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Basic Information
| CAS No.: | 601-88-7 |
|---|---|
| Name: | 2,6-Dichloronitrobenzene |
| Article Data: | 16 |
| Molecular Structure: | |
|
|
|
| Formula: | C6H3 Cl2 N O2 |
| Molecular Weight: | 192.001 |
| Synonyms: | 1,3-Dichloro-2-nitrobenzene;2,6-Dichloro-1-nitrobenzene; 2,6-Dichloronitrobenzene |
| EINECS: | 210-009-3 |
| Density: | 1.533 g/cm3 |
| Melting Point: | 71 ºC |
| Boiling Point: | 130ºC |
| Flash Point: | 118.9 °C |
| Appearance: | Powder, alcohol-resistant foam, water spray, carbon dioxide. |
| Hazard Symbols: |
 T
|
| PSA: | 45.82000 |
| LogP: | 3.42480 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2,6-Dichloroaniline With sodium tungstate (VI) dihydrate; sulfuric acid In methanol at 40℃; Stage #2: With dihydrogen peroxide In methanol; water at 40℃; for 9h; pH=0.5; Stage #3: With potassium hydroxide In methanol; water at 20 - 40℃; for 2h; Reagent/catalyst; pH-value; Temperature; Solvent; | 92% |
| With sodium perborate In acetic acid at 50 - 55℃; | 87% |
| With sodium perborate In acetic acid at 50 - 60℃; for 2h; | 87% |
- 601-88-7
2,6-dichloronitrobenzene
Conditions
| Conditions | Yield |
|---|---|
| With sodium nitrite In ethyl acetate at 70℃; for 16h; Temperature; Solvent; Sealed tube; chemoselective reaction; | 91% |
- 59992-52-8
2,6-dichloro-4-aminonitrobenzene
- 601-88-7
2,6-dichloronitrobenzene
- 129825-24-7
2,4-dichloro-3-nitroaniline
- 601-88-7
2,6-dichloronitrobenzene
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid at 110℃; Kochen des Reaktionsgemisches mit NaNO2 in Aethanol; |
- 541-73-1
1,3-Dichlorobenzene
A
- 611-06-3
2,4-dichloronitrobenzene
B
- 618-62-2
3,5-dichloro-1-nitrobenzene
C
- 601-88-7
2,6-dichloronitrobenzene
Conditions
| Conditions | Yield |
|---|---|
| With Nitrogen dioxide; ozone In dichloromethane at 0 - 5℃; for 1h; Yield given; | |
| With Nitrogen dioxide; ozone In dichloromethane at 0 - 5℃; for 1h; Yield given. Yields of byproduct given; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With nitric acid Heating; |
- 7697-37-2
nitric acid
- 541-73-1
1,3-Dichlorobenzene
A
- 611-06-3
2,4-dichloronitrobenzene
B
- 601-88-7
2,6-dichloronitrobenzene
...Expand
- 31592-84-4
N-(3,5-dichlorophenyl)-acetamide
- 601-88-7
2,6-dichloronitrobenzene
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: nitric acid / die Acetanilide trennt man mit CS2 zersetzt man durch Erhitzen mit konz.Schwefelsaeure View Scheme | |
| Multi-step reaction with 2 steps 1: Nitrieren; mann trennt das Gemenge durch CS2, worin sich nur 3.5-Dichlor-2-nitro-acetanilid loest, und verseift durch Erhitzen mit konz.Schwefelsaeure View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: acetic acid; calcium hypochlorite / 40 - 60 °C View Scheme |
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2,6-Dichloronitrobenzene
Chemistry
The molecular formula of 2,6-Dichloronitrobenzene(601-88-7) is C6H3Cl2NO2 and its formula weight is 192.
The density of 2,6-Dichloronitrobenzene(601-88-7) is 1.533 g/cm3 and it has a melting point of 71 °C. The boiling point is 272.9 °C at 760 mmHg . The refractive index is about 1.595 . Its flash point is 118.9 °C .
The chemical synonyms of 2,6-Dichloronitrobenzene(601-88-7) are Benzene, 1,3-dichloro-2-nitro-;2,6-Dichloronitrobenezene;1,3-DICHLORO-3-NITROBENZENE;1,3-Dichloro-2-nitrobenzene;2,6-Dichloronitrobenzene;1-Nitro-2,6-dichlorobenzene
The molecular structure of 2,6-Dichloronitrobenzene(601-88-7):
The density of 2,6-Dichloronitrobenzene(601-88-7) is 1.533 g/cm3 and it has a melting point of 71 °C. The boiling point is 272.9 °C at 760 mmHg . The refractive index is about 1.595 . Its flash point is 118.9 °C .
The chemical synonyms of 2,6-Dichloronitrobenzene(601-88-7) are Benzene, 1,3-dichloro-2-nitro-;2,6-Dichloronitrobenezene;1,3-DICHLORO-3-NITROBENZENE;1,3-Dichloro-2-nitrobenzene;2,6-Dichloronitrobenzene;1-Nitro-2,6-dichlorobenzene
The molecular structure of 2,6-Dichloronitrobenzene(601-88-7):