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5804-85-3

Basic Information
CAS No.: 5804-85-3
Name: DIETHYLALUMINUM CYANIDE SOLUTION
Molecular Structure:
Molecular Structure of 5804-85-3 (DIETHYLALUMINUM CYANIDE SOLUTION)
Formula: C5H10 Al N
Molecular Weight: 111.123
Synonyms: Aluminum,(cyano-C)diethyl-; Aluminum, cyanodiethyl- (7CI,8CI); Cyanodiethylalane;Cyanodiethylaluminum; Diethylaluminum cyanide
Density: g/cm3
Boiling Point: °Cat760mmHg
Flash Point: °C
Hazard Symbols: F,T+,N
Risk Codes: R11; R26/27/28; R32; R38; R48/20; R50/53; R63; R65; R67
Safety: 3587410
PSA: 23.79000
LogP: 2.03508
Synthetic route
5804-85-3

diethylaluminium cyanide

310435-48-4

(RS,2R)-(-)-N-[(tert-butyldimethylsilyl)oxy]-2-phenylacetylidene-p-toluenesulfinamide

310435-60-0

(RS,2S,3R)-(-)-N-(p-toluenesulfinyl)-2-amino-[(tert-butyldimethylsilyl)oxy]-3-phenylpropionitrile

Conditions
ConditionsYield
With isopropyl alcohol In tetrahydrofuran at -78 - 20℃; Addition;100%
5804-85-3

diethylaluminium cyanide

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

902472-98-4

tert-butyl 4-[benzyl(cyclopropylcarbonyl)amino]-4'-cyano-1,4'-bipiperidine-1'-carboxylate

Conditions
ConditionsYield
Stage #1: N-benzyl-N-piperidin-4-ylcyclopropanecarboxamide; N-tert-butyloxycarbonylpiperidin-4-one With titanium(IV) isopropylate In dichloromethane at 20℃; for 72h;
Stage #2: diethylaluminium cyanide In dichloromethane; toluene for 16h;
100%
306297-27-8

C13H20N2O

5804-85-3

diethylaluminium cyanide

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

C24H36N4O3

Conditions
ConditionsYield
Stage #1: C13H20N2O; N-tert-butyloxycarbonylpiperidin-4-one With titanium(IV) isopropylate at 25℃; for 24h;
Stage #2: diethylaluminium cyanide In toluene at 20℃; for 24h;
100%

rac-(4R,5S,6S)-1-benzyloxy-5,6-dihydroxy-5,6-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-azaspiro[3.5]non-8-ene-2,7-dione

5804-85-3

diethylaluminium cyanide

rac-(4R,5S,6S,8R)-1-benzyloxy-8-bromo-9-cyano-5,6-dihydroxy-5,6-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-azaspiro[3.5]nonane-2,7-dione

Conditions
ConditionsYield
Stage #1: rac-(4R,5S,6S)-1-benzyloxy-5,6-dihydroxy-5,6-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-azaspiro[3.5]non-8-ene-2,7-dione; diethylaluminium cyanide In tetrahydrofuran at 0 - 80℃; for 3h; Inert atmosphere;
Stage #2: With N-Bromosuccinimide In tetrahydrofuran at 0 - 20℃; for 0.25h; Product distribution / selectivity;
100%
5804-85-3

diethylaluminium cyanide

136233-98-2

(S)-2-((2S,3S)-3-Trimethylsilanyl-oxiranyl)-hexan-2-ol

137024-39-6

(E)-(S)-4-Hydroxy-4-methyl-oct-2-enenitrile

Conditions
ConditionsYield
In tetrahydrofuran for 2h; Heating;99%
5804-85-3

diethylaluminium cyanide

14618-80-5

(R)-benzyl glycidol

934623-81-1

(3R)-4-(benzyloxy)-3-hydroxybutanenitrile

Conditions
ConditionsYield
In toluene; benzene at 0 - 20℃;99%
5804-85-3

diethylaluminium cyanide

968-54-7

2,3-epoxy-17-methyl-androstan-17-ol

141691-37-4

(2R,3S,5S,8R,9S,10S,13S,14S,17S)-3,17-Dihydroxy-10,13,17-trimethyl-hexadecahydro-cyclopenta[a]phenanthrene-2-carbonitrile

Conditions
ConditionsYield
In toluene for 4h; Ambient temperature;98%
5804-85-3

diethylaluminium cyanide

98903-49-2, 98974-82-4, 106499-49-4

(1aβ,3α,3aα,6α,7aβ,7bβ)-3-<<(1,1-dimethylethyl)dimethylsilyl>oxy>octahydro-6-methyl-5H-oxireno<1>benzopyran-5-one

106455-96-3

(3R,4aR,5R,6R,8S,8aS)-8-(tert-Butyl-dimethyl-silanyloxy)-5-hydroxy-3-methyl-2-oxo-octahydro-chromene-6-carbonitrile

Conditions
ConditionsYield
In tetrahydrofuran; toluene for 3h; Ambient temperature;98%
16573-72-1

11-oxatricyclo<4.4.1.01,6>undeca-3,8-diene

5804-85-3

diethylaluminium cyanide

335201-94-0

trans-8a-hydroxy-1,4,4a,5,8,8a-hexahydronaphthalene-4a-carbonitrile

Conditions
ConditionsYield
In dichloromethane at 20℃;98%
5804-85-3

diethylaluminium cyanide

5877-56-5

(E)-N-benzylidene-2-methoxybenzenamine

60561-59-3

α-[(2-methoxyphenyl)amino]-benzeneacetonitrile

Conditions
ConditionsYield
With (R)-1,1'-Bi-2-naphthol In toluene at -78 - -40℃; for 3h;98%
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    DIETHYLALUMINUM CYANIDE SOLUTION Chemical Properties Boiling point 150 °C(Press: 0.07 Torr) density 0.87 g/mL at 20 °C Fp 45 °F BRN 3587410 Safety Information Hazard Codes F,T+,N Risk Statements 11-26/27/28-32-38-4

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