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CAS No.: | 620-20-2 |
---|---|
Name: | 3-Chlorobenzyl chloride |
Article Data: | 30 |
Molecular Structure: | |
Formula: | C7H6Cl2 |
Molecular Weight: | 161.031 |
Synonyms: | Toluene,m,a-dichloro- (8CI);1-Chloro-3-(chloromethyl)benzene;NSC 76577;m,a-Dichlorotoluene;m-Chlorobenzyl chloride;m-Chlorophenylmethyl chloride;a,3-Dichlorotoluene;a,m-Dichlorotoluene; |
EINECS: | 210-629-4 |
Density: | 1.247 g/cm3 |
Melting Point: | 69-71oC |
Boiling Point: | 213.7 °C at 760 mmHg |
Flash Point: | 98.9 °C |
Appearance: | Colorless to light yellow liquid |
Hazard Symbols: | C, N, Xn |
Risk Codes: | 34-51/53-43-36-20/21/22 |
Safety: | 26-36/37/39-45-61-14C |
Transport Information: | UN 2235 6.1/PG 3 |
PSA: | 0.00000 |
LogP: | 3.07880 |
Conditions | Yield |
---|---|
With dmap; triethylamine; p-toluenesulfonyl chloride In dichloromethane at 0 - 15℃; for 12.5h; | 31% |
With thionyl chloride | |
With phosphorus pentachloride at 100℃; | |
With thionyl chloride In pyridine Ambient temperature; |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium chloride; tetrabutyl-ammonium chloride In water at 20℃; Irradiation; Green chemistry; | 91% |
With N-chloro-succinimide; N-hydroxyphthalimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 80℃; for 3h; Sealed tube; Inert atmosphere; | 88% |
With N-hydroxyphthalimide; carbon tetrabromide; trichloroisocyanuric acid; copper(II) acetate monohydrate In dichloromethane at 25℃; for 40h; | 55% |
Conditions | Yield |
---|---|
With thionyl chloride; benzene |
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 110℃; |
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 25℃; Kinetics; |
B
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 110℃; |
B
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 110℃; entsteht analog aus Benzoyl-<2.4'-dichlor-dibenzylamin>; |
tetrachloromethane
(Z)-hepta-1,2,4-trien-6-yne
A
1-(2,2,2-trichloroethyl)-3-chlorobenzene
B
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
at 100℃; Product distribution; |
sulfuryl dichloride
meta-bromotoluene
dibenzoyl peroxide
A
meta-bromobenzyl bromide
B
1-Chloro-3-chloromethyl-benzene
C
3-bromobenzyl chloride
Conditions | Yield |
---|---|
at 110℃; |
1-(1-Chloro-2,2,2-trifluoro-ethyl)-3-methyl-benzene
C7H6Cl(1+)
B
1-Chloro-3-chloromethyl-benzene
Conditions | Yield |
---|---|
at 69.85℃; Thermodynamic data; chloride-transfer; |
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