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CAS No.: | 79387-69-2 |
---|---|
Name: | 5-Iodo-2-pyrimidone |
Article Data: | 10 |
Molecular Structure: | |
Formula: | C4H3 I N2 O |
Molecular Weight: | 221.985 |
Synonyms: | 2-Hydroxy-5-iodopyrimidine;5-Iodo-2(1H)-pyrimidinone; 5-Iodo-2-hydroxypyrimidine; 5-Iodo-2-pyrimidinone;5-Iodopyrimidin-2-ol |
Density: | 2.403g/cm3 |
Boiling Point: | 393.6ºC at 760 mmHg |
Flash Point: | 191.8ºC |
PSA: | 46.01000 |
LogP: | 0.78680 |
2-hydroxypyrimidine hydrochloride
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With methanol; iodine; silver sulfate at 20℃; for 16h; Darkness; | 94% |
Pyrimidin-2(1H)-one
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With N-iodo-succinimide In N,N-dimethyl-formamide for 48h; Ambient temperature; | 77.5% |
With N-iodo-succinimide In N,N-dimethyl-formamide | 11.35 g (77.5%) |
With N-iodo-succinimide In N,N-dimethyl-formamide | 11.35 g (77.5%) |
2-pyrimidinone hydrochloride
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With sodium dihydrogen phosphate; sodium iodine dichloride In water at 65℃; for 1.66667h; | 75% |
With Iodine monochloride; sodium chloride In water at 60℃; for 1h; | |
With N-iodo-succinimide In N,N-dimethyl-formamide at 20℃; for 48h; | |
With Iodine monochloride; acetic acid In water at 45 - 48℃; for 6h; Temperature; |
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