Detail of > 614-97-1
- MSDS Download
- CAS Number:
- 614-97-1
- Name:
1H-Benzimidazole,6-methyl-
- Superlist Name:
- 5-Methylbenzimidazole
- Formula:
- C8H8 N2
- Molecular Structure:
- Synonyms:
- 1H-Benzimidazole,5-methyl- (9CI); Benzimidazole, 5(or 6)-methyl- (7CI); Benzimidazole, 5-methyl-(8CI); 5-Methyl-1H-benzimidazole; 5-Methylbenzimidazole; NSC 3826
- Molecular Weight:
- 132.18
- EINECS:
- 210-401-4
- Density:
- 1.186 g/cm3
- Melting Point:
- 114-117 °C(lit.)
- Boiling Point:
- 169-172 ºC (1 mmHg),363.2 °C at 760 mmHg
- Flash Point:
- 204 °C
- Solubility:
- 25 MG/ML, CHCL3; CLEAR TO VERY SLIGHTLY HAZY, COLORLESS TO BROWN SOLUTION
- Appearance:
- WHITE TO LIGHT BROWN POWDER, CRYSTALS OR CRYSTALLINE POWDER AND/OR CHUNKS
- Hazard Symbols:
- Risk Codes:
- R22
- Safety:
- 22-24/25-36Details
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Reference
- Development of methods for synthesizing alkyl esters of benzimidazolyl-2-carbamic acid
- Development of methods for synthesizing alkyl esters of benzimidazolyl-2-carbamic acid. Atakuziev, A. A.; Kadyrov, Ch. Sh.; Gofen, G. I. (Inst. Khim. Rast. Veshchestv, Tashkent, USSR). Uzb. Khim. Zh., (3), 32-5 (Russian) 1976. CODEN: UZKZAC. DOCUMENT TYPE: Journal CA Section: 28 (Heterocyclic Compounds (More Than One Hetero Atom)) Me 2-benzimidazolecarbamate (I, R = Me, R1 = R2 = R3 = H) was obtained in 60% yield by boiling thiourea with Me2SO4, cooling, adding ClCO2Me, adding base at -20.degree. to a pH 6-7, and boiling with o-(H2N)2C6H4; in 90% yield when PhCH2Cl was substituted for Me2SO4; and in 86% yield from Ca cyanamide ClCO2Me, and o-(H2N)2C6H4. Addnl. obtained were 50-87% I (R = Et, R1 = H, Me, Cl, R2 = H, Me, R3 = H, Me).Except for chemicals metioned above, 614-97-1 and 6306-71-4 are also used. .
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