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| CAS No.: | 80532-66-7 |
|---|---|
| Name: | methyl α,β-epoxy-α-methylcinnamate |
| Article Data: | 10 |
| Molecular Structure: | |
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| Formula: | N/A |
| Molecular Weight: | 192.214 |
| Synonyms: | methyl α,β-epoxy-α-methylcinnamate |
| Density: | 1.168±0.06 g/cm3(Predicted) |
| Boiling Point: | 73-74 °C(Press: 0.2 Torr) |
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- 17639-93-9
2-chloro-propionic acid methyl ester
- 100-52-7
benzaldehyde
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In N,N-dimethyl-formamide 1.) 20 deg C, 72 h, 2.) 40 deg C, 24 h; | 80% |
| With sodium methylate In methanol; toluene at 0 - 20℃; Darzens condensation; | |
| With ethanol; sodium ethanolate |
- 21370-57-0, 22946-43-6, 25692-59-5
methyl 2-methyl-3-phenylacrylate
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| With 3-chloro-benzenecarboperoxoic acid In tetrachloromethane for 3h; Reflux; | 67% |
- 186581-53-3, 908094-01-9
diazomethane
- 25547-51-7
trans-2-methyl-3-phenyloxiranecarboxylic acid
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
- 92817-97-5
(2S,3R)-2-Hydroxy-3-methanesulfonyloxy-2-methyl-3-phenyl-propionic acid methyl ester
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| With sodium hydride In diethyl ether Yield given; |
- 92817-31-7
(2S,3S)-2-Hydroxy-3-methanesulfonyloxy-2-methyl-3-phenyl-propionic acid methyl ester
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| With sodium hydride In diethyl ether Yield given; |
- 100-52-7
benzaldehyde
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 1.) EtMgBr / 1.) THF, -78 deg C, 10 min View Scheme |
- 92817-30-6
methyl (syn-2,3-dihydroxy-2-methyl-3-phenyl)propionate
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: pyridine / 1.) overnight; 2.) 0 deg C, 1 h 2: NaH in mineral oil / diethyl ether View Scheme |
- 92817-29-3
(2RS,3RS)-2-methyl-2,3-dihydroxybenzenepropanoate
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: pyridine / 1.) overnight; 2.) 0 deg C, 1 h 2: NaH in mineral oil / diethyl ether View Scheme |
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: K2CO3 / methanol / 3 h / Ambient temperature 2: pyridine / 1.) overnight; 2.) 0 deg C, 1 h 3: NaH in mineral oil / diethyl ether View Scheme | |
| Multi-step reaction with 3 steps 1: K2CO3 / methanol / 3 h / Ambient temperature 2: pyridine / 1.) overnight; 2.) 0 deg C, 1 h 3: NaH in mineral oil / diethyl ether View Scheme |
- 1199-77-5
α-methylcinnamic acid
- 80532-66-7
methyl α,β-epoxy-α-methylcinnamate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: thionyl chloride / 3 h / 20 °C 2: 3-chloro-benzenecarboperoxoic acid / tetrachloromethane / 3 h / Reflux View Scheme |
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