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81262-69-3

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Basic Information
CAS No.: 81262-69-3
Name: N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine
Article Data: 1
Molecular Structure:
Molecular Structure of 81262-69-3 (N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine)
Formula: N/A
Molecular Weight: 207.272
Synonyms: N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine
Synthetic route
81279-27-8

1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 24h; Heating;
20850-43-5

5-(chloromethyl)-1,3-benzodioxole

sodium-compound of O-methyl-triethylene glycol

sodium-compound of O-methyl-triethylene glycol

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1.) LDA, hexamethylphosphoramide / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, overnight
2: triethylamine / H2O; acetone / 0 °C
3: NaN3 / H2O; acetone / 0.75 h / Ambient temperature
4: toluene / 0.5 h / Heating
5: Heating
6: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme

5-(2-Isocyanato-2-methyl-propyl)-benzo[1,3]dioxole

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Heating
2: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme
54508-53-1

2,2-dimethyl-3-<3,4-(methylenedioxy)phenyl>propionic acid

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: triethylamine / H2O; acetone / 0 °C
2: NaN3 / H2O; acetone / 0.75 h / Ambient temperature
3: toluene / 0.5 h / Heating
4: Heating
5: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme

3-Benzo[1,3]dioxol-5-yl-2,2-dimethyl-propionyl azide

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene / 0.5 h / Heating
2: Heating
3: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme

C15H18O6

81262-69-3

N-methyl-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethylamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: NaN3 / H2O; acetone / 0.75 h / Ambient temperature
2: toluene / 0.5 h / Heating
3: Heating
4: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme
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