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75-99-0

Basic Information
CAS No.: 75-99-0
Name: 2,2-Dichloropropionic acid
Article Data: 37
Molecular Structure:
Molecular Structure of 75-99-0 (2,2-Dichloropropionic acid)
Formula: C3H4Cl2O2
Molecular Weight: 142.97
Synonyms: Propionicacid, 2,2-dichloro- (8CI);2,2-DPA;2,2-Dichloropropanoic acid;2,2-Dichloropropionic acid;Alatex;Basinex P;DPA;Dalapon;Dalascam;NSC56352;Proprop;S 1315;S 95;S 95 (herbicide);Tripon;a,a-Dichloropropanoic acid;a,a-Dichloropropionic acid;
EINECS: 200-923-0
Density: 1.497 g/cm3
Melting Point: 166 °C (dec.)
Boiling Point: 187.5 °C at 760 mmHg
Flash Point: 76.1 °C
Solubility: 50.2 g/100 mL
Appearance: A colorless liquid.
Hazard Symbols: HarmfulXn
Risk Codes: 22-38-41-52/53
Safety: 26-39-61
Transport Information: UN 1760/3265
PSA: 37.30000
LogP: 1.26480
Synthetic route
2,2-dichloropropanal

2,2-dichloropropanal

75-99-0

2,2-Dichloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride; picoline hydrochloride; chlorine In chloroform at 65 - 70℃; for 24h; Oxidation;95%
With nitric acid; sodium nitrite In dichloromethane at 20℃; for 192h;66%

4-nitrosotetrahydro-2H-pyran-4-yl 2,2-dichloropropanoate

A

29943-42-8

Tetrahydro-4H-pyran-4-one

B

75-99-0

2,2-Dichloropropionic acid

C

10024-97-2

dinitrogen monoxide

Conditions
ConditionsYield
With water In methanol; aq. phosphate buffer at 20℃; for 24h; pH=7.4; Kinetics; Reagent/catalyst; Sealed tube;A n/a
B n/a
C 92%
802294-64-0

propionic acid

A

75-99-0

2,2-Dichloropropionic acid

B

598-78-7

(R,S)-2-chloropropionic acid

Conditions
ConditionsYield
With chlorine; pyrographite; propionic acid anhydride at 130℃; under 760.051 Torr; for 2.5h;A 10.47%
B 68.23%

pyruvic acid-(2,2-dichloro-propionic acid )-anhydride

A

75-99-0

2,2-Dichloropropionic acid

B

127-17-3

2-oxo-propionic acid

Conditions
ConditionsYield
Zieht schon an der Luft rasch Wasser an und zerfaellt;
598-78-7

(R,S)-2-chloropropionic acid

75-99-0

2,2-Dichloropropionic acid

Conditions
ConditionsYield
With chlorine; phosphorus trichloride at 180℃;
With phosphonic acid; chlorine at 180℃;
56511-21-8

2,2-dichloro-propionic acid anilide

75-99-0

2,2-Dichloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride at 140℃;
75265-14-4

p-methoxyphenyl 2,2-dichloropropanoate

A

75-99-0

2,2-Dichloropropionic acid

B

150-76-5

4-methoxy-phenol

Conditions
ConditionsYield
With hydrogenchloride; water In various solvent(s) at 25℃; Rate constant; Thermodynamic data; Kinetics; var. temps.; ΔG(activ.), ΔH(activ.), ΔS(activ.), ΔCp(activ.);
With hydrogenchloride; water In various solvent(s) at 25℃; Mechanism;
With 2-Butoxyethanol; water at 20 - 48℃; Rate constant; Thermodynamic data; ΔG<*>, ΔH<*>, ΔS<*>, ΔCp<*>; reagents ratio;
With water at 25℃; under 750.06 Torr; Rate constant; Thermodynamic data; hydrolysis, ΔGp(excit.), ΔHp(excit.), ΔSp(excit.), ΔUv(excit.), ΔSv(excit.),solvent and pressure dependence;
75265-14-4

2,2-Dichloro-propionic acid p-tolyl ester

A

75-99-0

2,2-Dichloropropionic acid

B

150-76-5

4-methoxy-phenol

Conditions
ConditionsYield
With at-poly(methacrylic acid) In water at 25℃; Rate constant; Thermodynamic data; Kinetics; ΔG+, ΔH+; further inhibitors;
79-43-6

dichloro-acetic acid

77-78-1

dimethyl sulfate

75-99-0

2,2-Dichloropropionic acid

Conditions
ConditionsYield
With n-butyllithium; lithium diisopropyl amide 1.) THF, hexane, -78 deg C, 5 min., 2.) room temp., 1 h; Yield given. Multistep reaction;
598-78-7

(R,S)-2-chloropropionic acid

A

75-99-0

2,2-Dichloropropionic acid

B

3278-46-4

chloropon

C

39881-29-3

2,2,3,3-tetrachloropropanoic acid

Conditions
ConditionsYield
With chlorine; phosphorus trichloride for 4h; Heating; Yields of byproduct given;A 9.38 g
B n/a
C n/a
With chlorine; phosphorus trichloride for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
With chlorine; phosphorus trichloride for 4h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
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Chemistry

Product Name: 2,2-Dichloropropionic acid (CAS NO.75-99-0)


Molecular Formula: C3H4Cl2O2
Molecular Weight: 142.97g/mol
Mol File: 75-99-0.mol
Einecs: 200-923-0
Appearance: Clear yellow liquid
Melting Point: 166°C (dec.)
Boiling point: 187.5 °C at 760 mmHg
Storage Temperature: 0-6°C
Flash Point: 76.1 °C
Density: 1.497 g/cm3
Refractive index: 1.4544
Water Solubility: 50.2 g/100 mL
Sensitive: Moisture Sensitive
Surface Tension: 43.5 dyne/cm
Enthalpy of Vaporization: 46.71 kJ/mol
Vapour Pressure: 0.282 mmHg at 25°C
XLogP3-AA: 1.3
H-Bond Donor: 1
H-Bond Acceptor: 2
Product Categories: API intermediates; Aliphatic halogenatedAlphabetic; D; DA - DH; Herbicides; Pesticides&Metabolites

Toxicity Data With Reference

1.    

skn-rbt 100 µg/24H open

    AIHAAP    American Industrial Hygiene Association Journal. 23 (1962),95.
2.    

mmo-omi 500 ppm

    IJEBA6    Indian Journal of Experimental Biology. 11 (1973),114.
3.    

skn-rat LD50:>5 g/kg

    FAATDF    Fundamental and Applied Toxicology. 7 (1986),299.

Consensus Reports

EPA Genetic Toxicology Program. Reported in EPA TSCA Inventory.

Safety Profile

A corrosive with low toxicity by skin contact. A skin irritant. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl.
Safety Information of 2,2-Dichloropropionic acid (CAS NO.75-99-0):
Hazard Codes: Xn,Xi,F
Risk Statements: 22-38-41-52/53-40-36/37/38 
22:  Harmful if swallowed
36:  Irritating to the eyes 
37:  Irritating to the respiratory system
38:  Irritating to the skin
40:  Limited evidence of a carcinogenic effect 
41:  Risk of serious damage to eyes 
53:  May cause long-term adverse effects in the aquatic environment
Safety Statements: 26-39-61-36-16
16:  Keep away from sources of ignition - No smoking
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:  Wear suitable protective clothing
39:  Wear eye/face protection
61:  Avoid release to the environment. Refer to special instructions safety data sheet

Standards and Recommendations

OSHA PEL: TWA 1 ppm
ACGIH TLV: TWA 5 ppm, Not Classifiable as a Human Carcinogen
DFG MAK: 1 ppm (5.9 mg/m3)

Specification

 2,2-Dichloropropionic acid ,its CAS NO. is 75-99-0,the synonyms is Dichloropropionicacid ; 2,2-Dichloropropanoic acid ; 2,2-Dichloro-propanoicaci ; 2,2-Dichloropropanoicacid ; 2,2-Dichloro-propionicaci ; 2,2-DPA ; Acide2,2-Dichloropropionique ; Alatex .