CAS No.619-17-0,4-Nitroanthranilic acid Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	619-17-0
Name:	4-Nitroanthranilic acid
Article Data:	31

Formula:	C₇H₆N₂O₄
Molecular Weight:	182.136
Synonyms:	Anthranilicacid, 4-nitro- (6CI,7CI,8CI);2-Amino-4-nitrobenzoic acid;2-Carboxy-5-nitroaniline;4-Nitro-2-aminobenzoic acid;NSC 7789;
EINECS:	210-583-5
Density:	1.568 g/cm³
Melting Point:	257 °C (dec.)(lit.)
Boiling Point:	431.4 °C at 760 mmHg
Flash Point:	214.7 °C
Solubility:	<0.01 g/100 mL at 22 °C in water
Appearance:	Orange crystalline powder
Hazard Symbols:	Xi
Risk Codes:	36/37/38
Safety:	26-37/39
PSA:	109.14000
LogP:	1.97960

Synthetic route

: 87840-68-4
diethyl 2,4-dinitrobenzylidenemalonate

: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With diethylamine; tert-butyl alcohol for 48h; Ambient temperature;	75%
With sodium hydrogencarbonate; diethylamine; tert-butyl alcohol Mechanism; 1.) room temp., 48 h, 2.) chloroform;	75%

: 610-30-0
2,4-dinitrobenzoic acid

: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With ferrous(II) sulfate heptahydrate; ammonia In water at 50 - 60℃;	67%

: 99-60-5
2-chloro-4-nitrobenzoic acid

: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
Stage #1: 2-chloro-4-nitrobenzoic acid With copper(l) iodide; sodium azide; ethanol; caesium carbonate; N,N`-dimethylethylenediamine at 20 - 95℃; Inert atmosphere; Sealed tube; Stage #2: With hydrogenchloride In water pH=2 - 3;	62%

: 5466-84-2
4-nitrophthalic anhydride

A: 616-79-5
2-amino-5-nitro-benzoic acid

B: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With ammonium hydroxide Behandeln des entstandenen Gemisches mit alkal. Natriumhypochlorit-Loesung;

: 13138-53-9
4-nitrophthalic amide

A: 616-79-5
2-amino-5-nitro-benzoic acid

B: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With alkaline aqueous potassium hypobromite

: 951-97-3
2-acetamido-4-nitrobenzoic acid

: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With ethanol; sulfuric acid
With hydrogenchloride; ethanol
With hydrogenchloride
With hydrogenchloride In water for 1h; Reflux;

: 65911-47-9
4-nitro-2-carbamoylbenzoic acid

: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
With hydrogenchloride; potassium hydroxide; bromine 1.) heating, 1 h, 2.) 0 deg C; Yield given. Multistep reaction;
With sodium hypochlorite In water at 0 - 30℃; Temperature;

: 121-14-2
2,4-dinitrotoluene

: 71-43-2
benzene

A: 92-52-4
biphenyl

B: 109466-84-4
2-amino-4-nitrobenzaldehyde

C: 99-09-2
3-nitro-aniline

D: 619-17-0
4-Nitroanthranilic acid

Conditions

Conditions	Yield
at 343℃; Product distribution; Mechanism; thermolysis in supercritical benzene; other temperature, pressure;	A 100.0 (unit not given) B 35.8 (unit not given) C 20.0 (unit not given) D 22.5 (unit not given)

...Expand

: N-(2-methyl-7-nitro-4-oxo-4H-quinazolin-3-yl)-diacetamide

permanganate: permanganate

: 619-17-0
4-Nitroanthranilic acid

: 38527-51-4
7-nitro-2-phenyl-4H-benzo[d][1,3]oxazin-4-one

alkali: alkali

A: 65-85-0
benzoic acid

B: 619-17-0
4-Nitroanthranilic acid

...Expand

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Chemistry

Detail of 4-NITROANTHRANILIC ACID (619-17-0).
Molecular Structure:

Name:4-NITROANTHRANILIC ACID
CAS Number:619-17-0
Molecular Formula:C₇H₆N₂O₄
Molecular Weight:182.15
EINECS:210-583-5
Density:1.568 g/cm³
Melting Point:268-270 ^oC (dec.)
Boiling Point:431.4 ^oC at 760 mmHg
Flash Point:214.7 ^oC
Solubility:<0.01 g/100 mL at 22^oC in water
Appearance:right yellow powder
Properties:Orange prisms from EtOH (aq).
CAS DataBase Reference:619-17-0(CAS DataBase Reference)
EPA Substance Registry System:619-17-0(EPA Substance)
Synonyms of 4-NITROANTHRANILIC ACID (619-17-0):
P-NITROANTHRANILIC ACID;2-amino-4-nitro-benzoicaci;4-nitro-anthranilicaci;4-Nitro-2-aminobenzoic acid;4-NITROANTHRANILIC ACID;2-AMINO-4-NITROBENZOIC ACID;4-NITROANTHRANILIC ACID, TECH., 90%;4-NitroAnthranillicAcid

Toxicity Data With Reference

mmo-sat 10 µg/plate

ENMUDM Environmental Mutagenesis. 8 (Suppl 7)(1986),1.

Consensus Reports

NCI Carcinogenesis Bioassay (feed); No Evidence: mouse, rat NCITR* National Cancer Institute Carcinogenesis Technical Report Series. (Bethesda, MD 20014) No. NCI-CG-TR-109 ,1978. . Reported in EPA TSCA Inventory.

Safety Profile

Mutation data reported. When heated to decomposition it emits toxic fumes of NO_x. See also NITRO COMPOUNDS of AROMATIC HYDROCARBONS.
Safety Information of 4-NITROANTHRANILIC ACID (619-17-0).
Hazard Codes:Xi
Risk Statements:36/37/38
Safety Statements:26-37/39
WGK Germany:3
RTECS:CB3675000
Hazardous Substances Data:619-17-0(Hazardous Substances Data)