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56718-71-9

Basic Information
CAS No.: 56718-71-9
Name: p-(2-Methoxyethyl) phenol
Article Data: 21
Molecular Structure:
Molecular Structure of 56718-71-9 (p-(2-Methoxyethyl) phenol)
Formula: C9H12O2
Molecular Weight: 152.193
Synonyms: Phenol,p-(2-methoxyethyl)- (6CI,7CI);4-(2-Methoxyethyl)phenol;p-Hydroxyphenethyl methyl ether;4-(2-methoxyethyl)-phenol;
EINECS: 260-354-9
Density: 1.06 g/cm3
Melting Point: 42-45 °C(lit.)
Boiling Point: 239.9 °C at 760 mmHg
Flash Point: 97.8 °C
Solubility: 8.42g/L at 20℃
Appearance: White Powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 29.46000
LogP: 1.58110
Synthetic route
32136-81-5

alpha-methoxy-4-hydroxyacetophenone

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethanol under 2327.2 Torr; for 4h;96%
With hydrogen under 3000.3 Torr; Pressure; Heating;80%
With hydrogen; acetic acid; palladium on activated charcoal
With H2; acetic acid; palladium-carbon0.54 g (3.6 mmol=61%)

4-hydroxyphenyl glyoxal dimethylacetal

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
palladium-carbon In hydrogenchloride; methanol70%
With hydrogen; palladium-carbon In hydrogenchloride; methanol59%
With hydrogen; palladium-carbon In methanol53%
With hydrogenchloride; hydrogen; palladium-carbon In methanol47%
501-94-0

p-hydroxyphenethyl alcohol

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With sulfuric acid In methanol40%
In methanol31%
Multi-step reaction with 3 steps
1: ethanol / 9 h / Heating
2: 1.) NaH / 1.) THF, reflux, 30 min; 2.) THF, reflux, 6 h
3: H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr / Ambient temperature
View Scheme

4-(2-methoxyethenyl)phenol

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With hydrogen In ethyl acetate at 50℃; under 30402 Torr; for 16h;10 g
67-56-1

methanol

28145-35-9

4-(2-chloroethyl)phenol

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With sodium methylate at 50℃; for 7h; Reagent/catalyst;92%
98627-35-1

1-(benzyloxy)-4-(2-methoxyethyl)benzene

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In tetrahydrofuran at 20℃; under 3000.3 Torr; for 24h;82%
With hydrogen; palladium on activated charcoal In ethanol under 3102.9 Torr; for 24h; Ambient temperature;
With palladium 10% on activated carbon; hydrogen under 37503.8 Torr; for 3h;38.6 g
953422-33-8

2-(4'-hydroxyphenyl)ethyl methyl carbonate

616-38-6

carbonic acid dimethyl ester

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
With Amberlyst 15 for 36h; Reflux;95%
501-94-0

p-hydroxyphenethyl alcohol

144-55-8

sodium hydrogencarbonate

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
In methanol65%
67-56-1

methanol

4-((3H-diazirin-3-yl)methyl)phenol

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
at 20℃; for 2h; Inert atmosphere; UV-irradiation;57%
14140-15-9

4-(2-bromoethyl)phenol

124-41-4

sodium methylate

56718-71-9

4-(2-methoxyethyl)phenol

Conditions
ConditionsYield
In methanol at 20℃; for 3h;79%
With methanol
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Specification

The 4-(2-Methoxyethyl)-phenol is an organic compound with the formula C9H12O2. The systematic name of this chemical is 4-(2-methoxyethyl)phenol. With the CAS registry number 56718-71-9, it is also named as phenol, 4-(2-methoxyethyl)-. The product's categories are Aromatic Phenols; Phenoles and Thiophenoles; Various Metabolites and Impurities; Intermediates & Fine Chemicals; Metabolites & Impurities; Pharmaceuticals; Organic Building Blocks; Oxygen Compounds; Phenols. Besides, it should be stored in a closed cool and dry place. It is an important pharmaceutical intermediate, which is mainly used to produce an effective drug in the treatment of cardiovascular disease.

Physical properties about 4-(2-Methoxyethyl)-phenol are: (1)ACD/LogP: 1.41; (2)ACD/LogD (pH 5.5): 1.41; (3)ACD/LogD (pH 7.4): 1.4; (4)ACD/BCF (pH 5.5): 6.88; (5)ACD/BCF (pH 7.4): 6.87; (6)ACD/KOC (pH 5.5): 138.48; (7)ACD/KOC (pH 7.4): 138.14; (8)#H bond acceptors: 2; (9)#H bond donors: 1; (10)#Freely Rotating Bonds: 4; (11)Polar Surface Area: 18.46 Å2; (12)Index of Refraction: 1.525; (13)Molar Refractivity: 44.06 cm3; (14)Molar Volume: 143.5 cm3; (15)Polarizability: 17.46×10-24cm3; (16)Surface Tension: 38.8 dyne/cm; (17)Density: 1.06 g/cm3; (18)Flash Point: 97.8 °C; (19)Enthalpy of Vaporization: 49.62 kJ/mol; (20)Boiling Point: 239.9 °C at 760 mmHg; (21)Vapour Pressure: 0.0252 mmHg at 25°C.

Preparation: this chemical can be prepared by 1-(4-hydroxy-phenyl)-2-methoxy-ethanone. This reaction will need reagent H2, catalyst 10 percent Pd/C and solvent ethanol. The reaction time is 4 hours. The yield is about 96%.



Uses of 4-(2-Methoxyethyl)-phenol: it can be used to produce 1-allyloxy-4-(2-methoxy-ethyl)-benzene by heating. It will need reagent K2CO3 and solvent acetone with reaction time of 7 hours. The yield is about 85%.

When you are using this chemical, please be cautious about it as the following:
This chemical is irritating to eyes, respiratory system and skin. When you are using it, wear suitable protective clothing. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: Oc1ccc(cc1)CCOC
(2)InChI: InChI=1/C9H12O2/c1-11-7-6-8-2-4-9(10)5-3-8/h2-5,10H,6-7H2,1H3
(3)InChIKey: FAYGEALAEQKPDI-UHFFFAOYAX
(4)Std. InChI: InChI=1S/C9H12O2/c1-11-7-6-8-2-4-9(10)5-3-8/h2-5,10H,6-7H2,1H3
(5)Std. InChIKey: FAYGEALAEQKPDI-UHFFFAOYSA-N