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754-96-1

Basic Information
CAS No.: 754-96-1
Name: 1H,1H,10H,10H-PERFLUORO-1,10-DECANEDIOL
Article Data: 2
Molecular Structure:
Molecular Structure of 754-96-1 (1H,1H,10H,10H-PERFLUORO-1,10-DECANEDIOL)
Formula: C10H6F16O2
Molecular Weight: 462.131
Synonyms: 1,8-Dimethylolperfluorooctane;1H,1H,10H,10H-Perfluoro-1,10-decanediol;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-Hexadecafluoro-1,10-decanediol;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol;
Density: 1.673 g/cm3
Melting Point: 135-137 °C(lit.)
Boiling Point: 271 °C at 760 mmHg
Flash Point: 117.7 °C
Appearance: white powder and chunks
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 37/39-26
PSA: 40.46000
LogP: 4.05340
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Specification

The 1,10-Decanediol,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluoro- with CAS registry number of 754-96-1 is also known as 1H,1H,10H,10H-Perfluoro-1,10-decanediol and 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-Hexadecafluorodecane-1,10-diol. Its systematic name is 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-Hexadecafluorodecane-1,10-diol. Besides, it is white powder and chunks, which belongs to categories of Organic Building Blocks; Oxygen Compounds; Polyols.

Physical properties about this chemical are: (1) ACD/LogP: 5.36; (2) # of Rule of 5 Violations: 1; (3) ACD/LogD (pH 5.5): 5.36; (4) ACD/LogD (pH 7.4): 5.36; (5) ACD/BCF (pH 5.5): 7019.34; (6) ACD/BCF (pH 7.4): 7019.29; (7) ACD/KOC (pH 5.5): 19713.77; (8) ACD/KOC (pH 7.4): 19713.64; (9) #H bond acceptors: 2; (10) #H bond donors: 2; (11) #Freely Rotating Bonds: 11; (12) Polar Surface Area: 18.46 Å2  ; (13) Index of Refraction: 1.313; (14) Molar Refractivity: 53.79 cm3; (15) Molar Volume: 276.1 cm3; (16) Polarizability: 21.32×10-24 cm3; (17) Surface Tension: 18.9 dyne/cm; (18) Density: 1.673 g/cm3; (19) Flash Point: 117.7 °C; (20) Enthalpy of Vaporization: 59.12 kJ/mol; (21) Boiling Point: 271 °C at 760 mmHg; (22) Vapour Pressure: 0.000868 mmHg at 25°C.

Preparation of 1,10-Decanediol,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluoro-: this chemical is prepared by reaction of hexadecafluoro-decanedioic acid diethyl ester.

The reaction needs reagent LiAlH4 and solvent tetrahydrofuran at the temperature of 0 ℃ for 1 hour and reflux for 12 hours. The yield is about 90%.

Uses of 1,10-Decanediol,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluoro-: It is used to produce other chemicals. For example, it is used to produce 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexafluorodecyl 1,10-ditosylate.

The reaction needs solvent pyridine at the temperature of 0 ℃. The yield is about 80%.

When you are using this chemical, please be cautious about it as the following:
As a chemical, it is irritating to eyes, respiratory system and skin. During using it, wear suitable gloves and eye/face protection. If contact with eyes accidently, rinse immediately with plenty of water and seek medical advice.

People can use the following data to convert to the molecule structure:
(1) SMILES: FC(F)(C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)CO)C(F)(F)CO;
(2) InChI: InChI=1/C10H6F16O2/c11-3(12,1-27)5(15,16)7(19,20)9(23,24)10(25,26)8(21,22)6(17,18)4(13,14)2-28/h27-28H,1-2H2;
(3) InChIKey: NSKCTPBWPZPFHW-UHFFFAOYAO;
(4) Std. InChI: InChI=1S/C10H6F16O2/c11-3(12,1-27)5(15,16)7(19,20)9(23,24)10(25,26)8(21,22)6(17,18)4(13,14)2-28/h27-28H,1-2H2;
(5) Std. InChIKey: NSKCTPBWPZPFHW-UHFFFAOYSA-N