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67827-72-9

Basic Information
CAS No.: 67827-72-9
Name: 2-Methoxy-5-nitroaniline hydrochloride
Molecular Structure:
Molecular Structure of 67827-72-9 (2-Methoxy-5-nitroaniline hydrochloride)
Formula: C7H8N2O3.HCl
Molecular Weight: 204.613
Synonyms: Benzenamine,2-methoxy-5-nitro-, monohydrochloride (9CI);o-Anisidine, 5-nitro-,hydrochloride (5CI);2-Methoxy-5-nitroaniline hydrochloride;
EINECS: 267-234-5
Density: 1.318[at 20℃]
Melting Point: 119-123 °C
Boiling Point: 351.8 °C at 760 mmHg
Flash Point: 166.6 °C
Solubility: 297g/L at 25℃
Hazard Symbols: N,T
Risk Codes: R50/53; R23/24/25
PSA: 81.07000
LogP: 3.09200
Synthetic route
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

108-24-7

acetic anhydride

33721-54-9

N-(2-methoxy-5-nitrophenyl)acetamide

Conditions
ConditionsYield
at 80℃; for 8h;93.48%
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

99-59-2

3-amino-4-methoxynitrobenzene

Conditions
ConditionsYield
With sodium hydroxide In water pH=8;83.7%
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

C9H9IN2O4

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 8 h / 80 °C
2: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3: potassium iodide / N,N-dimethyl-formamide / 8 h / 120 °C
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

acetic acid-(2,3-dimethoxy-5-nitro-anilide)

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: potassium iodide / N,N-dimethyl-formamide / 8 h / 120 °C
4.1: copper(l) iodide / methanol; 1,4-dioxane / 12 h / 90 °C
4.2: 4 h / 80 °C
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

C9H11BrN2O2

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 8 h / 80 °C
2: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3: iron; acetic acid / 6 h / 75 - 80 °C
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

C15H16BrNO4

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: iron; acetic acid / 6 h / 75 - 80 °C
4.1: hydrogenchloride / water / 1 h / -25 °C
4.2: 0.25 h / -10 °C
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

C13H14BrNO3

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: iron; acetic acid / 6 h / 75 - 80 °C
4.1: hydrogenchloride / water / 1 h / -25 °C
4.2: 0.25 h / -10 °C
5.1: hydrogenchloride / water; ethanol / 8 h / Reflux
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

triethyl 4-bromo-5-methoxy-1H-pyrrolo(2,3-f)quinoline-2,7,9-tricarboxylate

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: iron; acetic acid / 6 h / 75 - 80 °C
4.1: hydrogenchloride / water / 1 h / -25 °C
4.2: 0.25 h / -10 °C
5.1: hydrogenchloride / water; ethanol / 8 h / Reflux
6.1: dichloromethane / 24 h / 20 °C
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

81770-66-3

4,5-dimethoxy-1H-pyrrolo<2,3-f>quinoline-2,7,9-tricarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: iron; acetic acid / 6 h / 75 - 80 °C
4.1: hydrogenchloride / water / 1 h / -25 °C
4.2: 0.25 h / -10 °C
5.1: hydrogenchloride / water; ethanol / 8 h / Reflux
6.1: dichloromethane / 24 h / 20 °C
7.1: copper(l) iodide / methanol; 1,4-dioxane / 8 h / Reflux
View Scheme
67827-72-9

2-methoxy-5-nitroaniline hydrochloride

triethyl 4-ethoxy-5-methoxy-1H-pyrrolo(2,3-f)quinoline-2,7,9-tricarboxylate

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: 8 h / 80 °C
2.1: methanesulfonic acid; N-Bromosuccinimide / 12 h / 25 °C / Cooling with ice
3.1: iron; acetic acid / 6 h / 75 - 80 °C
4.1: hydrogenchloride / water / 1 h / -25 °C
4.2: 0.25 h / -10 °C
5.1: hydrogenchloride / water; ethanol / 8 h / Reflux
6.1: dichloromethane / 24 h / 20 °C
7.1: copper(l) iodide / 1,4-dioxane / 8 h / Reflux
View Scheme
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    Prime Molecular Co., Ltd. is an advanced chemical intermediates manufacture with ?two R&D centers and two production sites in China, all well-equipped with dedicated and profession

  • PRIME MOLECULAR CO.,LIMITED

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  • 2-Methoxy-5-nitroaniline hydrochloride

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    67827-72-9

    2-Methoxy-5-nitroaniline hydrochloride

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    High quality Products with prompt delivery Package:based on customer requirement Application:organic intermediates Transportation:By air or By sea Port:any port of China

    Wuhan Chemwish Technology Co., Ltd is one of China's leading chemical corporations, which can offer customers for more than 50,000 pharmaceutical intermediates. We have a dedicated

  • Wuhan Chemwish Technology Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-27-67849912

    Address:Room 1311, Unit 2, Block1, Innovation Road East Lake High-tech Development Zone Wuhan, Hubei,P.R. China

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  • 2-methoxy-5-nitroanilinium chloride

  • Casno:

    67827-72-9

    2-methoxy-5-nitroanilinium chloride

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    CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio

    CFTC PharmaChem is a service based company in China, a pharmachem division of Changzhou Foreign Trade Corp.,supplying raw materials, intermediates, APIs and fine chemicals for the

  • Changzhou Foreign Trade Corp

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    Business Type:Trading Company

    Tel:+86-519-86623222

    Address:29F/D, 99 Yanling West Road, Changzhou, Jiangsu, China

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  • 2-Methoxy-5-Nitroaniline Hydrochloride

  • Casno:

    67827-72-9

    2-Methoxy-5-Nitroaniline Hydrochloride

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    high purity Application:Drug intermediates Materials intermediates and active molecules

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

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    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

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  • 2-Methoxy-5-nitroaniline hydrochloride

  • Casno:

    67827-72-9

    2-Methoxy-5-nitroaniline hydrochloride

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Jay Chemicals was established in 1988 by a group of technocrats from the prestigious Indian Institute of Technology (IIT), Mumbai, to manufacture quality Fine Organic Intermediate

  • Jay Chemicals

    India  |  Contact Details

    Business Type:Trading Company

    Tel:91-22-2511 9081, 25167253

    Address:504-Damji Shamji Trade Centre, Station Road, Vidhyavihar (West) Mumbai 400 086. India.

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Specification

The 2-Methoxy-5-nitroaniline hydrochloride, with the cas registry number 67827-72-9 and EINECS registry number 267-234-5, is also called 2-Methoxy-5-nitroanilinium chloride. And the molecular formula of the chemical is C7H8N2O3.HCl.

The characteristics of this chemical are as followings: (1)ACD/LogP: 1.69; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 1.69; (4)ACD/LogD (pH 7.4): 1.69; (5)ACD/BCF (pH 5.5): 11.37; (6)ACD/BCF (pH 7.4): 11.38; (7)ACD/KOC (pH 5.5): 198.3; (8)ACD/KOC (pH 7.4): 198.47; (9)#H bond acceptors: 5; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 3; (12)Polar Surface Area: 58.29 Å2; (13)Flash Point: 166.6 °C; (14)Enthalpy of Vaporization: 59.65 kJ/mol; (15)Boiling Point: 351.8 °C at 760 mmHg; (16)Vapour Pressure: 4.01E-05 mmHg at 25°C.

Addtionally, the following datas could be converted into the molecular structure:
(1)SMILES: Cl.[O-][N+](=O)c1ccc(OC)c(N)c1
(2)InChI: InChI=1/C7H8N2O3.ClH/c1-12-7-3-2-5(9(10)11)4-6(7)8;/h2-4H,8H2,1H3;1H
(3)InChIKey: JBBNYKPRONOPHN-UHFFFAOYAJ