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84996-11-2

Basic Information
CAS No.: 84996-11-2
Name: 4-(Ethylsulphonyl)-2-nitrophenol
Article Data: 4
Molecular Structure:
Molecular Structure of 84996-11-2 (4-(Ethylsulphonyl)-2-nitrophenol)
Formula: C8H9NO5S
Molecular Weight: 231.229
Synonyms: EINECS 284-947-7;4-hydroxy-3-nitrophenylethylsulfone;OR8348;
Density: 1.463g/cm3
Melting Point: 137-139oC
Boiling Point: 410.3°Cat760mmHg
Flash Point: 201.9°C
PSA: 108.57000
LogP: 2.69800
Synthetic route
859537-79-4

4-hydroxy-phenyl-ethylsulfone

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
With nitric acid; acetic acid at 80℃; for 3h;100%
74159-80-1

1-chloro-4-(ethylsulphonyl)-2-nitrobenzene

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
With sodium hydroxide at 95℃; for 3h; Temperature; Autoclave;97%
51572-44-2

4-(ethylsulfonyl)-1-methoxy-2-nitrobenzene

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
With formic acid; hydrogen bromide at 90℃; for 30h; Temperature;92%
1195-46-6

4-(ethylthio)phenol

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Oxone / water; ethanol / 18 h / 20 °C
2: nitric acid; acetic acid / 3 h / 80 °C
View Scheme
637-89-8

4-sulfanylphenol

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / 2 h / 20 °C
2: Oxone / water; ethanol / 18 h / 20 °C
3: nitric acid; acetic acid / 3 h / 80 °C
View Scheme
5120-72-9

4-chlorophenyl ethyl sulfide

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dihydrogen peroxide; sodium tungstate (VI) dihydrate / ethyl acetate / 5 h / 30 - 55 °C / Large scale
2: nitric acid; sulfuric acid / 2 h / 0 - 20 °C / Large scale
3: sodium hydroxide / 3 h / 95 °C / Autoclave
View Scheme
7205-80-3

1-(ethylsulfonyl)-4-chlorobenzene

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nitric acid; sulfuric acid / 2 h / 0 - 20 °C / Large scale
2: sodium hydroxide / 3 h / 95 °C / Autoclave
View Scheme
98-68-0

4-methoxy-phenyl-sulphonyl chloride

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium sulfite / water; tetrahydrofuran / 20 h / -5 - 0 °C
2: methanol / 2 h / 65 °C
3: nitric acid / 70 °C
4: hydrogen bromide; formic acid / 30 h / 90 °C
View Scheme
Multi-step reaction with 4 steps
1: sodium sulfite / water; tetrahydrofuran / 20 h / -5 - 0 °C
2: ethanol / 2 h / 80 °C
3: nitric acid / 70 °C
4: hydrogen bromide; formic acid / 30 h / 90 °C
View Scheme
6462-50-6

sodium 4-methoxybenzenesulfinate

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: methanol / 2 h / 65 °C
2: nitric acid / 70 °C
3: hydrogen bromide; formic acid / 30 h / 90 °C
View Scheme
Multi-step reaction with 3 steps
1: ethanol / 2 h / 80 °C
2: nitric acid / 70 °C
3: hydrogen bromide; formic acid / 30 h / 90 °C
View Scheme
7205-79-0

1-(ethylsulfonyl)-4-methoxybenzene

84996-11-2

4-(ethylsulfonyl)-2-nitro-phenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nitric acid / 70 °C
2: hydrogen bromide; formic acid / 30 h / 90 °C
View Scheme
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    4-(ETHYLSULFONYL)-2-NITROPHENOLAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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