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594-11-6

Basic Information
CAS No.: 594-11-6
Name: methylcyclopropane
Article Data: 72
Molecular Structure:
Molecular Structure of 594-11-6 (methylcyclopropane)
Formula: C4H8
Molecular Weight: 56.1075
Synonyms: Cyclopropylmethane;Methylcyclopropane
Density: 0.766g/cm3
Melting Point: -177.3°C
Boiling Point: 0.5°C at 760 mmHg
PSA: 0.00000
LogP: 1.41630
Synthetic route
14104-20-2

silver tetrafluoroborate

116840-62-1

C5H5(CO)2FeCH2CH2CH(CH3)Br

594-11-6

methylcyclopropane

Conditions
ConditionsYield
In benzene-d6 byproducts: AgBr; Addn. of a soln. of iron compound to a frozen suspn. of AgBF4 at liquid nitrogen temp., sealing NMR tube under high vac., warming to room temp. and shaking.; Not isolated, NMR, MS, GC.;70%
64-17-5

ethanol

106359-12-0

5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A

18387-24-1

5,5-dimethyl-5-sila-2-hexanol

B

594-11-6

methylcyclopropane

C

(3-Ethoxy-butyl)-trimethyl-silane

Conditions
ConditionsYield
With water Product distribution; Rate constant; Mechanism; competitive reaction; use (R)-(-)-enriched compound, add of LiClO4, KOH, KOBs, LiOBs;A 63%
B 20%
C 17%
87145-50-4

(η5-cyclopentadienyl)dicarbonylrhenacyclopentane

A

106-98-9

1-butylene

B

tricarbonylcyclopentadienylrhenium

C

594-11-6

methylcyclopropane

Conditions
ConditionsYield
In benzene-d6 thermolysis of Re-complex in benzene-d6 in sealed tube at 100°C; identified by (1)H NMR gas chromy.;A <1
B 50%
C 40%
75-89-8

2,2,2-trifluoroethanol

106359-12-0

5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A

18387-24-1

5,5-dimethyl-5-sila-2-hexanol

B

594-11-6

methylcyclopropane

C

Trimethyl-[3-(2,2,2-trifluoro-ethoxy)-butyl]-silane

Conditions
ConditionsYield
With water at 25℃; Rate constant; Product distribution; Mechanism; competitive reaction; use (R)-(-)-enriched compound, add of LiClO4, KOH, KOBs, LiOBs;A 26%
B 27%
C 47%

bis(pentamethylcyclopentadienyl)titanacyclopentane(CH2CH2)

A

74-85-1

ethene

B

3404-63-5

2-ethyl-1,3-butadiene

C

594-11-6

methylcyclopropane

D

106-99-0

buta-1,3-diene

Conditions
ConditionsYield
In neat (no solvent, solid phase) placing of Ti-compd. in a Schlenk tube, rapid heating up to 200°C under reduced pressure in an oil bath; condensing of products in a NMR tube, detected by (1)H NMR, GLC and MS;A 43%
B 16%
C 19%
D 31%

Cyclopropylmethyl-phosphonic acid isopropyl ester 2-thioxo-2H-pyridin-1-yl ester

A

106-98-9

1-butylene

B

594-11-6

methylcyclopropane

Conditions
ConditionsYield
With 2,2'-azobis(isobutyronitrile); 2-methylpropan-2-thiol In benzene Heating;A 3%
B 0.2%
2465-56-7

methylene

A

106-98-9

1-butylene

B

590-18-1

(Z)-2-Butene

C

624-64-6

trans-2-Butene

D

594-11-6

methylcyclopropane

Conditions
ConditionsYield
Produkt5: Isobutylen;
1190-22-3

1,3-dichlorobutane

594-11-6

methylcyclopropane

Conditions
ConditionsYield
With N-methyl-acetamide; zinc at 60 - 70℃;
107-80-2

1,3-dibromobutane

594-11-6

methylcyclopropane

Conditions
ConditionsYield
With copper In tetrahydrofuran at -70℃; for 0.166667h; further reaction with other α,ω-dihaloalkanes at other temperatures;97 % Chromat.
With ethanol; zinc
With propan-1-ol; water; zinc
2465-56-7

methylene

75-19-4

cyclopropane

A

106-98-9

1-butylene

B

590-18-1

(Z)-2-Butene

C

624-64-6

trans-2-Butene

D

594-11-6

methylcyclopropane

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