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| CAS No.: | 623-33-6 |
|---|---|
| Name: | Glycine ethyl ester hydrochloride |
| Article Data: | 55 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H10ClNO2 |
| Molecular Weight: | 139.582 |
| Synonyms: | ethoxycarbonylmethylazanium;Glycine ethyl ester;Ethyl glycinate hydrochloride;Glycine hydrochloride ethyl ester;Ethyl aminoacetate hydrochloride;Ethyl glycinate;Glycine Ethylester Hydrochoride;H-Gly-OEt·HCl;Glycine Ethyl Ester HCl; |
| EINECS: | 210-787-4 |
| Density: | 1 g/cm3 |
| Melting Point: | 145-146 °C(lit.) |
| Boiling Point: | 109.5 °C at 760 mmHg |
| Solubility: | >1000 g/L (20 °C) in water |
| Appearance: | Crystalline |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 41 |
| Safety: | 26-39-24/25 |
| PSA: | 52.32000 |
| LogP: | 1.01050 |
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N,N-dibenzylglycine ethyl ester
- 623-33-6
glycine ethyl ester hydrochloride
| Conditions | Yield |
|---|---|
| With 1,1,2-trichloroethane; 10% palladium on activated carbon; hydrogen In methanol under 760.051 Torr; for 1h; chemoselective reaction; | 99% |
| Conditions | Yield |
|---|---|
| With thionyl chloride at 25 - 30℃; for 0.583333h; microwave irradiation; | 98% |
| With thionyl chloride Reflux; | 97% |
| With thionyl chloride at -10 - 20℃; for 2h; Heating / reflux; | 90.4% |
- 85231-98-7
C13H26NO7P
- 623-33-6
glycine ethyl ester hydrochloride
| Conditions | Yield |
|---|---|
| With hydrogenchloride In benzene Ambient temperature; | 91% |
| Conditions | Yield |
|---|---|
| With thionyl chloride In ethanol at -10℃; for 2h; Heating / reflux; | 90.4% |
| With thionyl chloride In ethanol for 2h; | 90.4% |
| Conditions | Yield |
|---|---|
| With thionyl chloride at -20℃; for 2h; Reflux; Inert atmosphere; | 90% |
| Conditions | Yield |
|---|---|
| at -5 - 60℃; for 4h; | 85% |
| Conditions | Yield |
|---|---|
| With triphenylphosphine In tetrahydrofuran; water for 12h; Ambient temperature; | 83% |
- 14011-27-9
ethyl chloronitroacetate
- 623-33-6
glycine ethyl ester hydrochloride
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In ethanol at 35 - 40℃; | 65.3% |
| Conditions | Yield |
|---|---|
| With ammonium formate; palladium on activated charcoal In methanol for 0.333333h; Ambient temperature; | 64% |
- 64-17-5
ethanol
- 80478-56-4
ethyl N-(2-diethoxyacetyl)glycinate
A
- 623-33-6
glycine ethyl ester hydrochloride
B
- 6065-82-3
Ethyl diethoxyacetate
| Conditions | Yield |
|---|---|
| With hydrogenchloride for 3h; Heating; | A 35% B 38% |
| With hydrogenchloride for 3h; Product distribution; Heating; | A 35% B 38% |
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Chemistry
Molecular Structure of Glycine ethyl ester hydrochloride (CAS NO.623-33-6):
.png)
IUPAC Name: ethyl 2-aminoacetate hydrochloride
Name : Glycine ethyl ester hydrochloride
Molecular Formula : C4H9NO2.HCl; C4H10ClNO2
Molecular Weight : 139.58
CAS Registry Number : 623-33-6
EINECS : 210-787-4
BRN: 3594034
H bond acceptors: 3
H bond donors: 2
Freely Rotating Bonds: 4
Polar Surface Area: 26.3 Å2
Storage temp: Store at RT
Melting point: 145-148 oC
Water solubility: >1000 g/L (20 oC)
Solubility: >1000 g/L (20 °C)
Sensitive: Hygroscopic
Enthalpy of Vaporization: 34.82 kJ/mol
Boiling Point: 109.5 °C at 760 mmHg
Vapour Pressure: 24.7 mmHg at 25°C
InChI
InChI=1/C4H9NO2.ClH/c1-2-7-4(6)3-5;/h2-3,5H2,1H3;1H
Smiles
C(OCC)(C[NH3+])=O.[ClH-]
Product Categories: Food and Feed Additive; Amino Acid Derivatives; Amino Acids; Glycine [Gly, G]; Amino Acids and Derivatives; Amino Acid Ethyl Esters; Amino Acids (C-Protected); Biochemistry; Amino hydrochloride
Toxicity Data With Reference
| 1. | ipr-mus LD50:750 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) AD277-689 . |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Moderately toxic by intraperitoneal route. When heated to decomposition it emits toxic vapors of NOx, HCl, and Cl−.
Hazard Codes: 
Xi
Risk Statements: 41
R41:Risk of serious damage to the eyes.
Safety Statements: 26-39-24/25
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S39:Wear eye / face protection.
S24/25:Avoid contact with skin and eyes.
WGK Germany: 3
RTECS: MC0525000
HS Code: 29224995
Specification
Glycine ethyl ester hydrochloride , with CAS number of 623-33-6, can be called Glycineethylesterhydrochlor ; Glycocollethylesterhydrochloride ; usafdo-10 ; H-gly-oet HCl ; Glycine ethyl ester ; Glycine ethyl ester HCl ; Glycine ethyl ester hydrochloride ; Glycine-oet HCl .
Glycine ethyl ester hydrochloride (CAS NO.623-33-6) is pesticide and pharmaceutical intermediates, also used in biochemical research. It has been prepared by the action of absolute alcohol and hydrogen chloride on glycine;from glycyl chloride and alcohol;by the action of ammonia or hexamethylenetetramine on chloroacetic acid, and subsequent hydrolysis with alcoholic hydrochloric acid; by the action of hydrogen chloride and alcohol onmethyleneaminoacetonitrile;and by the reduction of ethyl cyanoformate or the corresponding imido ester hydrochloride.