Detail of "77029-01-7"

CAS Number:
77029-01-7
Name:
1-Naphthalenecarbonitrile,6-methoxy-
Molecular Structure:
Formula:
C₁₂H₉NO
Molecular Weight:
183.21
Synonyms:
1-Naphthonitrile,6-methoxy- (4CI);5-Cyano-2-methoxynaphthalene;6-Methoxy-1-cyanonaphthalene;6-Methoxy-1-naphthalenecarbonitrile;
Density:
1.16 g/cm³
Boiling Point:
348.2 °C at 760 mmHg
Flash Point:
146.9 °C

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Synthesis of a conjugated nitrile from a benzylic ketone via a cyanotrimethylsilane adduct: 3,4-dihydro-6-methoxynaphthalene-1-carbonitrile: Synthesis of a conjugated nitrile from a benzylic ketone via a cyanotrimethylsilane adduct: 3,4-dihydro-6-methoxynaphthalene-1-carbonitrile. Jacobs, Stephen A.; Harvey, Ronald G. (Ben May Lab., Univ. Chicago, Chicago, IL 60637, USA). J. Org. Chem., 48(25), 5134-5 (English) 1983. 1078-19-9 and 77029-01-7 are cas registry numbers of chemicals which are used as reagents here. CODEN: JOCEAH. ISSN: 0022-3263. DOCUMENT TYPE: Journal CA Section: 25 (Benzene, Its Derivatives, and Condensed Benzenoid Compounds) Section cross-reference(s): 32 A convenient one-pot synthesis of 3,4-dihydro-6-methoxynaphthalene-1-carbonitrile (I) and its dehydrogenation to the steroid intermediate II were described. Addn. of Me3SiCN to 6-methoxy-1-tetralone catalyzed by BF3 gave an adduct which with POCl3 in pyridine gave I. Dehydrogenation of I was accomplished by heating with S-Pd/C. .