWA 0.1 mg(Sn)/m3; STEL 0.2 mg(Sn)/m3 (skin).
NIOSH REL: (Organotin Compounds) TWA 0.1 mg(Sn)/m3

Analytical Methods

For occupational chemical analysis use NIOSH: Organotin Compounds 5504.