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57266-69-0

Basic Information
CAS No.: 57266-69-0
Name: 3-Chloropicolinic acid
Article Data: 7
Molecular Structure:
Molecular Structure of 57266-69-0 (3-Chloropicolinic acid)
Formula: C6H4ClNO2
Molecular Weight: 157.556
Synonyms: 3-Chloro-2-pyridinecarboxylicacid;
Density: 1.47 g/cm3
Melting Point: 148-150 °C
Boiling Point: 297.6 °C at 760 mmHg
Flash Point: 133.8 °C
Appearance: off-white solid
Hazard Symbols: IrritantXi,HarmfulXn
Risk Codes: 22-36
Safety: 26
PSA: 50.19000
LogP: 1.43320
Synthetic route

lithium; 3-chloro-pyridine-2-carboxylate

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
With Amberlyst(R) IR-200 In methanol at 20℃; for 0.25h;53%
72093-03-9

3-chloro-2-methylpyridine

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
With potassium permanganate for 21.5h; Heating;45%
1462-86-8

3-amino-pyridine-2-carboxylic acid

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite Anschliessend Behandeln mit CuCl;
57841-92-6

3-chloropicolinanilide

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
With hydrogenchloride for 15h; Heating;
98-98-6

2-Picolinic acid

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: BuLi; 2,2,6,6-tetramethylpiperidine / tetrahydrofuran; hexane / 0.67 h / -75 - 0 °C
1.2: 72 percent / hexachloroethane / tetrahydrofuran; hexane / 0 - 20 °C
2.1: 53 percent / Amberlyst(R) IR-200 / methanol / 0.25 h / 20 °C
View Scheme
10354-53-7

N-phenylpicolinamide

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) n-BuLi, 2.) CCl3CCl3 / 1.) THF, -78 deg C - 0.5 h, room temperature - 1 h, 2.) THF, -78 deg C - 1 h, room temperature - 2 h
2: aq. HCl / 15 h / Heating
View Scheme
38180-46-0

3-chloro-2-cyanopyridine

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
In methanol; sodium hydroxide; dichloromethane
With sodium hydroxide at 95℃; for 2h; pH=2-3;
1702-17-6

Clopyralid

A

98-98-6

2-Picolinic acid

B

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
With Graphite; sodium hydroxide In water at 25℃; for 3h; Electrolysis;
With Graphite; sodium hydroxide In water at 25℃; for 6h; pH=11.5 - 13.5; Reagent/catalyst; pH-value; Electrolysis;
462-08-8

pyridin-3-ylamine

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydrogenchloride; dihydrogen peroxide / water / 2 h / 5 °C
1.2: 0.42 h / -5 °C
1.3: 1.33 h / 15 - 30 °C
2.1: hydrazine hydrate / ethanol / 6 h / Reflux; Inert atmosphere
3.1: sodium hydroxide / 2 h / 95 °C / pH 2-3
View Scheme
2402-77-9

2,3-dichloro-pyridine

57266-69-0

3-chloropyridine-2-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / ethanol / 6 h / Reflux; Inert atmosphere
2: sodium hydroxide / 2 h / 95 °C / pH 2-3
View Scheme
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    3-CHLOROPICOLINIC ACID

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  • 57266-69-0  CAS NO.57266-69-0

  • Casno:

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    57266-69-0 CAS NO.57266-69-0

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  • 3-Chloropicolinic acid

  • Casno:

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    3-Chloropicolinic acid

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    3-Chloropicolinic acid

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  • 3-chloro-2-picolinic acid cas no. 57266-69-0 97%

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    3-Chloropyridine-2-carboxylic acid

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    57266-69-0

    3-Chloropicolinic acid

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    3-Chloropicolinic Acid

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    3-Chloropyridine-2-carboxylic acid

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Specification

The 3-Chloropicolinic acid has the cas register number 57266-69-0. And it has other names as iflab-bb f1926-0037; 3-chloropyridine-2-carboxylic acid; 3-chloropicolinic acid; 3-chloropyridine-2-carboxylicacid98%; 3-chloro-2-pyridinecarboxylic; 3-chloro-2-picolinic acid.

The physical properties of this chemical are as followings: (1)ACD/LogP: 0.30 ; (2)ACD/BCF (pH 5.5): 1; (3)ACD/BCF (pH 7.4): 1; (4)ACD/KOC (pH 5.5): 1; (5)ACD/KOC (pH 7.4): 1; (6)#H bond acceptors: 3; (7)#H bond donors: 1; (8)#Freely Rotating Bonds: 1; (9)Polar Surface Area: 39.19 ; (10)Index of Refraction: 1.59; (11)Molar Refractivity: 36.16 cm3; (12)Molar Volume: 107.1 cm3; (13)Polarizability: 14.33×10-24 cm3; (14)Surface Tension: 61 dyne/cm; (15)Density: 1.47 g/cm3; (16)Flash Point: 133.8 °C; (17)Enthalpy of Vaporization: 56.76 kJ/mol; (18)Boiling Point: 297.6 °C at 760 mmHg; (19)Vapour Pressure: 0.000599 mmHg at 25°C.

This is a kind of off-white solid, and it is usually used as a useful synthetic intermediate. Being among the irritant chemicals, it is irritant to the eyes, and it may cause inflammation to the skin or other mucous membranes. Besides, it is harmful if swallowed and it may also cause damage to health. So when you contact with this chemical, you should be very cautious and had better take the following instructions. If in case of contacting with eyes, rinse immediately with plenty of water and seek medical advice.

This kind of chemical is usually applied in BPC(bulk pharmaceutical chemicals) and the medical intermediates. As to its raw materials, there are various, including hydrochloric acid, ethyl acetate, sulfuric acid , toluene, sodium nitrite, potassium permanganate, zinc, 6-chloro-2-methyl-3-nitropyridine, 3-amino-2-picoline; While its product categories are pharmacetical; pyridine; aromatics; pyridines.

In addition, you could obtain the molecular structure by converting the following datas:
SMILES:Clc1cccnc1C(=O)O
InChI:InChI=1/C6H4ClNO2/c7-4-2-1-3-8-5(4)6(9)10/h1-3H,(H,9,10)
InChIKey:XTMUXJBJCMRWPG-UHFFFAOYAF