CAS No.5840-01-7,Lilolidine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	5840-01-7
Name:	Lilolidine
Article Data:	14

Formula:	C11H11 N
Molecular Weight:	157.215
Synonyms:	1,7-Trimethyleneindol;1,8-Trimethyleneindole; 5,6-Dihydro-4H-pyrrolo[3,2,1-ij]quinoline; Indole,1,7-(1,3-propanediyl)-; Lilolidene
EINECS:	691-285-6
Density:	1.16 g/cm³
Melting Point:	80-81°C
Boiling Point:	318.377 °C at 760 mmHg
Flash Point:	146.349 °C
Safety:	24/25
PSA:	4.93000
LogP:	2.58750

Synthetic route

: 124730-56-9
5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-1-carboxylic acid

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With quinoline; copper chromite at 185℃; for 3h;	93%
With quinoline; copper chromite at 185℃; for 2h;	72%
With copper chromite In quinoline at 185℃; for 2h;	72%
With quinoline; copper chromite at 185℃; for 4h;	58%
copper(II) chromite In quinoline at 185℃; for 4h;	58%

: 16078-37-8
5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
Stage #1: 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one With diisobutylaluminium hydride In tetrahydrofuran; toluene at -20 - -10℃; Stage #2: With hydrogenchloride In tetrahydrofuran; water; toluene at 40℃; for 0.5h; Temperature; Concentration; Reagent/catalyst;	88.9%

: 1220339-77-4
5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline 1,2-dicarboxylic acid

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
Stage #1: 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline 1,2-dicarboxylic acid With quinoline; copper at 238℃; for 3h; Stage #2: With hydrogenchloride In water Stage #3: With sodium hydroxide In water	72%

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 107-21-1
ethylene glycol

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With Pt/Al2O3; zinc(II) oxide In neat (no solvent) at 175℃; for 24h; Sealed tube;	50%

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 107-21-1
ethylene glycol

A: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

B: 52704-48-0
2-[1,2,3,4-tetrahydroquinolin-1-yl]ethan-1-ol

Conditions

Conditions	Yield
With palladium on activated charcoal; zinc(II) oxide In water at 150℃; for 24h; Sealed tube;	A 45% B 45%
With palladium on activated charcoal; zinc(II) oxide In water at 150℃; for 24h; Sealed tube;

...Expand

: 91-22-5
quinoline

: 107-21-1
ethylene glycol

A: 635-46-1
1,2,3,4-tetrahydroisoquinoline

B: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With palladium 10% on activated carbon; zinc In water at 150℃; for 24h; Autoclave;	A 37% B 16%
With palladium 10% on activated carbon; zinc In water at 150℃; for 40h; Autoclave;	A 33 %Spectr. B 33 %Spectr.
With palladium 10% on activated carbon; zinc In water at 150℃; for 70h; Autoclave;	A 45 %Spectr. B 50 %Spectr.

...Expand

: 117273-45-7
5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With quinoline; copper oxide-chromium oxide; hydrogen at 190℃;

: 1026530-18-6
[(E)-8-Allyl-3,4-dihydro-2H-quinolin-1-ylimino]-acetic acid

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With potassium hydroxide; sulfuric acid 1.) ethanol, 120 deg C, 4 h, 2.) ethanol, reflux, 4 h; Yield given. Multistep reaction;

: 2-[(E)-8-Allyl-3,4-dihydro-2H-quinolin-1-ylimino]-propionic acid ethyl ester

: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With pyridine; sulfuric acid; acetic anhydride 1.) ethanol, 3.5 h; Yield given. Multistep reaction;

: 194231-71-5
1-allyl-7-bromo-1H-indole

A: 16886-08-1
1-allylindole

B: 5840-01-7
5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In toluene for 12h; Heating; Yield given. Yields of byproduct given;
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In toluene for 12h; Product distribution; Heating; different N-substituted-7-bromoindoles;

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Chemistry

Molecule structure of Lilolidine (CAS NO.5840-01-7):

Molecular Weight: 157.2117 g/mol
Molecular Formula: C₁₁H₁₁N
Density: 1.166 g/cm³
Melting Point: 80-81°C
Boiling Point: 318.377 °C at 760 mmHg
Flash Point: 146.349 °C
Index of Refraction: 1.656
Molar Refractivity: 49.546 cm³
Molar Volume: 134.785 cm³
Polarizability: 19.641×10^-24 cm³
Surface Tension: 44.838 dyne/cm
Enthalpy of Vaporization: 53.758 kJ/mol
Vapour Pressure: 0.001 mmHg at 25 °C
InChI: InChI=1/C11H11N/c1-3-9-5-2-7-12-8-6-10(4-1)11(9)12/h1,3-4,6,8H,2,5,7H2 Copy
InChIKey: QCCKSFHMARIKSK-UHFFFAOYAA
Product Categories of Lilolidine (CAS NO.5840-01-7): Pale White Powder

Specification

Lilolidine (CAS NO.5840-01-7) is also named as 2,3-dihydro-1H-pyrrolo[3,2,1-ij]quinoline ; 5,6-dihydro-4h-pyrrolo[3,2,1-ij]quinoline ; 1,7-Trimethyleneindole .