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6292-59-7

Basic Information
CAS No.: 6292-59-7
Name: 4-tert-Butylbenzenesulfonamide
Article Data: 17
Molecular Structure:
Molecular Structure of 6292-59-7 (4-tert-Butylbenzenesulfonamide)
Formula: C10H15NO2S
Molecular Weight: 213.301
Synonyms: Benzenesulfonamide,p-tert-butyl- (6CI,8CI);4-(1,1-Dimethylethyl)benzenesulfonamide;NSC 9911;p-(tert-Butyl)phenylsulfonamide;p-tert-Butylbenzenesulfonamide;
EINECS: 613-109-9
Density: 1.152 g/cm3
Melting Point: 136-138 °C
Boiling Point: 337.2 °C at 760 mmHg
Flash Point: 157.7 °C
Appearance: white solid
Hazard Symbols: IrritantXi
Risk Codes: 20/21/22
Safety: 22-36/37/39
PSA: 68.54000
LogP: 3.41260
Synthetic route
15084-51-2

4-tert-butylbenzenesulfonyl chloride

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With ammonium hydroxide for 72h; Ambient temperature;99%
With ammonium hydroxide In ethyl acetate at 20℃; for 1h;95%
With ammonium hydroxide In acetone at 20℃;94%

4,N-di-tert-butyl-benzenesulfonamide

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With scandium tris(trifluoromethanesulfonate) In nitromethane at 50℃; for 5h;96%
5636-16-8

4-tert-Butyl-N-isopropyl-benzenesulfonamide

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With chromium(III) acetate hydroxide; periodic acid In acetonitrile at 20℃; for 14h;94%
52436-75-6

(4-tert-butylphenyl)diazonium tetrafluoroborate

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine In water; acetonitrile at 80℃; for 12h; Inert atmosphere;84%
With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine In water; acetonitrile at 80℃; for 12h; Inert atmosphere; Schlenk technique;84%

4-(tert-butyl)-N,N-diethylbenzenesulfonamide

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With chromium(III) acetate hydroxide; periodic acid In acetonitrile at 20℃; for 16h;81%
2396-68-1

4-t-butylbenzenethiol

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; ammonium carbamate In methanol at 25℃; for 24h; Inert atmosphere; chemoselective reaction;80%

potassium tert-butyltrifluoroboranuide

701-34-8

4-bromo-benzenesulfonic acid amide

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; nickel(II) bis(2,2,6,6-tetramethylheptane-3,5-dionate); Ir(dF(CF3)ppy)2(bpy)PF6; zinc dibromide In N,N-dimethyl acetamide at 27℃; for 72h; Inert atmosphere; Irradiation;44%
1-tert-butyl-benzene-sulfonyl chloride-(4)

1-tert-butyl-benzene-sulfonyl chloride-(4)

ammonium carbonate

ammonium carbonate

6292-59-7

4-tert-butylbenzenesulphonamide

253185-03-4, 253185-04-5

tert-butylbenzene

6292-59-7

4-tert-butylbenzenesulphonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 6 h / Reflux
2: ethanol / 1 h / 0 °C
View Scheme
6292-59-7

4-tert-butylbenzenesulphonamide

150728-13-5

4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine

150727-06-3

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

Conditions
ConditionsYield
Stage #1: 4-tert-butylbenzenesulphonamide; 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine With potassium carbonate In acetonitrile at 25 - 83℃; Large scale reaction;
Stage #2: Large scale reaction;
100%
With potassium carbonate In dimethyl sulfoxide at 100 - 105℃;100%
Stage #1: 4-tert-butylbenzenesulphonamide With potassium carbonate In toluene at 50℃; for 0.5h; Large scale;
Stage #2: 4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine With tetrabutylammomium bromide In toluene at 110℃; for 10h; Large scale;
97%
Raw Materials
15084-51-2
Downstream Products
150727-06-3
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    4-tert-Butylbenzenesulfonamide Basic information Product Name: 4-tert-Butylbenzenesulfonamide Synonyms: BUTTPARK 44\03-78;4-TERT-BUTYLBENZENESULFONAMIDE;4-TERT-BUTYLBENZENESULPHONAMIDE;4-(TERT-BUTYL)BENZENE-1-SULFONAMIDE;P-TERT-BUTYL-BENZENESU

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Chemistry

Molecular Structure:

Molecular Formula: C10H15NO2S
Molecular Weight: 213.2966
IUPAC Name: 4-tert-Butylbenzenesulfonamide
Synonyms of 4-tert-Butylbenzenesulfonamide (CAS NO.6292-59-7): Buttpark 44\03-78 ; 4-(tert-Butyl)benzene-1-sulfonamide ; p-tert-Butyl-benzenesulfonamide ; TertiaryButylBenzeneSulphonamide ; 4-(1,1-Dimethylethyl)benzenesulfonamide
CAS NO: 6292-59-7
Melting point: 136-138 ° C 
Index of Refraction: 1.536
Molar Refractivity: 57.71 cm3
Molar Volume: 185 cm3
Surface Tension: 40.8 dyne/cm
Density: 1.152 g/cm3
Flash Point: 157.7 °C
Enthalpy of Vaporization: 58.04 kJ/mol
Boiling Point: 337.2 °C at 760 mmHg
Vapour Pressure: 0.000107 mmHg at 25°C

 

Uses

 4-tert-Butylbenzenesulfonamide (CAS NO.6292-59-7) is used as an intermediate for bosentan.

Safety Profile

Safety Information of 4-tert-Butylbenzenesulfonamide (CAS NO.6292-59-7):
Hazard Codes:Xi
Risk Statements:20/21/22
20/21/22:Harmful by inhalation, in contact with skin and if swallowed
Safety Statements:22-36/37/39
22:Do not breathe dust
36/37/39:Wear suitable protective clothing, gloves and eye/face protection
Hazard Note:Irritant