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63971-25-5

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Basic Information
CAS No.: 63971-25-5
Name: 3-AMINO-5,7-DIMETHYLADAMANTAN-1-OL Hydrochloride
Article Data: 3
Molecular Structure:
Molecular Structure of 63971-25-5 (3-AMINO-5,7-DIMETHYLADAMANTAN-1-OL Hydrochloride)
Formula: C12H21NO
Molecular Weight: 195.305
Synonyms: 1-Amino-3,5-dimethyl-7-hydroxyadamantane;1-AMINO-7-HYDROXY-3,5-DIMETHYLADAMANTANE;3-Amino-5,7-dimethyl-adamantan-1-ol;
Density: 1.197 g/cm3
Boiling Point: 269.4 °C at 760 mmHg
Flash Point: 116.8 °C
PSA: 46.25000
LogP: 2.50930
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Synthetic route
19982-07-1

1-acetamido-3,5-dimethyladamantane

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N-(3-hydroxy-5,7-dimethyladamantan-1-yl)acetamide

B

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1,3-dihydroxy-5,7-dimethyladamantane

C

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
Stage #1: 1-acetamido-3,5-dimethyladamantane With nitric acid
Stage #2: With acetic acid; urea In water		A 17%
B 9%
C n/a
...Expand

C22H38N2O5

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloromethane / 1 h / 20 °C
2: hydrogen / methanol / 12 h
View Scheme

C12H22N2O*C2HF3O2

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
With hydrogen In methanol for 12h;
707-37-9

1,3-dimethyl-5-adamantanol

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: tetrabutyl-ammonium chloride; methanol; cerium(III) chloride / acetonitrile / 16 h / 20 °C / Irradiation; Inert atmosphere; Sealed tube
2: dichloromethane / 1 h / 20 °C
3: hydrogen / methanol / 12 h
View Scheme
41100-52-1

memantine hydrochloride

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
With sulfuric acid; nitric acid at 20℃; for 39h; Cooling with ice;4.4 g
19982-07-1

1-acetamido-3,5-dimethyladamantane

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: potassium hydroxide; butan-1-ol / 130 °C
1.2: pH 8 - 9
2.1: sulfuric acid; nitric acid / 39 h / 20 °C / Cooling with ice
View Scheme
941-37-7

3,5-dimethyl-1-bromoadamantane

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 8 h / 130 °C
2.1: potassium hydroxide; butan-1-ol / 130 °C
2.2: pH 8 - 9
3.1: sulfuric acid; nitric acid / 39 h / 20 °C / Cooling with ice
View Scheme
63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

89139-48-0

3-(3-oxobenzo[d]isothiazol-2(3H)-yl)propanoic acid

N-(3-hydroxy-5,7-dimethyladamantan-1-yl)-3-(3-oxobenzo[d]isothiazol-2(3H)-yl)propanamide

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 70h; Inert atmosphere;36%

3-(4-fluoro-3-oxobenzo[d]isothiazol-2(3H)-yl)propanoic acid

63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

N-(3-hydroxy-5,7-dimethyladamantan-1-yl)-3-(4-fluoro-3-oxobenzo[d]isothiazol-2(3H)-yl)propanamide

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 70h; Inert atmosphere;25%
63971-25-5

3-amino-5,7-dimethyladamantan-1-ol

82152-06-5

2-(3-Oxo-3h-benzo[d]isothiazol-2-yl)-acetic acid

N-(3-hydroxy-5,7-dimethyladamantan-1-yl)-2-(3-oxobenzo[d]isothiazol-2(3H)-yl)acetamide

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 70h; Inert atmosphere;17%
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 70h;17%
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Chemistry

Product Name: 1-Amino-7-hydroxy-3,5-dimethyladamantane (CAS NO.63971-25-5)

Molecular Formula: C12H21NO
Molecular Weight: 195.30g/mol
Mol File: 63971-25-5.mol
Boiling point: 269.4 °C at 760 mmHg
Flash Point: 116.8 °C
Density: 1.197 g/cm3
Index of Refraction: 1.608 
Molar Refractivity: 56.38 cm3 
Molar Volume: 163 cm3 
Surface Tension: 66.4 dyne/cm
Enthalpy of Vaporization: 58.94 kJ/mol 
Vapour Pressure: 0.000964 mmHg at 25°C
Product Categories: Adamantane derivatives

Specification

 1-Amino-7-hydroxy-3,5-dimethyladamantane , its CAS NO. is 63971-25-5 , the synonyms are 1-Hydroxy-3-amino-5,7-dimethyladamantane ; 2,1-Hydroxy-3-amino-5,7-dimethyladamantane .