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6870-94-6

Basic Information
CAS No.: 6870-94-6
Name: Pregna-1,4-diene-3,20-dione,11,17-dihydroxy-6-methyl-, (6a,11b)-
Article Data: 4
Molecular Structure:
Molecular Structure of 6870-94-6 (Pregna-1,4-diene-3,20-dione,11,17-dihydroxy-6-methyl-, (6a,11b)-)
Formula: C22H30 O4
Molecular Weight: 358.478
Synonyms: Pregna-1,4-diene-3,20-dione,11b,17-dihydroxy-6a-methyl- (6CI,7CI,8CI); 11b,17a-Dihydroxy-6a-methylpregna-1,4-diene-3,20-dione; NSC 125051
Density: 1.21g/cm3
Melting Point: 222-231℃
Boiling Point: 530.3°C at 760 mmHg
Flash Point: 288.6°C
PSA: 74.60000
LogP: 2.83120
Synthetic route
83-43-2

Methylprednisolone

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
ueber mehrere Stufen;
53-36-1

methylprednisolone acetate

A

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

B

61919-52-6

11β-hydroxy-6α-methyl-1,4-androstadiene-3,17-dione

C

6α-methylprednisone acetate

Conditions
ConditionsYield
Product distribution; Rate constant; Irradiation; radiolytic degradation;

C26H42O6

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid / tetrahydrofuran / pH 2 - 3
2: D-glucose; potassium dihydrogenphosphate / water; methanol / 50 h
View Scheme
7055-53-0

11β,17-dihydroxy-6α-methyl-pregn-4-ene-3,20-dione

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
With potassium dihydrogenphosphate; D-glucose In methanol; water for 50h;
1882-82-2

17-hydroxy-pregn-4-ene-3,11,20-trione

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: trimethyloxosulfonium bromide; orthoformic acid triethyl ester / 5 h
2: sodium tetrahydroborate / tetrahydrofuran / 12 h
3: phthalic anhydride; dihydrogen peroxide / ethyl acetate / 6 h
4: magnesium / tetrahydrofuran / 4 h
5: sulfuric acid / tetrahydrofuran / pH 2 - 3
6: D-glucose; potassium dihydrogenphosphate / water; methanol / 50 h
View Scheme
74332-34-6

3,3;20,20-bis-ethanediyldioxy-17-hydroxy-pregn-5-en-11-one

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / tetrahydrofuran / 12 h
2: phthalic anhydride; dihydrogen peroxide / ethyl acetate / 6 h
3: magnesium / tetrahydrofuran / 4 h
4: sulfuric acid / tetrahydrofuran / pH 2 - 3
5: D-glucose; potassium dihydrogenphosphate / water; methanol / 50 h
View Scheme
41870-77-3

3,3;20,20-bis-ethanediyldioxy-pregn-5-ene-11β,17-diol

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: phthalic anhydride; dihydrogen peroxide / ethyl acetate / 6 h
2: magnesium / tetrahydrofuran / 4 h
3: sulfuric acid / tetrahydrofuran / pH 2 - 3
4: D-glucose; potassium dihydrogenphosphate / water; methanol / 50 h
View Scheme

C25H38O7

6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: magnesium / tetrahydrofuran / 4 h
2: sulfuric acid / tetrahydrofuran / pH 2 - 3
3: D-glucose; potassium dihydrogenphosphate / water; methanol / 50 h
View Scheme
6870-94-6

11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione

64-19-7

acetic acid

53-36-1

methylprednisolone acetate

Conditions
ConditionsYield
Stage #1: 11β,17α-dihydroxy-6α-methyl-1,4-pregnadiene-3,20-dione With iodine; calcium oxide In methanol; dichloromethane
Stage #2: acetic acid With potassium acetate In acetone at 45 - 50℃; for 2h;
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  • Pregna-1,4-diene-3,20-dione,11,17-dihydroxy-6-methyl-, (6a,11b)- cas  6870-94-6

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    Pregna-1,4-diene-3,20-dione,11,17-dihydroxy-6-methyl-, (6a,11b)- cas 6870-94-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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    Business Type:Trading Company

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