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69045-84-7

Basic Information
CAS No.: 69045-84-7
Name: 2,3-Dichloro-5-(trifluoromethyl)pyridine
Article Data: 22
Molecular Structure:
Molecular Structure of 69045-84-7 (2,3-Dichloro-5-(trifluoromethyl)pyridine)
Formula: C6H2Cl2F3N
Molecular Weight: 215.99
Synonyms: 2,3-Dichloro-5-(trifluoromethyl)pyridine;5,6-Dichloro-3-(trifluoromethyl)pyridine;2,3-Dichloro-5-trifluoromethylpyridine;Pyridine,2,3-dichloro-5-(trifluoromethyl)-;
EINECS: 410-340-5
Density: 1.542 g/cm3
Melting Point: 8-9 °C
Boiling Point: 188.5 °C at 760 mmHg
Flash Point: 79.4 °C
Appearance: Light yellow liquid
Hazard Symbols: HarmfulXn, DangerousN, IrritantXi
Risk Codes: 20/22-41-43-51/53-36/37/38
Safety: 24-26-37/39-61
Transport Information: UN 3082 9/PG 3
PSA: 12.89000
LogP: 3.40720
Synthetic route
69045-83-6

2,3-dichloro-5-(trichloromethyl)pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
With hydrogen fluoride; tungsten(VI) chloride at 170 - 180℃; under 1500.15 Torr; for 5h; Reagent/catalyst; Temperature; Pressure; Autoclave;92%
With antimony(III) fluoride for 0.166667h; Heating; Irradiation;80.4%
With pyridine; iron(III) chloride; hydrogen fluoride at 130 - 175℃; Autoclave;73%
82107-24-2

2,2-dichloro-3,3,3-trifluoro-propionaldehyde

107-13-1

acrylonitrile

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
copper(l) chloride In acetonitrile at 190℃; for 0.5h;60%
7783-56-4

antimony(III) fluoride

69045-83-6

2,3-dichloro-5-(trichloromethyl)pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
With antimonypentachloride
52334-81-3

2-chloro-5-trifluoromethylpyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
With iron(III) chloride In water
With antimonypentachloride; iron(III) chloride In water
With chlorine; iron(III) chloride
Stage #1: 2-chloro-5-trifluoromethylpyridine under 15001.5 Torr; for 2h; Autoclave; Inert atmosphere;
Stage #2: With chlorine at 0 - 150℃; under 15001.5 Torr; for 20h; Temperature; Reagent/catalyst; Inert atmosphere;
52334-81-3

2-chloro-5-trifluoromethylpyridine

13283-01-7

tungsten(VI) chloride

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

72537-17-8

2-fluoro-3-chloro-5-(trifluoromethyl)pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
With FeCl3
7440-02-0

nickel

72537-17-8

2-fluoro-3-chloro-5-(trifluoromethyl)pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
With FeCl3 In (2S)-N-methyl-1-phenylpropan-2-amine hydrate

4-formyl-2,4-dichloro-5,5,5-trifluorovaleronitrile

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

3099-50-1

3-trichloromethyl-pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: phosphorus pentachloride / 16 h / 210 °C / Autoclave
2: hydrogen fluoride; iron(III) chloride; pyridine / 130 - 175 °C / Autoclave
View Scheme
Multi-step reaction with 3 steps
1: phosphorus pentachloride / 16 h / 210 °C / Autoclave
2: phosphorus pentachloride / 16 h / 210 °C / Autoclave
3: hydrogen fluoride; iron(III) chloride; pyridine / 130 - 175 °C / Autoclave
View Scheme

5-chloro-3-trichloromethyl pyridine

69045-84-7

2,3-dichloro-5-trifluoromethylpyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: phosphorus pentachloride / 16 h / 210 °C / Autoclave
2: hydrogen fluoride; iron(III) chloride; pyridine / 130 - 175 °C / Autoclave
View Scheme
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Chemistry


IUPAC Name: 2,3-Dichloro-5-(trifluoromethyl)pyridine
Canonical SMILES: C1=C(C=NC(=C1Cl)Cl)C(F)(F)F
InChI: InChI=1S/C6H2Cl2F3N/c7-4-1-3(6(9,10)11)2-12-5(4)8/h1-2H
InChIKey: ABNQGNFVSFKJGI-UHFFFAOYSA-N
Empirical Formula: C6H2Cl2F3N
Molecular Weight: 215.988 
EINECS: 410-340-5
Product Categories: Halides; Pyridines; Pyridine; Pyridine series; Chloropyridines; Halopyridines; C6Heterocyclic Building Blocks; Halogenated Heterocycles; Heterocyclic Building Blocks 
Appearance: Light yellow liquid
Index of Refraction: 1.47
Molar Refractivity: 39.11 cm3
Molar Volume: 140 cm3
Surface Tension: 30.9 dyne/cm
Density: 1.542 g/cm3
Flash Point: 79.4 °C
Enthalpy of Vaporization: 40.73 kJ/mol
Boiling Point: 188.5 °C at 760 mmHg
Vapour Pressure: 0.825 mmHg at 25°C
Melting Point of 2,3-Dichloro-5-trifluoromethyl pyridine (CAS NO.69045-84-7): 8-9 °C

Safety Profile

Hazard Codes: Xn,IrritantXi,  N
Risk Statements:
41:  Risk of serious damage to eyes 
43:  May cause sensitization by skin contact 
20/22:  Harmful by inhalation and if swallowed 
36/37/38:  Irritating to eyes, respiratory system and skin 
51/53:  Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment 
Safety Statements:
24:  Avoid contact with skin 
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
61:  Avoid release to the environment. Refer to special instructions safety data sheet
37/39:  Wear suitable gloves and eye/face protection 
RIDADR:UN 3082 9/PG 3
WGK Germany:2
Hazard Note:Irritant

Specification

 2,3-Dichloro-5-trifluoromethyl pyridine (CAS NO.69045-84-7), its Synonyms are Pyridine, 2,3-dichloro-5-(trifluoromethyl)- ; 2,3-Dichloro-5-(trifluoromethyl)pyridine .