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637-64-9

Basic Information
CAS No.: 637-64-9
Name: TETRAHYDROFURFURYL ACETATE
Article Data: 28
Molecular Structure:
Molecular Structure of 637-64-9 (TETRAHYDROFURFURYL ACETATE)
Formula: C7H12O3
Molecular Weight: 144.17
Synonyms: 2-Furanmethanol,tetrahydro-, acetate (9CI);Furfuryl alcohol, tetrahydro-, acetate(6CI,7CI,8CI);2-(Acetoxymethyl)oxolane;2-(Acetoxymethyl)tetrahydrofuran;NSC4872;Tetrahydrofurfuryl acetate;
EINECS: 211-296-8
Density: 1.061 g/mL at 25 °C(lit.)
Boiling Point: 194-195 °C753 mm Hg(lit.)
Flash Point: 184 °F
Solubility: Soluble in water, ether, chloroform
PSA: 35.53000
LogP: 0.72850
Synthetic route
97-99-4

Tetrahydrofurfuryl alcohol

108-24-7

acetic anhydride

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With phosphoric acid In acetonitrile at 50℃; for 3h;99%
With zirconium sulfophenyl phosphonate In dichloromethane at 20℃; for 3h; Acetylation;97%
With aluminum triflate at 20℃; for 0.00555556h;96%
821-09-0

n-Pent-4-enyl alcohol

64-19-7

acetic acid

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With dihydrogen peroxide; potassium iodide at 20℃; for 4h;87%
97-99-4

Tetrahydrofurfuryl alcohol

75-36-5

acetyl chloride

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With pyridine In chloroform for 2h; Ambient temperature;86%
durch Veresterung;
97-99-4

Tetrahydrofurfuryl alcohol

64-19-7

acetic acid

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With iron(III) chloride at 20℃; for 9h; Esterification;85%
With sulfuric acid durch Veresterung;
With hydrogenchloride durch Veresterung;
With molecular sieve at 120℃; for 8h;
141-78-6

ethyl acetate

161617-56-7

2-Methoxymethoxymethyl-tetrahydro-furan

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With indium (III) iodide for 16h; Heating;85%
710-14-5

tetrahydrofurfuryl tetrahydropyranyl ether

75-36-5

acetyl chloride

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With sodium iodide In acetonitrile for 6h; Ambient temperature;84%
821-09-0

n-Pent-4-enyl alcohol

2570-63-0

thallium(III) triacetate

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
In benzene Ambient temperature;83%
In benzene Mechanism; Heating; intramolecular cyclization of other unsaturated alcohols;83%
97-99-4

Tetrahydrofurfuryl alcohol

127-19-5

N,N-dimethyl acetamide

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With cerium(IV) oxide at 155℃; for 36h; Inert atmosphere; Sealed tube;82%
821-09-0

n-Pent-4-enyl alcohol

2570-63-0

thallium(III) triacetate

A

3265-65-4

tetrahydro-2H-pyran-3-yl acetic acid

B

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
In acetic acid at 60℃; for 0.333333h;A 32%
B 30%
In acetic acid at 60℃; for 0.333333h; Mechanism; intramolecular cyclization of other unsaturated alcohols;A 32%
B 30%
97-99-4

Tetrahydrofurfuryl alcohol

127-09-3

sodium acetate

637-64-9

tetrahydrofurfuryl acetate

Conditions
ConditionsYield
With acetic acid; benzene
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Specification

The 2-Furanmethanol,tetrahydro-, 2-acetate, with the CAS registry number 637-64-9, is also known as 2-(Acetoxymethyl)tetrahydrofuran. It belongs to the product category of Ester Flavor. Its EINECS registry number is 211-296-8. This chemical's molecular formula is C7H12O3 and molecular weight is 144.16838. Its IUPAC name is called oxolan-2-ylmethyl acetate. The product should be sealed and stored in cool and dry place. What's more, it should be protected from strong oxides.

Physical properties of 2-Furanmethanol,tetrahydro-, 2-acetate: (1)ACD/LogP: 0.16; (2)ACD/LogD (pH 5.5): 0.16; (3)ACD/LogD (pH 7.4): 0.16; (4)#H bond acceptors: 3; (5)#Freely Rotating Bonds: 3; (6)Index of Refraction: 1.434; (7)Molar Refractivity: 35.78 cm3; (8)Molar Volume: 137.3 cm3; (9)Surface Tension: 34.7 dyne/cm; (10)Density: 1.049 g/cm3; (11)Flash Point: 84.4 °C; (12)Enthalpy of Vaporization: 44.17 kJ/mol; (13)Boiling Point: 205.5 °C at 760 mmHg; (14)Vapour Pressure: 0.249 mmHg at 25°C.

Preparation: this chemical can be prepared by Tetrahydrofurfuryl alcohol and acetic anhydride. This reaction will need inorganic acid.

Uses of 2-Furanmethanol,tetrahydro-, 2-acetate: it can be used to produce Essigsaeure-2,5-dibrom-pentyl-ester by heating. This reaction will need reagent bromotrimethylsilane with reaction time of 48 hours. The yield is about 87%.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: CC(=O)OCC1CCCO1
(2)InChI: InChI=1S/C7H12O3/c1-6(8)10-5-7-3-2-4-9-7/h7H,2-5H2,1H3
(3)InChIKey: AAQDYYFAFXGBFZ-UHFFFAOYSA-N