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915095-94-2

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Basic Information
CAS No.: 915095-94-2
Name: (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan
Article Data: 12
Molecular Structure:
Molecular Structure of 915095-94-2 ((3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan)
Formula: C17H16ClIO2
Molecular Weight: 414.67
Synonyms: 查看更多英文别名"> (S)-3-(4-(2-Chloro-5-iodobenzyl)phenoxy)tetrahydrofuran;(3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan;(S)-3-(4-(2-chloro-5-iodobenzyl)phenoxy)-tetrahydrofuran;Empagliflozin Intermediate1;Empagliflozin II;Empagliflozin intermediate;查看更多英文别名
EINECS: 619-599-0
Density: 1.578±0.06 g/cm3 (20 oC 760 Torr)
Boiling Point: 476.0±45.0 °C(Predicted)
PSA: 18.46000
LogP: 4.70310
Related products
Synthetic route
915095-87-3

(S)-(2-chloro-5-iodophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
With aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane In toluene at 0 - 23℃; for 2.5h;93%
With aluminum (III) chloride; sodium tetrahydroborate In tetrahydrofuran for 5h; Reflux;90%
With potassium borohydride; trifluoroacetic acid In tetrahydrofuran at 0 - 20℃; for 0.5h;85%
1459754-32-5

4-(2-chloro-5-iodobenzyl)phenol

112052-11-6

toluene-4-sulfonic acid (S)-(tetrahydrofuran-3-yl)ester

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; potassium iodide In acetonitrile at 50 - 55℃; Large scale;90.1%

(S)-3-(4-(5-iodo-2-aminobenzyl)phenoxy)tetrahydrofuran

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Stage #1: (S)-3-(4-(5-iodo-2-aminobenzyl)phenoxy)tetrahydrofuran With hydrogenchloride; sodium nitrite In water at -10 - 0℃; for 2.5h;
Stage #2: With hydrogenchloride; copper(l) chloride In water at 20 - 80℃; for 3h;		75.2%
462-06-6

fluorobenzene

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide / 5 h / 25 - 30 °C
2: potassium tert-butylate / tetrahydrofuran / 3 h / 16 - 25 °C
3: 1,1,3,3-Tetramethyldisiloxane / aluminum (III) chloride / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / 5 h / 25 - 30 °C
1.2: 6 h / 20 - 30 °C
2.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C
2.2: 1.83 h / 20 - 21 °C
3.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; aluminum (III) chloride / N,N-dimethyl-formamide / 25 - 45 °C / Industry scale
2.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C / Industry scale
3.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C / Industry scale
3.2: 20 - 51 °C / Industry scale
View Scheme
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h
1.2: 1 h / 0 - 5 °C
2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 16 - 25 °C
3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 5 - 10 °C
View Scheme
19094-56-5

2-chloro-5-iodobenzoic acid

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide / 5 h / 25 - 30 °C
2: potassium tert-butylate / tetrahydrofuran / 3 h / 16 - 25 °C
3: 1,1,3,3-Tetramethyldisiloxane / aluminum (III) chloride / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / 5 h / 25 - 30 °C
1.2: 6 h / 20 - 30 °C
2.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C
2.2: 1.83 h / 20 - 21 °C
3.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; aluminum (III) chloride / N,N-dimethyl-formamide / 25 - 45 °C / Industry scale
2.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C / Industry scale
3.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C / Industry scale
3.2: 20 - 51 °C / Industry scale
View Scheme
915095-86-2

(2-chloro-5-iodophenyl)(4-fluorophenyl)methanone

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 3 h / 16 - 25 °C
2: 1,1,3,3-Tetramethyldisiloxane / aluminum (III) chloride / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C
1.2: 1.83 h / 20 - 21 °C
2.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C
View Scheme
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 4 h / 16 - 25 °C / Industry scale
2.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 18 - 26 °C / Industry scale
2.2: 20 - 51 °C / Industry scale
View Scheme
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
2: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 0 - 23 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 20 °C
2: sodium tetrahydroborate; aluminum (III) chloride / tetrahydrofuran / 5 h / Reflux
View Scheme
281652-58-2

2-chloro-5-iodobenzoylchloride

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: aluminum (III) chloride / 1 h / 0 - 25 °C
2: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
3: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 0 - 23 °C
View Scheme
Multi-step reaction with 3 steps
1: aluminum (III) chloride / dichloromethane / 6 h / -5 °C
2: potassium tert-butylate / tetrahydrofuran / 20 °C
3: sodium tetrahydroborate; aluminum (III) chloride / tetrahydrofuran / 5 h / Reflux
View Scheme
108-95-2

phenol

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: polyposphoric acid / 50 - 85 °C
2: potassium iodide; potassium carbonate / acetonitrile / 50 - 55 °C
3: potassium borohydride; trifluoroacetic acid / tetrahydrofuran / 0.5 h / 0 - 20 °C
View Scheme
1459754-40-5

(2-chloro-5-iodophenyl)(4-hydroxyphenyl)methanone

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium iodide; potassium carbonate / acetonitrile / 50 - 55 °C
2: potassium borohydride; trifluoroacetic acid / tetrahydrofuran / 0.5 h / 0 - 20 °C
View Scheme
35421-08-0

4-hydroxybenzyl chloride

915095-94-2

(3S)-3-[4-[(2-chloro-5-iodophenyl)methyl]phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sulfonyl chloride / dichloromethane / 3 h / -5 - 0 °C
1.2: 4.5 h / Reflux
2.1: zinc(II) chloride / ethyl acetate / 6 h / Reflux
3.1: hydrogenchloride; sodium nitrite / water / 2.5 h / -10 - 0 °C
3.2: 3 h / 20 - 80 °C
View Scheme
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    Name: (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan Synonyms: Empagliflozin intermediate CAS: 915095-94-2 MF: C17H16ClIO2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Appli

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  • Empagliflozin Intermediate 915095-94-2 API Manufacturer

  • Casno:

    915095-94-2

    Empagliflozin Intermediate 915095-94-2 API Manufacturer

    Min.Order: 10 Gram

    FOB Price:  USD $ 0.0-0.0

    Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best serv

    Hubei Xinrunde Chemical Co., Ltd. dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredient(s)

  •  Hubei Langyou International Trading Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+8618874586545

    Address:No.43, Xinandu Industrial Park, East and West Lake District, Wuhan, Hubei, China

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  • (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan 915095-94-2

  • Casno:

    915095-94-2

    (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan 915095-94-2

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

    Shanghai Upbio Tech Co.,Ltd (Former Onchem (China)Co.,Ltd) is a comprehensive manufacturer and an international distribution of chemicals throughout the world, The predecessor of

  •  Shanghai Upbio Tech Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-52196435

    Address:No.2 Floor,No.979 Yunhan Rd,Nicheng,Pudong New Area,Shanghai,China

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  • (S)-3-(4-(2-Chloro-5-iodobenzyl)phenoxy)tetrahydrofuran WITH CAS:915095-94-2

  • Casno:

    915095-94-2

    (S)-3-(4-(2-Chloro-5-iodobenzyl)phenoxy)tetrahydrofuran WITH CAS:915095-94-2

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 720.0-720.0

    Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

    Baoji Guokang Healthchem co.,ltd located in Baoji High-tech Zone,is epitomizing international,cooperative and honest.We are a young company full of action and energy,and our profes

  •  Baoji Guokang Healthchem co.,ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-917-3909592

    Address:China

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  • (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

  • Casno:

    915095-94-2

    MSDS/COA Download

    (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 12.0-16.0

    1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

    Hebei Quanhe Biotechnology Co. LTD. is an enterprise specializing in the research and development, production and trade of pharmaceutical intermediates, apis and chemical raw mater

  •  Hebei Quanhe Biotechnology Co. LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+8619003195089

    Address:Haida Business Center, Xiangdu District

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  • (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

  • Casno:

    915095-94-2

    (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

    The company is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds,

  •  Henan Wentao Chemical Product Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-370-2722992

    Address:32 Room, 5th Floor, Building 11, No. 6 Yinxing Road, High-tech Industrial Development Zone, Zhengzhou City, Henan Province

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  • (3S)-3-(4-(2-chloro-5-iodobenzyl)phenoxy)tetrahydrofuran

  • Casno:

    915095-94-2

    (3S)-3-(4-(2-chloro-5-iodobenzyl)phenoxy)tetrahydrofuran

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua

    Triumph International Development Limilted is engaged in the API, pharmaceutical intermediates research and developmen.Adhering to the "customer first" business philosophy,we suppl

  •  Triumph International Development Limilted

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-536-7971999

    Address:Yinhai Road,Shouguang

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  • (3S)-3-[4-[(2-CHLORO-5-IODOPHENYL)METHYL]PHENOXY]TETRAHYDRO-FURAN 915095-94-2

  • Casno:

    915095-94-2

    (3S)-3-[4-[(2-CHLORO-5-IODOPHENYL)METHYL]PHENOXY]TETRAHYDRO-FURAN 915095-94-2

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

  •  Afine Chemicals Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

  • Casno:

    915095-94-2

    (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

    Hangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service profession

  •  Hangzhou Keyingchem Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85378921

    Address:Jintong international Building, No.113,Huayuangang Street, Gong shu District, Hangzhou,Zhejiang, China.

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  • (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

  • Casno:

    915095-94-2

    (3S)-3-[4-[(2-Chloro-5-iodophenyl)methyl]phenoxy]tetrahydro-furan

    Min.Order: 4 Kilogram

    FOB Price:  USD $ 0.0-0.0

    A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

    T&W GROUP was established in 2007, headquartered in Shanghai, China. By integrating people, technology and potential, we endeavor to work for a better life. We are in the business

  •  SHANGHAI T&W PHARMACEUTICAL CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-61551611

    Address:601, No. 1, 2277 Nong, Zu Chongzhi Road, Zhangjiang Hightech. Park, Pudong

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  • Featured products (3S)-3-[4-[(2-Chloro-5-iodophenyl)Methyl]phenoxy]tetrahydro-furan（915095-94-2）

  • Casno:

    915095-94-2

    Featured products (3S)-3-[4-[(2-Chloro-5-iodophenyl)Methyl]phenoxy]tetrahydro-furan（915095-94-2）

    Min.Order: 100 Gram

    FOB Price:  USD $ 0.0-0.0

    Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

    We are a team of industry experts, dedicated to delivering the best chemical solutions from quality suppliers across China. Putting our customers first, we take a holistic approach

  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-189 8945 5137

    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

       Inquiry Now

  • (S)-4-iodo-1-chloro-2-(4-tetrahydrofuran-3-yloxy-benzyl)-benzene

  • Casno:

    915095-94-2

    (S)-4-iodo-1-chloro-2-(4-tetrahydrofuran-3-yloxy-benzyl)-benzene

    Min.Order: 10 Gram

    FOB Price:  USD $ 100.0-100.0

    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

  •  Zibo Hangyu Biotechnology Development Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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