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| CAS No.: | 625-23-0 |
|---|---|
| Name: | 2-METHYL-2-HEXANOL |
| Article Data: | 54 |
| Molecular Structure: | |
|
|
|
| Formula: | C7H16 O |
| Molecular Weight: | 116.203 |
| Synonyms: | 1,1-Dimethyl-1-pentanol;2-Methyl-2-hexanol; 2-Methyl-2-hydroxyhexane; Butyldimethylcarbinol; NSC 21977 |
| Density: | 0.812 g/mL at 25 °C(lit.) |
| Melting Point: | -30.45°C (estimate) |
| Boiling Point: | 141-142 °C(lit.) |
| Flash Point: | 105 °F |
| Solubility: | 9.61g/L(25 oC) |
| Appearance: | CLEAR COLOURLESS TO LIGHT YELLOW LIQUID |
| Risk Codes: | R10 |
| PSA: | 20.23000 |
| LogP: | 1.94750 |
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- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
| Conditions | Yield |
|---|---|
| With heptanal; 1,2-bis-(diphenylphosphino)ethane In dichloromethane at 0℃; for 6h; | A 95% B 27% |
- 693-04-9
butyl magnesium bromide
- 99051-01-1
2,3,3-trimethyl-2-butyl peroxybenzoate
A
- 625-23-0
2-methylhexan-2-ol
B
- 1009-14-9
phenyl butyl ketone
C
- 1855-13-6
5-phenylnonan-5-ol
| Conditions | Yield |
|---|---|
| In diethyl ether at 0℃; for 2h; | A 14% B 2% C 9% D 86% |
| Conditions | Yield |
|---|---|
| With n-hexan-2-one In dichloromethane at -25℃; for 6h; | A 3% B 74% |
| With n-hexan-2-one; Methyltitantrichlorid,Triphenylphosphin In dichloromethane at -25℃; for 6h; Product distribution; other phosphane-complexes and reagents; | A 67% B 10% |
- 591-78-6
n-hexan-2-one
- 74-88-4
methyl iodide
A
- 625-23-0
2-methylhexan-2-ol
B
- 97795-56-7
5,6-Dimethyl-decane-5,6-diol
| Conditions | Yield |
|---|---|
| With Pr 1.) THF, 20 deg C, 2.) -20 deg C; | A 70% B 7% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-bromo-butane With magnesium In tetrahydrofuran Inert atmosphere; Schlenk technique; Stage #2: acetone In tetrahydrofuran at 0℃; Inert atmosphere; Schlenk technique; Stage #3: With hydrogenchloride; water In tetrahydrofuran at 0℃; Inert atmosphere; Schlenk technique; | 67% |
| With magnesium | 62% |
| (i) Mg, (ii) /BRN= 635680/; Multistep reaction; |
- 591-78-6
n-hexan-2-one
- 2747-38-8
methyltrichlorotitanium
A
- 625-23-0
2-methylhexan-2-ol
B
- 4128-31-8
rac-octan-2-ol
| Conditions | Yield |
|---|---|
| With heptanal; Methyltitantrichlorid,Triphenylphosphin In dichloromethane at -25℃; for 6h; Product distribution; other phosphane-complexes and reagents; | A 67% B 10% |
- 109-72-8, 29786-93-4
n-butyllithium
- 99051-01-1
2,3,3-trimethyl-2-butyl peroxybenzoate
A
- 625-23-0
2-methylhexan-2-ol
B
- 1009-14-9
phenyl butyl ketone
C
- 1855-13-6
5-phenylnonan-5-ol
| Conditions | Yield |
|---|---|
| In hexane at 0℃; for 2h; | A 30% B 36% C 26% D 22% |
- 109-72-8, 29786-93-4
n-butyllithium
- 99051-01-1
2,3,3-trimethyl-2-butyl peroxybenzoate
A
- 625-23-0
2-methylhexan-2-ol
B
- 594-83-2
2,3,3-trimethyl-2-butanol
C
- 1855-13-6
5-phenylnonan-5-ol
| Conditions | Yield |
|---|---|
| In hexane at 0℃; for 2h; | A 30% B 30% C 26% D 22% |
- 85371-47-7
β,β-dibromovinyl methyl ether
- 67-64-1
acetone
A
- 625-23-0
2-methylhexan-2-ol
B
- 36677-85-7
4-Methoxy-2-methylbut-3-yne-2-ol
C
- 85371-42-2
(E)-3-Bromo-4-methoxy-2-methyl-3-buten-2-ol
D
- 85371-43-3
(Z)-3-Bromo-4-methoxy-2-methyl-3-buten-2-ol
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran at -80℃; | A n/a B 15% C n/a D n/a |
| Conditions | Yield |
|---|---|
| With diethyl ether |
- Total:26 Page 1 of 1 1
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